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1.
This study reports the effect of different types of thermo-mechanical excursion (TME) on growth of intermetallic compound (IMC) layer formed at the interface of Sn-3.0%Ag-0.5%Cu solder and Cu substrate. 1 mm thick solder joints were prepared by reflowing at 270 °C for either 60 or 90 s. Solder joints were then exposed to one of the following TME: (i) isothermal aging at 60 °C for 48, 96 and 144 h, (ii) thermal cycling between − 25 and 125 °C for 100, 200 and 400 cycles, and (iii) thermo-mechanical cycling between − 25 and 125 °C for 100, 200 and 400 cycles, wherein a shear strain of 10% per cycle was imposed on the joint. Finite element analysis (FEA) was performed to ascertain the effects of imposed shear strain and volumetric expansion due to the formation of IMC on the stress field in the solder joint. Irrespective of the type of TME, the thickness of the IMC layer increased with time. However, IMC thickness increased relatively more rapidly under thermo-mechanical cycling condition, indicating strain enhanced coarsening of the interfacial IMC layer. FEA showed that high stresses were generated in the IMC layer and near solder-IMC interface due to the formation of IMC layer as well as imposed external strain, which might then not only enhance the IMC growth kinetics, but also affect the morphology of the IMC layer.  相似文献   

2.
A robust solder joint in crystalline silicon solar cell assembly is necessary to ensure its thermo-mechanical reliability. The solder joint formed using optimal parameter setting accumulates minimal creep strain energy density which leads to longer fatigue life. In this study, thermo-mechanical reliability of solder joint in crystalline silicon solar cell assembly is evaluated using finite element modelling (FEM) and Taguchi method. Geometric models of the crystalline silicon solar cell assembly are built and subjected to accelerated thermal cycling utilizing IEC 61215 standard for photovoltaic panels. In order to obtain the model with minimum accumulated creep strain energy density, the L9 (33) orthogonal array was applied to Taguchi design of experiments (DOE) to investigate the effects of IMC thickness (IMCT), solder joint width (SJW) and solder joint thickness (SJT) on the thermo-mechanical reliability of solder joints. The solder material used in this study is Sn3.8Ag0.7Cu and its non-linear creep deformation is simulated using Garofalo-Arrhenius creep model. The results obtained indicate that solder joint thickness has the most significant effect on the thermo-mechanical reliability of solder joints. Analysis of results selected towards thermo-mechanical reliability improvement shows the design with optimal parameter setting to be: solder joint thickness — 20 μm, solder joint width — 1000 μm, and IMC thickness — 2.5 μm. Furthermore, the optimized model has the least damage in the solder joint and shows a reduction of 47.96% in accumulated creep strain energy density per cycle compared to the worst case original model. Moreover, the optimized model has 16,264 cycles to failure compared with the expected 13,688 cycles to failure of a PV module designed to last for 25 years.  相似文献   

3.
The eutectic Au80Sn20 solder alloy has been applied in semiconductor assemblies and other industries for years. Due to some superior physical properties, Au/Sn alloy gradually becomes one of the best materials for soldering in electronic devices and components packaging but the voids growth in AuSn solder joints is one of the many critical factors governing the solder joint reliability. Voids may degrade the mechanical robustness of the die attach and consequently affect the reliability and thermal conducting performance of the assembly. Severe thermal cycles [− 55 °C/+175 °C] have highlighted degradations in AuSn die attach solder. The inspection of as-prepared die-attachments by X-ray and SEM (observation of cross-section) shows that the initial voids sizes were increased and a propagation of transverse cracks inside the joint between voids has appeared after ageing, it was featured also the existence of the IMC typical scallop-shape morphology with the phase structure of (Ni, Au)3Sn2 on as-reflowed joints. In this paper, we evaluate the origin of these degradations and ways to address them.  相似文献   

