THE RELATIVE INFLUENCE OF DIELECTRIC AND OTHER DRYING TECHNIQUES ON THE PHYSICO - MECHANICAL PROPERTIES OF A PHARMACEUTICAL TABLET EXCIPIENT. PARTI: COMPACTION CHARACTERISTICS.

The relative Influence of nine techniques for drying wet granulated microcrystal-lline cellulose (MCC) on the subsequent compaction characteristics was studied In terms of the tensile strength and corrected work of failure of the tablets. Wet granulation resulted in a substantial decrease in compatibility. However, the drying technique used was found to affect the degree of loss in compatibility. In general, microwave-vacuum drying using the “high” process type resulted in the production of granules with the highest compatibility followed by freeze drying and fluidized bed drying. Granules dried under ambient conditions, and granules tray dried to “just dry” or “over dried” conditions resulted In tablets possessing approximately comparable compatibilites, with the poorest compaction characteristics being exhibited by vacuum dried granules, in addition It was found that use of a “low” drying process type during microwave- vacuum drying yielded granules with inferior compaction characteristics to those dried by the “high” process type. Radio frequency drying was found to yield granules which produced tablets having slightly inferior tensile strength to tray dried material, although the tablet work of failure values were comparable. The effect of drying technique on the subsequent compaction characteristics was not found to be directly related to the moisture content of the granules.     

Compressive characteristics of cellular solids produced using vacuum-microwave, freeze, vacuum and hot air dehydration methods

Dried cellular solids were produced using different hydrocolloids such as locust bean gum, low methoxy pectin, methyl cellulose and tapioca starch. They were dried to less than 5% (w.b) moisture content using freeze-drying, vacuum drying, vacuum microwave drying or air-drying methods. The dry cellular solids were subjected to uniaxial compression using a Texture analyzer to study the compressive characteristics. True stress–strain relationship curves were developed for the dry cellular solids produced by different drying methods. Hencky’s strain was calculated for true strain. Comparisons of samples dried by different drying methods were done in terms of their compressive characteristics at various water activities. No matter the type of drying, the dried materials were brittle at low water activity, plastic at medium water activity and elastomeric at higher water activity levels. Due to non-uniformity in air-dried samples and more closed pores in vacuum dried samples as well as less mechanical strength, these two were considered inferior for production of strong elastomeric foams. Microwave vacuum dried foams were mechanically the strongest. All the microwave vacuum dried samples were close in their Young’s modulus. Increases in microwave power did not make any appreciable changes in pore structures although higher microwave power levels resulted in faster drying.     

PERFORMANCE STUDY OF A RE-CIRCULATING CABINET DRYER USING A HOUSEHOLD DEHUMIDIFIER

The performance and operating characteristics of a low temperature re-circulating cabinet dryer using a dehumidifier loop were studied using alfalfa. Chopped alfalfa, initially at 70% moisture content, was dried to 10% moisture content in the dryer. Two dryer setups were used. The dryers in each case had a partitioned cabinet with trays of material on one side and a stack of one or two small household dehumidifiers on the other side. Air was re-circulated through the material from bottom to the top and back through the dehumidifiers. Two drying configurations were tested. In one, the material was left on the trays until drying was complete (batch or fixed tray drying). In the other configuration, the trays were moved from top to bottom, introducing a new tray at the top while removing an old tray from bottom. Drying air temperature ranged from 25 to 45°C. The average air velocity through the material was 0.38 m/s. Alfalfa chops dried in 5 h in the fixed tray drying and in 4 h in the moving tray drying. The specific moisture extraction rate ranged from 0.35 to 1.02 kg/kWh for batch drying and stayed at an average value of 0.50 kg/kWh for continuous/moving tray drying.     

