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采用悬浮液进样火焰原子吸收光谱法(FAAS法)测定土壤样品中微量锰;并对样品的粒度、悬浮液的浓度、介质酸度、校正方法及抗干扰等进行了探讨。结果表明,本法简便、快速、准确可靠。 相似文献
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《硅酸盐通报》2015,(Z1)
采用高能球磨法制备水基Fe_3O_4磁性颗粒,研究了转速对其研磨效果、粘度、沉降稳定性、样品形貌及流变性能的影响。结果表明:球磨机转速对Fe_3O_4磁性颗粒悬浮液的粘度和沉降稳定性的影响很大。在相同的研磨时间内,随着转速的提高悬浮液中超细颗粒的含量增多,转速为200 r/min,球磨机对物料有很好的研磨效果;悬浮液的零场粘度先增大后减小;悬浮液的沉降率先减小后增大,沉降量是先变少后变多的过程,当球磨机转速定为200 r/min时,所得样品的稳定性最好;磁场强度低于65 mT时,在相同磁场强度下,低转速制取样品的剪切应力较大。磁场强度高于65 mT时,在相同磁场强度下,高转速制取样品的剪切应力较大。 相似文献
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悬浮液进样石墨炉原子吸收光谱法测定饲料样品中痕量铜 总被引:2,自引:0,他引:2
采用悬浮液进样技术并结合灵敏度较高的石墨炉原子吸收光谱法测定饲料样品中的痕量铜,对悬浮液介质、基体改进剂进行了选择,对灰化和原子化过程进行了探讨,本法的精密度(RSD)为4.12%,加标收回率为97.0%。 相似文献
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为研究高浓度纳米颗粒悬浮液的粒径分布表征,引入超声谱高浓度颗粒粒径测量理论(核壳模型),同时搭建了一套超声法高浓度悬浮液粒径测量实验装置,并进行理论模型的实验验证,测得体积浓度为10%至30%的纳米铟锡金属氧化物(Indium Tin Oxides,ITO)水性悬浮液的超声衰减,通过数据反演技术最终获取样品的颗粒粒径分布。结果表明:高浓度纳米颗粒悬浮液中声衰减系数随浓度增加但偏离线性递增趋势,与核壳模型数值模拟更接近。同时,粒径反演的结果与高速离心沉降法也较为吻合。 相似文献
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使用合适表面处理剂,通过剪切、搅拌混合和超声波处理,制备了高浓度n—SiOx分散悬浮液;在合适的剪切强度下,将分散悬乳液按n-SiOx质量分数为2.0%均匀分散在天然乳胶中,制备了n-SiOx补强型天然乳胶膜试样。乳胶膜直角撕裂强度测试结果和扫描电子显微镜图像分析表明,n-SiOx粒子较好地分散在天然乳胶中,能与乳胶分子链形成较为牢固的整体结构,其剪切强度较白炭黑试样提高了52.32%;n-SiOx悬浮液浓度是实验的主要影响因素,超声波分散时间、25G工作头转速和均质分散时间次之。 相似文献
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电石渣的排放及贮存量日益递增,电石渣硅铁的资源化利用也成为亟待解决的难题。为实现电石渣硅铁的高值化应用,以干法电石渣中分离出的磁性硅铁为加重质配制重介质悬浮液,并探究了悬浮液密度、黏土含量和硅铁粒度等因素对其粘度及沉降特性的影响。结果表明,增大悬浮液密度或黏土用量以及减小硅铁粒度均会使悬浮液的粘度提高,从而使加重质颗粒的沉降速度下降,稳定性得到提升。此外,为了进一步验证该悬浮液体系用于实际分选的可行性,将不同密度的悬浮液用于选煤浮沉试验分选混合煤样,在密度为1.30 g/cm3和1.40 g/cm3的重介质悬浮液中,浮煤产率高且灰分含量较初始煤样大幅降低,说明该悬浮液体系具有良好的分选性能。 相似文献
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Noor Faeizah Amat Andanastuti Muchtar Mariyam Jameelah Ghazali Norziha Yahaya 《Ceramics International》2014
The stability of nano-zirconia 3YSZ powder in suspension was extensively studied by the colloidal method, and the optimum sintering temperature of the green sample fabricated through slip casting was determined. Zirconia suspensions with 10 vol% powder loading were prepared with distilled water, and HNO3 was used to adjust the pH of the suspension to pH 1–6. All of the suspensions were subjected to sedimentation test, and the results showed that the suspensions adjusted to pH 2 had the lowest sediment volume. This finding indicates that a suspension with pH 2 produces higher packing density. Viscosity test was carried out for the suspensions added with dispersant ranging from 0.3 wt% to 0.7 wt% polyethyleneimine (PEI) with and without pH adjustment. The suspension containing 0.5 wt% PEI with pH 2 adjustment produced the lowest viscosity because of interparticle bond breakage in the aggregates, thus forming colloidally stable suspensions. The zirconia suspension containing 0.5 wt% PEI and whose pH was adjusted to pH 2 was chosen to be slip casted into cylindrical shape. Green samples were sintered at various sintering temperatures that ranged from 1100 °C to 1500 °C through a two-step sintering method. The sample sintered at 1500 °C was found to be porosite-free, and its highest relative