4.
《Microelectronics Reliability》2015,55(11):2391-2395
In this paper, vibration tests are conducted to investigate the influence of temperature on PCB responses. A set of combined tests of temperature and vibration is designed to evaluate solder interconnect reliability at 25 °C, 65 °C and 105 °C. Results indicate that temperature significantly affects PCB responses, which leads to remarkable differences in vibration loading intensity. The PCB eigenfrequency shifts from 290 Hz to 276 Hz with an increase of test temperature from 25 °C to 105 °C, during which the peak strain amplitude is almost the same.Vibration reliability of solder interconnects is greatly improved with temperature rise from 25 °C to 105 °C. Mean time to failure (MTTF) of solder joint at 65 °C and 105 °C is increased by 70% and 174% respectively compared to that of solder joint at 25 °C. Temperature dominates crack propagation path of solder joint during vibration test. Crack propagation path is changed from the area between intermetallic compound (IMC) layer and Cu pad to the bulk solder with temperature increase.  相似文献   

5.
SnPb-SnAgCu mixed solder joints with Sn-Pb soldering Sn-Ag-Cu Pb-free components are inevitably occurred in the high reliability applications. In this study, the interfacial behaviors in Sn-37Pb and Sn-3.0Ag-0.5Cu mixed solder joints was addressed and compared with Sn-37Pb solder joints and Sn-3.0Ag-0.5Cu solder joints with the influence from isothermal aging and electromigration. Considering the difference on the melting point between Sn-3.0Ag-0.5Cu and Sn-37Pb solder, two mixed solder joints: partial mixing and full mixing between Sn-Pb and Sn-Ag-Cu solders were reached with the peak reflowing temperature of 190 and 250 °C, respectively. During isothermal aging, the intermetallic compound (IMC) layer increased with aging time and its growth was diffusion controlled. There was also no obvious affect from the solder composition on IMC growth. After electromigration with the current density of 2.0 × 103 A/cm2, Sn-37Pb solder joints showed the shortest lifetime with the cracks observed at the cathode for the stressing time < 250 h. In Sn-3.0Ag-0.5Cu Pb-free solder joints, current stressing promoted the growth of IMC layer at the interfaces, but the growing rate of IMC at the anode interface was far faster than that at the cathode interface. Therefore, there existed an obvious polarity effect on IMC growth in Sn-Ag-Cu Pb-free solder joints. After Sn-37Pb was mixed with Sn-3.0Ag-0.5Cu Pb-free solder, whether the partial mixing or the full mixing between Sn-Pb and Sn-Ag-Cu can obviously depress both the crack formation at the cathode side and the IMC growth at the anode.  相似文献   

6.
The vibration reliability of lead-free solder joints of Package-on-Package (PoP) is investigated by experimental tests and finite element method (FEM) simulations in this paper. A 14 × 14 mm two-tier PoP module was selected for this study. The natural frequencies and modes were determined by FEM and verified by experimental tests. The printed circuit board (PCB) assemblies are tested under harmonic vibration. Vibration test results show that the vibration reliability of top package is better than the bottom package, and the outermost corner solder joints of the bottom package are the critical solder joints for the PoP under vibration loading. The stress characteristics of solder joints obtained by FEM are well correlated with the experimental results. Failure mechanism analysis indicates that the bottom solder joints become the most vulnerable part of the PoP under vibration due to the bigger relative displacements between the PCB and the bottom package. The micro-structural analysis indicates that cracks usually originate in the bottleneck position of the solder balls, extend within bulk solder and then propagate along the interface between the IMC layer and the bulk solder. The influence of bottom solder joints standoff for vibration reliability was analyzed by FEM as well. Results show that the higher the bottom solder joints' standoff, the more difficult the failure for the PoP assembly.  相似文献   