Effect of three drying methods on the drying characteristics and quality of okra

The objective of this study was to compare the drying characteristics and quality of dried okra obtained by vacuum freeze drying (VFD), microwave vacuum drying (MVD), and pulse-spouted microwave vacuum drying (PSMVD). The quality parameters include color (L*, a*, and b*), texture (hardness and fracturability), shrinkage ratio (SR), nutrient retention (chlorophyll, flavonoids, and vitamin C), and sensory score was investigated. Vacuum freeze drying maximally preserved the original properties of samples. And the samples dried by PSMVD showed higher quality and more uniformity compared to MVD. Considering of all aspects comprehensively, such as cost-effectiveness, practicability, and scale-up, PSMVD was a promising technique which would match results obtained by vacuum freeze drying.     

PERFORMANCE STUDY OF A RE-CIRCULATING CABINET DRYER USING A HOUSEHOLD DEHUMIDIFIER

ABSTRACT

The performance and operating characteristics of a low temperature re-circulating cabinet dryer using a dehumidifier loop were studied using alfalfa. Chopped alfalfa, initially at 70% moisture content, was dried to 10% moisture content in the dryer. Two dryer setups were used. The dryers in each case had a partitioned cabinet with trays of material on one side and a stack of one or two small household dehumidifiers on the other side. Air was re-circulated through the material from bottom to the top and back through the dehumidifiers. Two drying configurations were tested. In one, the material was left on the trays until drying was complete (batch or fixed tray drying). In the other configuration, the trays were moved from top to bottom, introducing a new tray at the top while removing an old tray from bottom. Drying air temperature ranged from 25 to 45°C. The average air velocity through the material was 0.38 m/s. Alfalfa chops dried in 5 h in the fixed tray drying and in 4 h in the moving tray drying. The specific moisture extraction rate ranged from 0.35 to 1.02 kg/kWh for batch drying and stayed at an average value of 0.50 kg/kWh for continuous/moving tray drying.     

Drying Characteristics and Kinetics of Vacuum Microwave–Dried Potato Slices

Vacuum microwave dehydration characteristics and drying kinetics of potato slices were evaluated using a laboratory-scale dryer. The test materials were placed on a rotating tray to allow uniform exposure to the microwave field. The effect of drying conditions on the drying characteristics was investigated. As expected, higher drying rates were obtained with higher microwave power and lower vacuum levels. The effect of vacuum pressure on drying rate was not as significant as that of microwave power. The Henderson & Pabis model provided better simulation of the drying curves for potato slices. Empirical models are presented for the drying rate constant as a function of the microwave power and vacuum pressure for potato slices under the range of operating conditions tested.     

Production of dried ivy gourd sheet as a health snack

Ivy gourd (Coccinia grandis) has recently been recognized as a rich source of β-carotene. To add value to the fresh leaves a process to produce dried ivy gourd sheet as a health snack was the aim of this study. The effects of pretreatment, i.e., blanching in NaCl solution (0-3% w/v), and drying methods, i.e., hot air drying and vacuum drying at 60-80 °C, on the drying characteristics and quality, viz. colour, texture and β-carotene content of dried ivy gourd sheet were investigated. The results showed that dried sheet pretreated by brine blanching and vacuum drying resulted in better retention of colour and β-carotene as well as texture of the dried sheet as compared to the dried untreated and dried water blanched samples. Higher drying temperature also resulted in higher β-carotene retention due to shorter drying time.     

Variation in Drying Behavior and Final Moisture Content of Wood during Conventional Low Temperature Drying and Vacuum Drying of Betula pendula Timber

Conventional and vacuum drying experiments were conducted on Betula pendula timber, which was sawn from trees felled during three different seasons. The influence of the wood procurement season on drying behavior differed, on the one hand, between the drying phases above and below 30% moisture content in the conventional drying, and, on the other hand, between the conventional and vacuum drying methods. During the first steps of the conventional drying process, relative humidity in the kiln, as well as drying time and drying rate, varied according to the felling season. Variations in environmental conditions outside the kiln and the seasonal variation in the physical properties of the wood were presumed to be the reasons for differences in drying behavior. The difference in moisture content gradient, i.e., the difference in final moisture content between the inner wood and the surface layer of boards, was greater in conventionally dried timber than in vacuum-dried timber. In conventionally dried timber there was a clear seasonal variation in the gradient of final moisture content, which was greatest for winter-felled wood. The premature drying of the surface layer during the first steps of the conventional drying process of winter-felled wood was the reason for the higher gradient of moisture content. Storage of wood as logs decreased the standard deviation of the final moisture content.     

