TWO STAGE DRYING OF SYNTHETIC DETERGENTS

A key ingredient in granular synthetic detergents is Sodium Tripolyphosphate (STP). The hexahydrate of STP is unstable during the spray drying process. The decomposition (reversion) is shown to be solely a function of particle temperature. The reversion products interact with calcium ions in the wash water and form insoluble species. This results in undesirable deposition onto the fabrics. The goal of this study is to develop a drying process with lower temperatures to reduce the decomposition. This, in turn, will improve product quality by reducing undesirable fabric deposits.

A two stage drying process is used to reduce the drying temperatures. Experimental evidence is presented to demonstrate the near-elimination of STP decomposition.

The design of a production scale fluid bed dryer uses a ‘normalization'procedure to calculate the rate constants at constant bed temperature from the data taken at constant inlet air temperature. The rate constants are corrleated to bed temperature using an Arrhenius-like equation.     

MULTI-STAGE SPRAY DRYING METHOD IN MANUFACTURING HEAVY DUTY DETERGENTS

Collision of droplets; counter-current spray dryer; drying rate; heat transfer; nonphosphated detergent; spray drying

The spray drying method of non-phosphated granular detergents is studied to decrease the amount of agglomerate particles. The formation of agglomerates is mainly influenced by the concentration of droplets in spray cloud and the water content of droplets at the time of collision. The overlaps of different spray clouds should be de- creased.

The drying rate near the nozzle zone is considerably faster than that calculated by Ranz-Marshal's equation. According to these phenomena, “Multi-stage spray drying” is developed, which is characterized by in stalling plural spraying stages in a spray dryer.

Consequently, non-phosphated detergents are manufactured with the same powder properties and productivity as phosphated detergents.     

MULTI-STAGE SPRAY DRYING METHOD IN MANUFACTURING HEAVY DUTY DETERGENTS

Collision of droplets; counter-current spray dryer; drying rate; heat transfer; nonphosphated detergent; spray drying

The spray drying method of non-phosphated granular detergents is studied to decrease the amount of agglomerate particles. The formation of agglomerates is mainly influenced by the concentration of droplets in spray cloud and the water content of droplets at the time of collision. The overlaps of different spray clouds should be de- creased.

The drying rate near the nozzle zone is considerably faster than that calculated by Ranz-Marshal’s equation. According to these phenomena, “Multi-stage spray drying” is developed, which is characterized by in stalling plural spraying stages in a spray dryer.

Consequently, non-phosphated detergents are manufactured with the same powder properties and productivity as phosphated detergents.     

EFFECTS OF DRYING ON HEAD RICE YIELD USING FLUIDIZATION TECHNIQUE

ABSTRACT

Experimental results of fluidized bed paddy drying using high inlet air temperatures (140 and 150 °C) showed that head rice yield could be increased to a maximum value at a range of paddy final moisture contents of 19 to 22 % wet-basis. In case of reducing moisture content of paddy to lower than 19 % wet-basis, head rice yield of tempered paddy was higher than that of no-tempered one. Initial moisture contents of paddy that could increase head rice yield were in a range of 23 to 31 % wet-basis. As initial moisture content increased head rice yield increased. Whiteness of dried paddy was mostly accepted. However, if tempering temperature was higher than 60 °C, it may cause the problems for trade.     

EVALUATION OF DIFFERENT METHODS OF DRYING ON THE QUALITY OF OYSTER MUSHROOM (Pleurotus sp)

ABSTRACT

Mushrooms are extremely perishable and have a short shelf life period. To increase the post harvest lives, different methods of drying viz., sun diving, fluidized bed drying and thin layer drying with potassium metabisulphite (KMS) and blanching was done. The quality of mushroom dried in fluidized bed condition at 50°C for 80-120 minutes with 0.5 KMS was found to be superior to other drying methods. Rehydration ratio was also maximum in KMS treated mushroom and no significant difference at higher concentration. The treatment with KMS and blanching reduces the nutritive quality but improves the colour of the mushrooms when compared with sun dried samples. Storage of mushrooms after treatment with KMS at higher concentration (1.5%) reduces the microbial spoilage.     