7.
This work discusses the experimental set-up and data interpretation for high temperature and current stress tests of flip chip solder joints using the four-point Kelvin measurement technique. The single solder joint resistance responses are measured at four different four-point Kelvin structure locations in a flip chip package. Various temperatures (i.e., 125–165 °C) and electric current (i.e., 0.6–1.0 A) test conditions are applied to investigate the solder joint resistance degradation behavior and its failure processes. Failure criterion of 20% and 50% joint resistance increases, corresponding to solder and interfacial voiding, are employed to evaluate the solder joint electromigration reliability. The absolute resistance value is substantially affected by the geometrical layout of the metal lines in the four-point Kelvin structure, and this is confirmed by finite element simulation.Different current flow directions and strengths yielded different joint resistance responses. The anode joint, where electrons flow from the die to the substrate, usually measured an earlier resistance increase than the cathode joint, where electrons flow in the opposite direction. The change in measured joint resistances can be related to solder and interfacial voiding in the solder joint except for ±1 A current load, where resistance drop mainly attributed to the broken substrate Cu metallization as a result of “hot-spot” phenomenon. The solder joint temperature increases above the oven ambient temperature by ~25 °C, ~40 °C and ~65 °C for 0.6 A, 0.8 A and 1.0 A stress current, respectively. It is found that two-parameter log-normal distribution gives a better lifetime data fitting than the two-parameter Weibull distribution. Regardless of failure criterion used, the anode joint test cells usually calculated a shorter solder joint mean life with a lower standard variation of 0.3–0.6, as compared to the cathode joint test cells with a higher standard variation of 0.8–1.2. For a typical flip chip solder joint construction, electromigration reliability is mainly determined by the under bump metallization consumption and dissolution, with intermetallic compound formation near the die side of an anode joint.  相似文献   

8.
This study simulated the performance of Cu-cored solder joints in microelectronic components subjected to the extreme thermal cycling conditions often encountered in the automobile industry by comparing the thermal cycling behavior of Cu-cored solder joints containing two different coating layers of Sn–3.0Ag and Sn–1.0In with that of a baseline Sn–3.0Ag–0.5Cu solder joint under a severe temperature cycling range of ?55 to +150 °C. Both Cu-cored solder joints can be considered a potential solution to interconnects in microelectronic semiconductor packages used under harsh thermal conditions on account of their greater resistance to thermal stress caused by the severe temperature cycling than the baseline Sn–3.0Ag–0.5Cu solder joint.  相似文献   

9.
The drop resistance and fracture behavior of Sn–37Pb, Sn–3.0Ag–0.5Cu (SAC305), Sn–1.0Ag–0.5Cu (SAC105), and Sn–8.5Zn–0.5Ag–0.01Al–0.1 Ga (SnZn-5e) solder ball joints under the board-level drop test (BLDT) and the ball impact test (BIT) were studied. The results show that the drop reliabilities in terms of the characteristic life ratio from the Weibul plot are SnZn-5e : Sn–37Pb:SAC105:SAC305 = 3.1:2.9:2.1:1. It was observed that failure of Sn–37Pb occurred at the eutectic tin–lead phase whereas it took place at the brittle interface between the (Cu,Ni)6Sn5 inter-metallic compound and Ni layer in SAC305. The failure of SAC105 was found to be located within the solder matrix as well as at the interface of the inter-metallic compound. The failure of SnZn-5e depends on the morphology of the interfacial inter-metallic compound. The failure modes of Sn–37Pb and SAC305 after the BIT were similar to those after the BLDT. The maximum impact force (Fmax) and the initial fracture energy (E) from the BIT can be used to evaluate the drop reliability of solder joints.  相似文献   

10.
《Microelectronics Reliability》2014,54(11):2536-2541
While the Sn–Ag–Cu (SAC) family of solders are considered good candidate as lead-free solder replacement materials, their relatively short processing history and application result in a host of materials as well as reliability problems. For good metallurgical bonding and electrical connection, a thin, even layer of intermetallic compound (IMC) is required but excessive growth of the IMC layer will cause various reliability problems. This is especially critical for miniaturized solder pitches in very large scale integration circuits. This work adopts the composite approach of adding 0.15 and 0.30 wt.% of Pt into Sn–3.8Ag–0.7Cu alloy to study the effect of these additions to the IMC layer thickness between the solder and substrate. Alloys were isothermally aged at 150 °C for up to 1000 h to observe contribution of Pt in suppressing excessive IMC growth. It was found that when more Pt was added to the alloy, the IMC layer became more even and continuous. Voids and IMC layer thickness were reduced. This is attributed to the role of Pt in replacing Cu in the solder and thus impeding excessive diffusion.  相似文献   