EFFECT OF PRETREATMENT AND DRYING ON THE QUALITY OF OYSTER MUSHROOMS (PLEUROTUS OSTREATUS)

Fruiting bodies of oyster mushroom were dried by hot-air drying, vacuum-drying and freeze-drying in order to compare food qualities after drying. Prior to drying, mushrooms were subjected to blanching or dipping in sodium metabisulphite solution (1 or 5 g/L), or dipping in citric acid solution (1 or 5 g/L). Drying of raw mushrooms was taken as a control. Blanching reduced the attractiveness of dry mushrooms; sodium metabisulphite improved it. It has been found that pretreatment and drying method affect the course and rate of drying. Samples subjected to hot-air drying and vacuum-drying were darker than those freeze-dried, which were clearly more attractive. The hot-air and vacuum-dried mushrooms on rehydration were inferior in quality to the freeze-dried samples. Flavor of the freeze-dried mushroom was not significantly different from that of the hot-air dried mushrooms. Food quality of dried mushrooms depends significantly on the type of drier used.     

Variation in Drying Behavior and Final Moisture Content of Wood during Conventional Low Temperature Drying and Vacuum Drying of Betula pendula Timber

Conventional and vacuum drying experiments were conducted on Betula pendula timber, which was sawn from trees felled during three different seasons. The influence of the wood procurement season on drying behavior differed, on the one hand, between the drying phases above and below 30% moisture content in the conventional drying, and, on the other hand, between the conventional and vacuum drying methods. During the first steps of the conventional drying process, relative humidity in the kiln, as well as drying time and drying rate, varied according to the felling season. Variations in environmental conditions outside the kiln and the seasonal variation in the physical properties of the wood were presumed to be the reasons for differences in drying behavior. The difference in moisture content gradient, i.e., the difference in final moisture content between the inner wood and the surface layer of boards, was greater in conventionally dried timber than in vacuum-dried timber. In conventionally dried timber there was a clear seasonal variation in the gradient of final moisture content, which was greatest for winter-felled wood. The premature drying of the surface layer during the first steps of the conventional drying process of winter-felled wood was the reason for the higher gradient of moisture content. Storage of wood as logs decreased the standard deviation of the final moisture content.     

Controlling the morphology of ceramic and composite powders obtained via spray drying – A review

Spray drying is one of the most convenient methods for drying suspensions (slurries) and for granulation of materials. Spray dried powders have good flowability, narrow size distribution and controllable morphology. Morphology of powder particles (also called granules or microspheres) strongly affects the use and handling of powders. This review discusses the latest research on parameters that affect morphology and size of granules obtained by spray drying: atomization parameters, properties of sprayed slurry, mass transfer etc. The formation of hollow and dense granules is extensively reviewed. Granule size is affected by droplet size, slurry concentration and initial particle size. Morphology mostly depends on size distribution of initial ceramic particles, agglomeration tendency in the slurry and mechanical strength of the shell of a granule during the drying process compared to capillary force of the suspension liquid. Polymer additives (e.g. binders and lubricants) change the properties of granule shell and the evaporation of moisture; thus, polymer additives significantly affect morphology.     