多层振动流化床干燥器在活性炭干燥中的应用

介绍振动流化床及多层振动流化床干燥器的工作原理和结构及其优点 ,并分析了现有活性炭中生产应用的几种干燥设备的优缺点     

DRYING OF TOBACCO PARTICLES IN A MOBILISED BED

ABSTRACT

The drying performance of a novel device capable of mobilising a bed of fibrous materials is evaluated. The drying kinetic of the vegetable product used for this work, cut lamina tobacco particles, was determined from fixed bed experiments. A falling-rate period was observed for the entire drying curve. The results showed that the drying rate is controlled by internal mass transfer mechanism for gas superficial velocities above 0.8 m/ s. The proposed model is based on an effective liquid diffusion coefficient that varies with solids temperature according to an Arrhenius-type relationship. Batch drying experiments were carried out in the mobilised bed apparatus under various conditions of inlet air temperature, humidity and flowrate. Assuming perfect mixing and no internal resistance to heat transfer for the solids, the performance of the mobile bed can be predicted using the proposed internal liquid diffusion model     

加压流化床煤气化炉衬里材料的选择与烘制

加压流化床煤气化技术是近年来随着洁净煤技术的兴起而发展起来的新一代大型、先进煤气化技术。就加压流化床煤气化炉耐火衬里的特殊要求进行了耐火材料的选型,并根据所选耐火材料特性制定了烘炉工作曲线,并比较了烘炉所需实际燃料气量和估算值,结果表明计算值与实际值吻合较好,并为大型流化床反应器的烘炉工艺制定和实施提供一种理论参考和估算方法。     

惰性粒子流化床中的悬浮液干燥

用惰性粒子流化床干燥器对混凝土外加剂等5种物料进行了干燥实验研究，提出了计算体积传热系数的关联式．实验结果表明，由于惰性粒子的存在，强化了传热传质，体积传热系数可达3000W·m~(-3)·K~(-1)，但是，床层压力降较高．干燥强度（以蒸出水计）可达50～60kg·m~(-3)·h~(-1)，热效率30％～43％，若提高热风进口温度，后两项指标还可提高.     

AMARANTH GRAIN DRYING IN A FLUIDIZED BED

ABSTRACT

An empirical equation as a function of drying time and temperature was developed to calculate the moisture ratio required Tor balch fluidized bed dryers design for amaranth grain drying

The relative deviations of the moisture ratio values calculated with the proposed equation with regard to the experimental ones ranged between 0.014 and 0.095 for a drying air temperature between 60 and 100 ° C, and a grain initial moisture content between 23.5 and 16.6 % wb.     

A STOCHASTIC APPROACH TO THE DRYING OF SOLIDS IN A MULTI-STAGE FLUIDIZED BED

The residence times of solids flowing through a fluidized bed dryer exhibit dispersion about the mean. In this paper, expressions for the probability density functions of solids moisture content in the various stages of a multi-stage dryer are derived. A simple recurrence relationship for the moments of the distribution is also presented. The analysis is applied to the drying of cereal grains, and it is shown that the degree of drying increases with the number of stages in the dryer. Probability density functions of the moisture content are presented.     

DRYING OF GRANULAR PARTICLES IN A MULTISTAGE INCLINED FLUIDIZED BED WITH MECHANICAL VIBRATION

A mathematical model for the drying rate of granular particles in a multistage inclined fluidized bed(IFB) is presented from the standpoint of simultaneous heat and mass transfer, with taking the effect of mechanical vibration added vertically into consideration.

Steady-state distributions for the temperatures and concentrations of the particles and the heating gas, and for the moisture content of the particles are numerically calculated based on the present model. The calculated results show fairly good agreement with the experimental data, which were obtained from the drying experiments of brick particles in a three-stage IFB using comparatively low temperature air(40-60°C) as the heating gas.

It has been found within the range of the experimental conditions employed that, the mechanical vibration added vertically enhances the over-all drying rate of the particles and its effect can be considered equivalent to an increase in the air velocity.     

重质微细碳酸钙干燥方法与实验研究

着重对湿磨后的重质碳酸钙的浆液采用不同的干燥方法和装置进行了干燥实验。对其成品的有关指标和不同的干燥器的特性进行比较,对实际生产和应用有较好的参考价值。     

SLURRY DRYING IN GAS-PARTICLE CONTACTORS: FLUID-DYNAMICS AND CAPACITY ANALYSIS

The fluid-dynamic characteristics and evaporation capacities of several substrates (pure water, a mixture of water and carbohydrates, and apple pulps with maltodextrines) for conical spouted bed, fluidized bed and pneumatic dryers was compared.