11.
In this study, we evaluated the mechanical reliability of Sn-rich, Au–Sn/Ni flip chip solder bumps by using a sequential electroplating method with Sn and Au. After reflowing, the average diameter of the solder bump was approximately 80 μm and only a (Ni,Au)3Sn4 intermetallic compound (IMC) layer was formed at the interface. Due to the preferential consumption of Sn atoms within the solder matrix during aging, the solder matrix was transformed sequentially in the following order: β-Sn and η-phase, η-phase, and η-phase and ε-phase. In the bump shear test, the shear force was not significantly changed despite aging at 150 °C for 1000 h and most of the fractures occurred at the interfaces. The interfacial fracture was significantly related to the formation of brittle IMCs at the interface. The Sn-rich, Au–Sn/Ni flip chip joint was mechanically much weaker than the Au-rich, Au–Sn/Ni flip chip joint. The study results demonstrated that the combination of Sn-rich, Au–Sn solder and Ni under bump metallization (UBM) is not a viable option for the replacement of the conventional, Au-rich, Au–20Sn solder.  相似文献   

12.
The electronic packaging industry uses electroless nickel immersion gold (ENIG) or Cu-organic solderability preservative (Cu-OSP) as a bonding pad surface finish for solder joints. In portable electronic products, drop impact tests induce solder joint failures via the interfacial intermetallic, which is a serious reliability concern. The intermetallic compound (IMC) is subjected to thermal cycling, which negatively affects the drop impact reliability. In this work, the reliability of lead-free Sn-3.0Ag-0.5Cu (SAC) soldered fine-pitch ball grid array assemblies were investigated after being subjected to a combination of thermal cycling followed by board level drop tests. Drop impact tests conducted before and after thermal aging cycles (500, 1000, and 1500 thermal cycles) show a transition of failure modes and a significant reduction in drop durability for both SAC/ENIG and SAC/Cu-OSP soldered assemblies. Without thermal cycling aging, the boards with the Cu-OSP surface finish exhibit better drop impact reliability than those with ENIG. However, the reverse is true if thermal cycle (TC) aging is performed. For SAC/Cu-OSP soldered assemblies, a large number of Kirkendall voids were observed at the interface between the intermetallic and Cu pad after thermal cycling aging. The void formation resulted in weak bonding between the solder and Cu, leading to brittle interface fracture in the drop impact test, which resulted in significantly lower drop test lifetimes. For SAC/ENIG soldered assemblies, the consumption of Ni in the formation of NiCuSn intermetallics induced vertical voids in the Ni(P) layer.  相似文献   

13.
Intermetallic growth studies on Sn-Ag-Cu lead-free solder joints   总被引:4,自引:0,他引:4  
Solid-state intermetallic compound (IMC) growth behavior plays an important role in solder joint reliability of electronic packaging assemblies. The morphology and growth of interfacial IMC compounds between 95.5Sn-3.8Ag-0.7Cu Pb-free solders and nickel/gold (Ni/Au) surface finish on BGA solder joint specimen is reported. Digital imaging techniques were employed in the measurement of the average IMC growth thickness. The IMC growth behavior subjected to isothermal aging exposure at 125°C, thermal cycling (TC), and thermal shock (TS) with upper soak temperatures of 125°C are compared. An equivalent isothermal aging time is proposed for comparison of IMC layer growth data. It was noted that IMC layer growth under thermal cycling and thermal shock aging gives an acceleration factor of 1.4 and 2.3 based on the equivalent isothermal aging time.  相似文献   

14.
《Microelectronics Reliability》2014,54(12):2944-2950
Conductive adhesives play a major role in the electronic packaging industry as an alternative to solder due to their potential advantages that include mild processing conditions and superior thermo-mechanical performance. In a conductive adhesive interconnection, adequate mechanical and electrical performance and long-term reliability are critical.In this paper, the reliability of solderable isotropic conductive adhesive (ICA) interconnections was investigated. Reliability testing was performed via thermal shock (−55 to 125 °C, 1000 cycles) and high-temperature and high-humidity tests (85 °C, 85% RH, 1000 h). The interfacial microstructure of the solderable ICA was also investigated. Additionally, the fracture mode was investigated via mechanical pull strength testing before and after the reliability test. The electrical resistance of the solderable ICA interconnection showed improved stability compared to conventional ICAs, and similar stability to conventional solder paste (Sn–3Ag–0.5Cu and Sn–58Bi) due to the metallurgical interconnection formed by the molten LMPA fillers between the corresponding metallization layers. After the reliability tests, the grown IMC layer was composed of Cu6Sn5 (η-phase) and Cu3Sn (ε-phase), and the scallop-type IMC transformed into a layer-type IMC. The fracture propagated along the Cu–Sn IMC/SnBi interface and the fracture surface showed a semi-brittle fracture mode mixed with cleavage and ductile tear bands.  相似文献   

