REACH法规实施细则解读(二)

5 实施REACH法规的负面影响 2003年,欧盟委员会在其对化学品生产商和进口商的测试和注册费进行评估后的报告中称,估计在11年内(2008年至2018年),由测试和注册产生的直接成本总计约23亿欧元.如果有1%～2%的物质停止生产,面临高额替代时,下游用户将增加成本5～13亿欧元.这是针对欧盟范围内的化工企业和下游用户而言的.     

贝先国烹制的湘菜香飘沈阳

贝先国,现年31岁,从厨近20年,湖南测阳人,先后在长沙、郑州、北京等地工作,高级烹调技师,他曾在郑州市烹饪比赛获得金奖,现任丽湖蒸菜厨师长.丽湖蒸菜于2005年12月5号开业,其中三好旗舰店坐落于沈阳的IT中心三好街,营业面积600平方米,食物以湘菜为主,并根据东北的口味进行了改良,从色香味上看都属精品.店面布置得很优雅,大厅明亮,半隔断的小包房也很温馨.     

"5.12"汶川特大地震给四川工商职业技术学院造成巨大损失

本刊讯 "5.12"四川汶川8.0级特大地震,给地处都江堰市,紧邻地震中心汶川映秀镇的四川工商职业技术学院造成了巨大损失.地震袭来.建筑物左右摇晃,天花板和墙壁装饰纷纷脱落,电脑、文件柜等办公设备纷纷倒塌,学生7号宿舍、素质拓展馆和活动中心的半面墙壁轰然塌下.     

千年酱文化水乡得发扬——"2007中国首届酱文化国际高峰论坛"在浙江绍兴隆重举行

中国第一座酱文化博物馆开馆祭祖庆典暨2007中国首届酱文化(绍兴)国际高峰论坛于12月15日在浙江绍兴隆重举行.15日上午,在绍兴县平水镇的绍兴至味食品有限公司厂区内的中国酱文化博物馆门前,举行了盛大的开馆庆典及祭祀酱园鼻祖蔡邕仪式.开馆仪式结束后,有来自中、美、意、日、韩、新、泰七国和港台两地区的300多名专家、学者和企业家,又参加了于12月15日下午至17日,在浙江省绍兴隆重举行的"2007中国首届酱文化(绍兴)国际高峰论坛".     

小米的化学成分及物理性质的研究进展

系统地介绍了国内外对小米中各种化学成分及其营养保健功能的研究进展,包括碳水化合物、蛋白质和氨基酸、脂肪及脂肪酸、维生素、矿物质和微量元素、色素、肌醇、黄酮、多酚等的含量及营养保健功能.同时,对小米物理性质方面的研究进展也做了介绍.     

"头羊"的代价——参加中国(广东)国际印刷技术展首日走笔

中国(广东)国际印刷技术展览会作为北京国际印刷技术展览会的姊妹展,4月10日上午一开幕,立刻博得了满堂彩.为确保来参加展览的车辆及观众顺利进入现场,主办方得到了当地政府交管部门的支持,对展览馆附近一些道路进行了疏导,不相干的车辆及行人被有效疏散到别的地方.尽管首日上午阴雨绵绵,但丝毫没有影响到馆内汹涌的人流.     

中国黄酒的科研现状及发展

论述了中国黄酒近年的发展与行业整体科技水平的提升。酿造企业在设备上已,一泛实现了机械化与半机械化;工艺技术上在传统工艺的基础上应用了新工艺与新技术,提高了产品的质量安全水平;产品包装上出现了精美高雅的各式包装：产品品种上以新风格口感为导向,开发改变了单一的风格特征;在功能性研究上,除发现了γ-氨基丁酸外,还对黄酒中的功能性物质进行了深入的研究。     

中国名牌的综合效应——考量国产胶印机的诚信标杆

近年来,"中国制造"已经势不可挡地崛起并成为助推全球经济发展的强大动力.上海光华同北人、中景、大族冠华等一批优秀的单张胶印机制造商一道,在"中国制造"的世界潮流中,或争相推出高性价比的替代进口产品,或积极参与国际贸易把单张胶印机导入海外市场.目前,我国已经拥有几十家胶印机制造商,拥有年产销万余台胶印机的能力,能够满足国内10万家印刷企业90%以上的胶印机市场数量型需求,能够把胶印机销售到全球几十个国家.在这样的背景下,提出培育中国胶印机名牌的课题,从时机和条件方面看,都具备了相当的基础.     

全球标签市场现状及展望

到2011年,全球标签产量将达到500亿平方米,年增长率为7%总产值将达1000亿美元,年增长率为9%左右.受全球包装市场扩张的影响,特别是特殊饮料、个人护理产品和医药产品的异军突起,全球标签市场的发展前景也将更加广阔.此外,随着世界的不断发展,先进的物流和数据处理系统在发展中国家的普及、尖端技术的开发和渗透以及增值标签功能的日益完善也将为标签业的发展起到重要的推动作用.     