For fluidized and spouted beds, the presence of fluids increased the fluid-dynamics parameters over the values when only inert particles were present in the beds. In both cases it was proposed correlations to predict those effects. In the spouted bed drier, increasing the load of inert particles resulted in a slight increase of the water evaporation capacity, while in the fluidized bed drier the effect was more marked. For fluidized and spouted beds, under similar operation conditions, the maximums of the suspension drying capacities are lower than the values of water evaporation, but for pneumatic drying this effect was the opposite. In general terms, the maximal capacities of fluidized bed dryers are higher than those observed in the spouted bed dryers.     

DYNAMIC PRESSURE RISE IN THE DRYING CHAMBER AS A REMOTE SENSING METHOD FOR MONITORING THE TEMPERATURE OF THE PRODUCT DURING THE PRIMARY DRYING STAGE OF FREEZE DRYING

Abstract

A novel dynamic pressure rise method is developed as a remote sensing procedure for determining at different times during the primary drying stage of the freeze drying process (i) the temperature of the moving interface between the dried and frozen layers of the product, (ii) temperature close to the upper surface of the dried layer of the product, (iii) the temperature of the bottom surface of the frozen layer of the product, and (iv) the temperature profile of the frozen layer of the product. Furthermore, by knowing the temperature of the heating plate and determining the value of the temperature of the moving interface from the dynamic pressure rise method, the value of the position of the moving interface could be determined by an expression presented in this work     

RECENT PROGRESS OF SPRAY DRYING IN CHINA

Abstract

The development of spray drying technique during past 10 years in China is reviewed. Main achievements in research, development and utilization of three types of atomization are described and summarized. General trend of spray drying research and development in 21st century is forecasted.     

RECENT PROGRESS OF SPRAY DRYING IN CHINA

The development of spray drying technique during past 10 years in China is reviewed. Main achievements in research, development and utilization of three types of atomization are described and summarized. General trend of spray drying research and development in 21st century is forecasted.     

OSMO-CONVECTIVE DRYING OF GRAPES

In order to reduce browning of grapes during drying, a special drying method was developed and evaluated using a laboratory scale fluidized bed dryer. Fresh Thompson seedless grapes were initially dried by immersion in a fluidized bed of sugar. The mass ratio of grapes to sugar was 1:1. The flow rate of hot air (at 45 and 60^°C) was sufficient to fluidize the sugar bed, while grapes placed on the screen, 3 cm above the drying air distributor, remained generally stationary.

Due to the simultaneous osmotic and convection drying effects, the drying time was reduced by factor ∼1.5 as compared to drying under the similar conditions without added sugar. A special pre-treatment of dipping of grapes in ethyl oleate (2% solution in 0.5% sodium hydroxide) at 80†deg; C for 30 s further reduced the drying time by factor 2 in both cases. The color of osmo-convective dried grapes were comparable to that of sulfur dioxide treated grapes. The texture of osmo-convective dried grapes was more pliable (softer) than convective dried samples. The major problem associated with die osmo-convective drying of grapes on a sugar bed was the stickiness, caused by sugar, on the fruit surface. This was reduced by partially substituting sugar with semolina (maintaining a 1:1 ratio) to create fluidized bed.     

OSMO-CONVECTIVE DRYING OF GRAPES

ABSTRACT

In order to reduce browning of grapes during drying, a special drying method was developed and evaluated using a laboratory scale fluidized bed dryer. Fresh Thompson seedless grapes were initially dried by immersion in a fluidized bed of sugar. The mass ratio of grapes to sugar was 1:1. The flow rate of hot air (at 45 and 60^°C) was sufficient to fluidize the sugar bed, while grapes placed on the screen, 3 cm above the drying air distributor, remained generally stationary.

Due to the simultaneous osmotic and convection drying effects, the drying time was reduced by factor ～1.5 as compared to drying under the similar conditions without added sugar. A special pre-treatment of dipping of grapes in ethyl oleate (2% solution in 0.5% sodium hydroxide) at 80?deg; C for 30 s further reduced the drying time by factor 2 in both cases. The color of osmo-convective dried grapes were comparable to that of sulfur dioxide treated grapes. The texture of osmo-convective dried grapes was more pliable (softer) than convective dried samples. The major problem associated with die osmo-convective drying of grapes on a sugar bed was the stickiness, caused by sugar, on the fruit surface. This was reduced by partially substituting sugar with semolina (maintaining a 1:1 ratio) to create fluidized bed.     

喷雾干燥节能技术研究

通过从喷雾干燥所涉及的操作工艺参数和喷雾干燥工艺流程调整等方面进行探索 ,深入研究了影响喷雾干燥能耗的主要因素和相应的结果 ,并提出了针对性的解决喷雾干燥能耗高的方法 ,使得采用喷雾干燥达到理想的效果