Production of Crispy Granules of Fish: A Comparative Study of Alternate Drying Techniques

Three alternate dying methods—vacuum drying (VD), vacuum microwave drying (VMD), and pulse-spouted vacuum–microwave drying (PSVMD)—were examined experimentally for their potential as an industrial scale technology to produce granules of fish. Drying kinetics as well as key quality parameters such as expansion ratio, texture, color, sensory characteristics, and microstructure of crispy granules produced by these drying techniques were examined. Results showed that the drying time is reduced with an increase in microwave power level and with reduced pressure as expected. The quality of the granules is affected by the drying method and the operating parameters employed. Granules obtained using PSVMD at a microwave power density of 6.0 W/g displayed optimal quality required for the commercial product accepted by consumers.     

EFFECT OF PRETREATMENT AND DRYING ON THE QUALITY OF OYSTER MUSHROOMS (PLEUROTUS OSTREATUS)

Fruiting bodies of oyster mushroom were dried by hot-air drying, vacuum-drying and freeze-drying in order to compare food qualities after drying. Prior to drying, mushrooms were subjected to blanching or dipping in sodium metabisulphite solution (1 or 5 g/L), or dipping in citric acid solution (1 or 5 g/L). Drying of raw mushrooms was taken as a control. Blanching reduced the attractiveness of dry mushrooms; sodium metabisulphite improved it. It has been found that pretreatment and drying method affect the course and rate of drying. Samples subjected to hot-air drying and vacuum-drying were darker than those freeze-dried, which were clearly more attractive. The hot-air and vacuum-dried mushrooms on rehydration were inferior in quality to the freeze-dried samples. Flavor of the freeze-dried mushroom was not significantly different from that of the hot-air dried mushrooms. Food quality of dried mushrooms depends significantly on the type of drier used.

     

A Novel Atmospheric Freeze-Drying System Using a Vibro-Fluidized Bed with Adsorbent

Atmospheric freeze drying (AFD) in a vibro-fluidized bed dryer coupled with an adsorbent and multimode heat input is proposed for dehydration of food products at lower cost than the traditional freeze-drying process under vacuum. The aim of this project is to study the proposed AFD system using a vortex tube to produce low-temperature dry air, an alternative for producing dried food products of high quality. An experimental setup was designed and built to permit simultaneous application of convection, conduction, and radiation heat input to the drying material above its freezing point to ensure sublimation. A parametric evaluation over a broad range of possible parameter values was carried out using cubic-shaped potato and carrot as model heat-sensitive products. The influence of various system parameters on drying kinetics, quality, and functional properties of the dried products (color, rehydration properties, and morphology) were investigated. Comparison between physical quality and drying characteristics of the AFD system with AFD using fixed bed, fluidized bed dryer, and also with traditional vacuum freeze drying were carried out to investigate the viability of this new system. Results indicate that proposed system is an alternative to reduce the process time as well as to maintain the product quality at lower cost.     

A Vacuum Drying System for Green Hardwood Parts

A vacuum drying system was designed and fabricated and that system was used to dry green rough hardwood dimension. The red oak samples, 76.2 (long) × 7.62 (wide) × 2.54 (thick) cm, were dried from green moisture content (MC) to 7% MC in this system. They were dried at a pressure of 12 mm Hg and temperatures ranging from 30 to 50°C within 25 to 70 h. Drying quality tested included warp, internal checking, and surface checking. Moisture gradients along the length and thickness were measured. The standard prong test was used to assess the drying stresses. Vacuum drying was fast and the drying rate increased as the temperature increased. It was found that the general drying quality was good with no color change. Drying stresses including longitudinal and transverse stresses were small. There were no internal checks.     

A Novel Atmospheric Freeze-Drying System Using a Vibro-Fluidized Bed with Adsorbent

Atmospheric freeze drying (AFD) in a vibro-fluidized bed dryer coupled with an adsorbent and multimode heat input is proposed for dehydration of food products at lower cost than the traditional freeze-drying process under vacuum. The aim of this project is to study the proposed AFD system using a vortex tube to produce low-temperature dry air, an alternative for producing dried food products of high quality. An experimental setup was designed and built to permit simultaneous application of convection, conduction, and radiation heat input to the drying material above its freezing point to ensure sublimation. A parametric evaluation over a broad range of possible parameter values was carried out using cubic-shaped potato and carrot as model heat-sensitive products. The influence of various system parameters on drying kinetics, quality, and functional properties of the dried products (color, rehydration properties, and morphology) were investigated. Comparison between physical quality and drying characteristics of the AFD system with AFD using fixed bed, fluidized bed dryer, and also with traditional vacuum freeze drying were carried out to investigate the viability of this new system. Results indicate that proposed system is an alternative to reduce the process time as well as to maintain the product quality at lower cost.     