15.
《Microelectronics Reliability》2014,54(12):2922-2928
In this study, low-cycle fatigue test was conducted for a lead-free solder joint at two test temperatures (348 K, 398 K) and three strain amplitudes (3%, 4%, and 8%). Fatigue failure behavior was analyzed and the fatigue life was evaluated using the Coffin–Manson relationship and Morrow energy-based model. The results show that the maximum load gradually drops with increasing the number of loading cycles. When the strain range or temperature is low, the maximum load drop curve can be divided into three stages. Then, it degrades into a linear stage with increasing the strain range or temperature. Both the softening of solder and the reduction of effective load-bearing area are responsible for the maximum load drop depending on the test condition. Fatigue crack initiates at the corner of the solder joint and propagates along the strain concentrated zone. Spacing distance between fatigue striations is enlarged with increasing the temperature in accordance with the degradation of fatigue resistance. In addition, both the Coffin–Manson model and Morrow energy-based model can be used to evaluate the fatigue life of solder joint under high temperature. The fatigue ductility exponent α in Coffin–Manson model and the fatigue ductility coefficient C in Morrow model are dependent on temperature, whereas other parameters in these two models keep stable under different temperature.  相似文献   

16.
Non-conductive film with Zn nano-particles (Zn-NCF) is an effective solution for fine-pitch Cu-pillar/Sn–Ag bump interconnection in terms of manufacturing process and interfacial reliability. In this study, NCFs with Zn nano-particles of different acidity, viscosity, and curing speed were formulated and diffused Zn contents in the Cu pillar/Sn–Ag bumps were measured after 3D TSV chip-stack bonding. Amount of Zn diffusion into the Cu pillar/Sn–Ag bumps increased as the acidity of resin increased, as the viscosity of resin decreased, as the curing speed of resin decreased, and as the bonding temperature increased. Diffusion of Zn nano-particles into the Cu pillar/Sn–Ag bumps are maximized when the resin viscosity became lowered and the solder oxide layer was removed. To analyze the effects of Zn-NCF on IMC reduction, IMC height depending on aging time was measured and corresponding activation energies for IMC growth were calculated. For the evaluation of joint reliabilities, test vehicles were bonded using NCFs with 0 wt%, 1 wt%, 5 wt%, and 10 wt% of Zn nano-particles and aged at 150 °C up to 500 h. NCF with 10 wt% Zn nano-particle showed remarkable suppression in Cu6Sn5 and (Cu,Ni)6Sn5 IMC compared to NCFs with 0 wt%, 1 wt%, and 5 wt% of Zn nano-particles. However, in terms of Cu3Sn IMC suppression, which is the most critical goal of this experiment NCFs with 1 wt%, 5 wt%, and 10 wt% showed an equal amount of IMC suppression. As a result, it was successfully demonstrated that the suppression of Cu–Sn IMCs was achieved by the addition of Zn nano-particles in the NCFs resulting an enhanced reliability performance in the Cu/Sn–Ag bumps bonding in 3D TSV interconnection.  相似文献   

17.
《Microelectronics Reliability》2014,54(11):2523-2535
Thermal cycling tests have been performed for a range of electronic components intended for avionic applications, assembled with SAC305, SN100C and SnPbAg solder alloys. Two temperature profiles have been used, the first ranging between −20 °C and +80 °C (TC1), and the second between −55 °C and +125 °C (TC2). High level of detail is provided for the solder alloy composition and the component package dimensions, and statistical analysis, partially supported by FE modeling, is reported. The test results confirm the feasibility of SAC305 as a replacement for SnPbAg under relatively benign thermomechanical loads. Furthermore, the test results serve as a starting point for estimation of damage accumulation in a critical solder joint in field conditions, with increased accuracy by avoiding data reduction. A computationally efficient method that was earlier introduced by the authors and tested on relatively mild temperature environments has been significantly improved to become applicable on extended temperature range, and it has been applied to a PBGA256 component with SAC305 solder in TC1 conditions. The method, which utilizes interpolated response surfaces generated by finite element modeling, extends the range of techniques that can be employed in the design phase to predict thermal fatigue of solder joints under field temperature conditions.  相似文献   