HAVE A REST——欧宝卡车情景

正我对二战轮式车辆一直比较喜爱,而自己一直没有做过二战德军的卡车系列,在看了很多高手的卡车作品后自己也想开工一辆,我最终选择了制作一辆经典的欧宝3吨4×2卡车。欧宝卡车作为二战德军重要的轮式车辆,不仅产量很大而且根据不同的用途又衍生出了很多不同的型号,货厢版是最基本的欧宝3吨卡车,也是群众基础最好的一个版本,但正是因为做的人太多,对于我这种追求"个性"的人来说,做一个普通的货厢版无疑是缺乏吸引力的。为了让自己的欧宝卡车能别具一格,我查阅了一些欧     

Microencapsulation of flaxseed oil in flaxseed protein and flaxseed gum complex coacervates

Flaxseed oil, a rich source of omega-3 fatty acids, was microencapsulated in a novel matrix formed by complex coacervation between flaxseed protein isolate (FPI) and flaxseed gum (FG). This matrix was crosslinking with glutaraldehyde. Liquid microcapsules with three core (oil)-to-wall ratios (1:2, 1:3 and 1:4) were prepared and spray-dried or freeze-dried to produce powders. The microencapsulation efficiency, surface oil, morphology and oxidative stability of these microcapsules were determined. The spray-dried solid microcapsules had higher oil microencapsulation efficiency, lower surface oil content, smoother surface morphology and higher oxidation stability than the freeze-dried microcapsules. The highest microencapsulation efficiency obtained in spray-dried microcapsules was 87% with a surface oil of 2.78% at core-to-wall ratio 1:4 and oil load 20%. The oxidation stability obtained from spray-dried microcapsules at core-to-wall ratio of 1:4 was nearly double that of the unencapsulated flaxseed oil.     

酶法脱除亚麻籽胶的工艺研究

采用酶法脱除亚麻籽胶,并考察了酶的种类、酶解温度、酶解时间、pH值、酶加入量、总料液比对亚麻籽胶脱除效果的影响。通过单因素和正交试验确定了酶解脱除亚麻籽胶的最佳工艺条件:酶制剂为果胶酶、温度55℃、时间4h、pH值为3.5、酶加入量为100u/g、总料液比为1:6,该条件下亚麻籽的脱胶量可以达到9.53g。     

Complex coacervation between flaxseed protein isolate and flaxseed gum

Flaxseed protein isolate (FPI) and flaxseed gum (FG) were extracted, and the electrostatic complexation between these two biopolymers was studied as a function of pH and FPI-to-FG ratio using turbidimetric and electrophoretic mobility (zeta potential) tests. The zeta potential values of FPI, FG, and their mixtures at the FPI-to-FG ratios of 1:1, 3:1, 5:1, 10:1, 15:1 were measured over a pH range 8.0–1.5. The alteration of the secondary structure of FPI as a function of pH was studied using circular dichroism. The proportion of ɑ-helical structure decreased, whereas both β-sheet structure and random coil structure increased with the lowering of pH from 8.0 to 3.0. The acidic pH affected the secondary structure of FPI and the unfolding of helix conformation facilitated the complexation of FPI with FG. The optimum FPI-to-FG ratio for complex coacervation was found to be 3:1. The critical pH values associated with the formation of soluble (pHc) and insoluble (pH_ɸ1) complexes at the optimum FPI-to-FG ratio were found to be 6.0 and 4.5, respectively. The optimum pH (pH_opt) for the optimum complex coacervation was 3.1. The instability and dissolution of FPI–FG complex coacervates started (pHɸ₂) at pH 2.1. These findings contribute to the development of FPI–FG complex coacervates as delivery vehicles for unstable albeit valuable nutrients such as omega-3 fatty acids.     

炒籽温度对压榨亚麻籽油品质的影响

采用不同温度对亚麻籽进行炒籽并压榨制油,对压榨亚麻籽油的感官品质、理化指标及营养成分进行分析,研究炒籽温度对压榨亚麻籽油品质的影响。结果表明:随着炒籽温度的升高,压榨亚麻籽油的气味从坚果芳香过渡到严重焦糊味,色泽加深,在195℃炒籽45 min时形成热榨亚麻籽油特有的浓香型风味;营养成分如VE、总酚以及甾醇含量随炒籽温度升高而逐渐减少,在255℃炒籽45 min时,3种营养成分的损失率分别为75. 7%、76. 5%和88. 9%;酸价、过氧化值、茴香胺值、K232值、K270值随炒籽温度升高而增加,且炒籽温度对压榨亚麻籽油中主要脂肪酸含量有显著影响;适当炒籽对压榨亚麻籽油的氧化稳定性是有利的;高温炒籽压榨亚麻籽油中的营养成分含量与其理化指标密切相关,进而共同影响压榨亚麻籽油的品质。     