Review of Wood Drying Research in Brazil: 1984-2004

In Brazil, research on wood drying has been more focused on applied aspects than on fundamentals ones, and results have been published almost exclusively in Brazilian journals. The study of lumber deformation under aggressive drying conditions resulted in methods to group species and to define kiln schedules. Relationship between moisture content and electrical resistivity was used to improve quality control of dried lumber as well automatic control of the kiln drying process. Conventional kiln drying is the most common method for industrial drying, but seasoning and solar drying were also studied. The biggest research effort was directed to improve the drying of eucalypt lumber.     

OPTIMAL CONTROL OF THE PRIMARY AND SECONDARY DRYING STAGES OF BULK SOLUTION FREEZE DRYING IN TRAYS

The problem of operating a tray freeze dryer to obtain a desired final bound water content in minimum time is formulated as an optimal control problem with the use of the rigorous unsteady state mathematical model of Sadikoglu and Liapis [9] that has been found to describe satisfactorily the experimental dynamic behavior of the primary and secondary drying stages of bulk solution freeze drying of pharmaceuticals in trays. The heat input to the material being dried and the drying chamber pressure are considered to be control variables. Constraints are placed on the system state variables by the melting and scorch temperatures during primary drying, and by the scorch temperature during secondary drying. Necessary conditions of optimality for both the primary and secondary drying stages are derived and presented, and an approach for constructing the optimal control policies that would minimize the drying times for both the primary and secondary drying stages, is presented. The theoretical approach presented in this work was applied in the freeze drying of skim milk, and significant reductions in the drying times of primary and secondary drying were obtained, when compared with the drying times obtained using the operational policies reported in the literature, by using the optimal control policies constructed from the theory presented in this work. Furthermore, it is shown that the optimal control policy leads to the desired in practice result of having at the end of secondary drying temperature and bound water concentration profiles (in the dried layer) whose gradients are very small. It is also shown that by using the optimal control policy and an excipient capable of increasing the melting temperature without affecting product quality, one can significantly reduce the drying time of the primary drying stage.     

洋葱真空干燥动力学研究

为研究洋葱在真空干燥条件下的干燥特性,选用不同干燥条件对洋葱进行脱水处理,测定不同工艺条件下洋葱的干燥曲线和干燥速率曲线。结果表明,温度和真空度对洋葱真空干燥过程都有明显的影响,且洋葱真空干燥的动力学模型符合Page方程,并得到本试验条件下的动力学模型。     

THE EFFECT OF PROCESS CONDITIONS ON THE DRYING KINETICS AND REHYDRATION CHARACTERISTICS OF SOME MW-VACUUM DEHYDRATED FRUITS

ABSTRACT

The effect of drying conditions, namely, microwave power, vacuum pressure, as well as sample geometry, on the drying kinetics and rehydration characteristics of five microwave vacuum dehydrated fruits (apple, avocado, mushroom, pear and strawberry) was studied. The investigation involved a wide range of microwave power, vacuum pressure and sample size levels. The drying rate and the rehydration ratio, a measure of rehydration characteristics, were found to depend on the drying conditions. An empirical mass transfer model, involving a characteristic parameter for each process (drying and rehydration( as a function of process variables, namely, microwave power, vacuum pressure and sample size, was also tested with the data obtained in a microwave oven equipped with vacuum apparatus. Furthermore, a comparison of rehydration properties of microwave vacuum and conventionally dehydrated products, was conducted.