density was 99.6% of the theoretical density. Morphological studies detected pores in the microstructure of the samples sintered at low sintering temperatures (1100 and 1200 °C). By contrast, the samples sintered at 1400 and 1500 °C were fully densified. However, the grain size of the sample sintered at 1500 °C was 230 nm, which indicated excessive grain growth. The Vickers hardness of the sample sintered at 1400 °C was found to be highest (12.9 GPa) and comparable to results found in the literature. 相似文献
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乙螨唑为噁唑类新型专用杀螨剂,三唑锡为触杀作用较强的广谱性杀螨剂,由二者制成的复配悬浮剂可起到增效作用。开展了对23%乙螨唑·三唑锡悬浮剂防治柑橘红蜘蛛的田间药效试验。结果表明,有效成分浓度为200、100、50 mg/kg的23%乙螨唑·三唑锡悬浮剂,防治柑橘红蜘蛛速效性好,持效期长;药后1、3、10、15、20、30 d的防效均达到95%以上,与对照药剂20%三唑锡悬浮剂100 mg/kg和110 g/L乙螨唑悬浮剂比较,各处理与三唑锡对照防效相当,极显著优于乙螨唑对照。 相似文献
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D.C.-H. Cheng 《Powder Technology》1984,37(1):255-273
The literature and recent WSL results on suspensions of spherical particles are surveyed and summarised. It is concluded that the steady shear properties of a dense suspension is not characterised by an unique viscosity or flow curve, but rather it is described by a wide viscosity distribution or a shear stress - shear rate flow band whose mean and standard deviation are functions of solids concentration, particle size distribution and viscometric geometry and dimensions. The standard deviation (or data spread) increases with solids concentration and with decreasing viscometer gap to particle diameter ratio. This property is due to poor sample reproducibility in respect of solids concentration and particle size distribution and the inherent two-phase nature of suspension which gives rise to particle migration and consequently non-uniform packing density or structure in a sample. Because a dense suspension is increasingly sensitive to these factors as concentration is increased, the standard deviation can be very large. Because the details of packing structure vary with flow, the viscosity distribution or flow band depends on viscometric flow geometry and measuring element dimensions. The implications of this conclusion on the study and characterisation of dense suspension property and the prediction of its behaviour in industrial handling and process equipment are discussed. 相似文献
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研究了铬酸钡分光光度法应用于氯乙酸副产混合气中总硫含量测定的实例。探讨了气体采集、样品溶液处理和铬酸钡悬浮液配制等关键问题。硫元素经碱液吸收和双氧水氧化完全转化为硫酸根,硫酸根再与铬酸钡悬浊液反应,定量置换出铬酸根,溶液的吸光度即与硫酸根的浓度成正比。该方法的测定波长为372 nm,硫酸根质量浓度在0~10 mg/L线性关系好。该方法操作简单,精密度和准确度均符合测定要求,适用于工厂气体的实时监测。 相似文献
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The particle size distribution determined by means of the Coulter Counter TA II (CC TA II) apparatus was compared with two artificial distributions prepared from fractions of polymeric spherical particles. The data were numerically treated using a new distribution function, and the fit was satisfactory. The applicability of CC TA II along with the numerical and graphic evaluation is documented for a real sample of the product of suspension radical polymerization. 相似文献
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