亚麻籽脱皮及亚麻仁酱的研究

亚麻籽经160℃烘烤10min,在脱皮机上脱皮后,把仁皮混合物用12目和20目筛分成三部分,结果仁中含皮率为9.31%,皮中含仁率为0.89%,感官评价最好.产品中α-亚麻酸占到酱体总重的31.2%,比同重量亚麻籽的α-亚麻酸高出10.9%.包装为一次性消费小包装,净重3.5g,每包含有1g α-亚麻酸,是人体平均每天应需补充ω-3多不饱和脂肪酸的理论值.     

Laws of flaxseed mucilage extraction

This study examined the application of few-stages aqueous extraction of mucilage from whole flaxseed. Key processing conditions included temperature (40-100 °C), duration (0-60 min), seed to water ratio (1 to 5-30) and mixer rotational speed (0-240 revolutions per minute). It was found, that mucilage extraction from flaxseed is appropriate to carry out without swelling. The maximum yield of flaxseed mucilage was obtained at 80 ± 2 °C with seed to water ratio of 1 to 25. The equation, which described equilibrium solid yield during the extraction depending on the phases’ ratio and the temperature, was found. The equation of solid yield depending on duration and mixer rotational speed under the temperature of 80 ± 2 °C and the seed to water ratio of 1 to 25 was determined. It was showed, that the use of stirring is not expedient for the intensifying the process. The rational duration of extraction under the selected parameters was 30 ± 1 min. To increase the solid content in the extract the few-stages extraction was applied. The three-stage countercurrent extraction of flaxseed mucilage from whole seeds under the temperature of 80 ± 2 °C, the seed to water ratio of 1 to 25, the duration of each stage of 30 ± 1 min was established to receive flaxseed mucilage extract with content of solids from 0.70 to 0.72%, i.e. to extract from 98.3 to 99.1% of mucilage from flaxseed.     

亚麻籽油的热稳定性研究

通过加热试验,研究了亚麻籽油的热稳定性。结果表明:在高温加热条件下,亚麻籽油中α-亚麻酸含量有所降低,总反式脂肪酸的含量提高;在200℃和250℃条件下保持120 min后,亚麻籽油中α-亚麻酸的含量分别下降了6.1%和57.7%,总反式酸的含量分别为4.47%和20.89%。说明亚麻籽油作为烹调用油,烹调温度在200℃以下比较合适,加热时间不宜过长。     

Characteristics of flaxseed hull oil

Oils from two commercial flaxseed hulls extracted by six procedures were evaluated for physicochemical characteristics. Oil yield ranged from 9% to 28% depending on solvent and extraction. Lipid fractionation of crude flaxseed hull oil yielded 92.5% neutral lipids, 3.1% phospholipids, 2.4% acidic lipids and 2.1% free fatty acids. Flaxseed hull oil exhibited three thermal transitions between −35 and −13 °C with solvent dependent polymorphism. Thermal oxidation by differential scanning calorimetry (DSC) revealed three step oxidation of flaxseed hull oil with mean onset and oxidation temperatures at 121 and 150–253 °C, respectively depending on the extraction procedure. Flaxseed hull oil exhibited two-fold difference (0.6–1.2 μm Trolox equivalent/g) in antioxidant activity measured by a photochemiluminescence (PCL) assay. Supercritical CO₂ extracted the most oil with the highest antioxidant capacity of all evaluated procedures resulting in a defatted flaxseed hull containing the highest (53 mg/g) secoisolariciresinol diglucoside (SDG) level.     

Antioxidant activity of flaxseed oil

Effective concentration of antioxidants and its reactivity toward peroxil radicals (constant k7) have been measured by the chemiluminescence technique for flaxseed oil. Effective concentration of antioxidants is shown to depend on the technology of producing flaxseed oil; period of seed storage before use; and storing duration of flaxseed oil also. Minor component content of flaxseed oil, which may be the members of antioxidant pool, has been quantitatively estimated.     

Chromatographic separation of flaxseed phenolics

A column chromatography method for separation of phenolic compounds from flaxseed using Sephadex LH-20, RP-8 and silica gel is described. TLC analysis proved that separated fractions contained numerous phenolic compounds. All fractions exhibited a maximum UV absorption between 270 and 290 nm. Additional shoulders were observed between 274 and 350 nm. These results imply that lignans and their derivatives are the main phenolic compounds present in flaxseed.