18.
In the present study, the effect of Al2O3 nanoparticles on performances of Sn–58Bi solder were investigated in aspects of electro-migratio, shear strength and microhardness. The experimental results show that the Al2O3 nanoparticles significantly improved microstructure and mechanical performances of solder joints. With the addition of 0.5 wt% Al2O3, the intermetallic compounds (IMC) reduced from 2.5 μm to 1.27 μm after 288 aging hours at 85 °C. Furthermore, after electromigration test under a current density of 5 × 103 A/cm2 at 85 °C, Bi-rich layers formed at the anode side of both Al2O3 doped and plain solder. Moreover, the addition of Al2O3 nanoparticles reduced the mean thickness of Bi-rich layer. In addition, the growth rate of the IMC layer of Al2O3 doped solder decreased by 8% compared with the plain solder. Besides, the Al2O3 doped solder exhibited better performance than plain solder in microhardness after different aging times. While, the addition of Al2O3 significantly impeded the degradation of the shear strength of solder joint after aging for 48 and 288 h. Furthermore, it was worth noting that the fracture surface of doped solder showed a typical rough and ductile structure. However, plain solder exhibited a relatively smooth and fragile surface.  相似文献   

19.
Solder joint integrity has long been recognized as a key issue affecting the reliability of integrated circuit packages. In this study, both experimental and finite element simulation methods were used to characterize the mechanical performance and fracture behavior of micro-scale ball grid array (BGA) structure Cu/Sn–3.0Ag–0.5Cu/Cu solder joints with different standoff heights (h, varying from 500 to 100 μm) and constant pad diameter (d, d = 480 μm) and contact angle under shear loading. With decreasing h (or the ratio of h/d), results show that the stiffness of BGA solder joints clearly increases with decreasing coefficient of stress state and torque. The stress triaxiality reflects the mechanical constraint effect on the mechanical strength of the solder joints and it is dependent on the loading mode and increases dramatically with decreasing h under tensile loading, while the change of h has very limited influence on the stress triaxiality under shear loading. Moreover, when h is decreased, the concentration of stress and plastic strain energy along the interface of solder and pad decreases, and the fracture location of BGA solder joints changes from near the interface to the middle of the solder. Both geometry and microstructure greatly affect the shear behavior of joints, the average shear strength shows a parabolic trend with decreasing standoff height. Furthermore, the brittle fracture of BGA solder joints after long-time isothermal aging was investigated. Results obtained show that, under the same shear force, the stress intensity factors, KI and KII, and the strain energy release rate, GI, at the Sn–3.0Ag–0.5Cu/Cu6Sn5 interface and in the Cu6Sn5 layer obviously decrease with decreasing h, hence brittle fracture is more prone to occur in the joint with a large standoff height.  相似文献   

20.
In this study, experimental and numerical analyses on the solder joint reliability of plastic ball grid array under harsh random vibration and thermal loadings were presented. The chips were assembled on the daisy chained circuit boards for the test samples preparation, and a half of the samples were processed for underfill to investigate the underfill effects on the solder failures. Two consequential steps of the random vibrations, named as acceptance level and qualification level, were applied. Overall required root mean square (rms) of the power spectrum densities of the steps were 22.48 grms for one minutes and 31.78 grms for two minutes, respectively. A thermal shock test was then performed after the vibration tests. It was found that the samples did not show any solder failure under the test requirements, demonstrating the robustness of the packaging structure for potential space applications. The samples were further tested to induce the failures, and finite element analyses were performed to analyze the sample vibration behaviors and the solder stresses to compare the results with the test data. Finally, a simple analytical calculation for the natural frequency estimations was introduced to overcome the complex finite element modeling efforts.  相似文献   

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