Observation of Field-induced Anomaly in High-field Magnetization on a Complex Spin-Driven Multiferroic Compound, LiCu2−z Zn z O2

We performed high-field magnetization measurements in the pulse magnetic fields up to 55 T at low temperatures on a doped LiCu_2?z Zn _z O₂ (z=0.07). When H // c-axis, one anomaly was clearly observed in $\frac{dm}{dH}$ curves at ～9 T. The anomaly broadens as temperature increases and disappears at ～15 K, which is close to the critical temperature of spiral spin phase and the formation of isolated spin-dimer. Interestingly, an additional peak shows up at 4.2 K, indicating a possible boundary at ～5 K. On the other hand, when H // a-axis, one broad anomaly can be distinguish which is centered around 11.8 T. However, this anomaly only appears at T≤5.5 K, which is much lower than 15 K, indicating the origin of this anomaly could be different with those in H // c-axis. It is probably comes from the broken one-dimensional chain and the complex inter-chain interactions.     

Effect of Te Doping on the Structure and Superconductivity of K x Fe2−y Se2−z Te z Single Crystals

We report the structure, transport, and magnetic properties of K _x Fe_2?y Se_2?z Te _z single crystals grown by optical floating zone technique. The phase separation phenomena were observed in the Te-doped samples. With increasing Te doping level, the c-axis lattice parameter expands for both insulating/semiconducting and superconducting phases while the superconducting transition temperature (T _c) decreases and eventually vanishes at z = 0.51. The critical current density was estimated to be 10³–10⁴ A/cm² for the all doped samples. The upper critical field and anisotropic superconducting ratio increase with Te doping. We compared the results of critical current density J _c, upper critical field μ ₀ H _c2 and apparent thermally activated energy U ₀ for the samples with z = 0, 0.09, and 0.16. The influence of Te doping on the vortex pinning and the implication of U ₀ versus μ ₀ H is discussed.     

z浅析智能防窃电技术

窃电给供电企业造成巨大的经济损失。常规的防窃电方式已经很难有效的防止窃电。本文论述了几种常见的窃电方式,并阐述了当前常见的几种智能防窃电技术。     

低损耗z型铁氧体的研究

采用固相反应法制备(Ba3-xBixCo2Fe24-xCuxO41)铁氧体材料。研究铋、铜联合取代Z型六角铁氧体中钡、铁离子对材料性能的影响,结果表明,少量的取代量不会影响z相形成。取代量较少时(0.1≤x≤0.2),磁导率增大,有较高的品质因素Q,材料的介电常数和介电损耗都较小,小于800MHz材料的介电损耗tan<0.02。     

Cation composition variation observed in Y1Ba2Cu3O7−z

The cation concentration ratio in the individual grains (1 to 25 μm) of four Y₁Ba₂Cu₃O_7−z pellets was investiga spectroscopy. A spread in the cation composition was observed even in a sample showing a narrow superconducting transition. The concentrations of Y, Ba and Cu were in the ranges 12–20, 30–35 and 48–53 at%, respectively. It is, therefore, likely that the Y₁Ba₂Cu₃O_7−z structure covers a finite area on the YO_1.5-BaO-CuO phase diagram.     

Thermal Conductivity Properties of Bi2-αTlαSr2Ca2Cu3O10+z Glass-ceramic HT c Superconductor Rods

The Glass rods with nominal composition of (Bi _2- Tl )Sr ₂ Ca ₂ Cu ₃ O _10+z , where =0.15, 0.25 and 0.35, have been prepared by melt casting technique. Preferably c-axis oriented grains were grown after the sintering process. The thermal conductivity (T) measurements were performed between 30K and 290K and calculations were made using Wiedemann-Franz law. The (T) values of the samples varied between 3.8 to 8.9 mW/cm.K and showed strong dependence to the heating temperatures and compositions. The best T _c and T _zero were obtained to be 122 K and 115 K respectively.     

Mg含量对Mg3(1+z)Sb2化合物热电传输性能的影响

Mg₃Sb₂化合物具有良好的热电性能和成本优势, 受到研究者的广泛关注。由于Mg元素具有很高的饱和蒸汽压和化学反应活性, 因此Mg₃Sb₂在合成过程中含量难以精确控制。本研究利用固相反应/球磨结合放电等离子体烧结制备了不同Mg含量的Mg_3(1+z)Sb₂(z=0, 0.02, 0.04, 0.06和0.08)样品, 通过物相结构分析和热电性能测试, 研究了Mg含量对Mg₃Sb₂化合物热电性能的影响规律。结果表明, 随着名义Mg含量的增加, 实际Mg含量在Mg₃Sb₂化合物中由缺失状态转变为过量状态, Mg_3(1+z)Sb₂(z=0, 0.02, 0.04)样品存在Mg空位(${{\text{{V}'}}_{\text{Mg}}}$), 表现为p型传导; 而Mg_3(1+z)Sb₂ (z=0.06, 0.08)样品中存在间隙Mg($\text{Mg}_{\text{i}}^{\centerdot \centerdot }$), 表现为n型传导。Mg_3(1+0.04)Sb₂样品在较宽温区(室温至770 K)内保持最高的热电优值, 该样品最接近本征p型Mg₃Sb₂化合物的组成和热电性能。本研究表明, Mg含量对Mg_3(1+z)Sb₂化合物载流子类型和浓度以及迁移率具有一定的调控作用。     

z≤16的齿轮测量中的一个问题

《计量技术》辑编部: 根据机械工业部部标《渐开线圆柱齿轮精度》(JB179—83)要求,确定渐开线齿形测量部位,一般用两种方法;第一、按共轭齿轮啮合时的工作圆计算;第二、在相配齿轮不清楚时,按与标准齿条啮合时的工作圆计算。在按第二种方法计算齿廓起测点展开弧长b_1(或展开角φ_1,下同)时,一般都认为:齿数z≤16齿的齿轮,基圆半径r_b大于齿轮与标准齿条啮合时的工作圆半径R(即过齿条齿顶线与啮合线的交点T的圆,如图1所示),这时不需计     

z向流动RTM工艺树脂的流动浸润行为

研究了层间“离位”附载多孔薄膜结构形式增韧层的大厚度纤维预成型体中等代流体（树脂）沿预成型体厚度方向（z向）的流动行为,通过压力传感器监测z向流动RTM（z-RTM）工艺注射过程中进、出胶口压力的变化规律,进一步反推树脂在层间“离位”增韧与非增韧预成型体中的宏观流动及微观浸润模式。结果表明,在 z-RTM工艺注射过程中,树脂在沿纤维束间z向快速流动的同时完成对纤维丝束内部的浸润。层间“离位”附载的增韧层虽延缓了树脂的宏观流动,但使流动前锋曲面更加平滑。层间“离位”增韧预成型体z向渗透率为3.5×10^-15m²,与非增韧预成型体的z向渗透率2.9×10^-14m²相比,降低约一个数量级。     

预应力连续箱梁桥的基准动力有限元模型研究z

介绍了作为预应力混凝土连续梁桥的通扬运河特大桥的环境激励振动试验,并利用基     

高温稀土永磁体Sm(CoCuFeZr)z的研究现状

总结了影响高温磁体使用温度的关键因素，分析了成分对高温永磁体Sm(CoCuFeZr）z使用温度的影响，概括了高温永磁体Sm(CoCuFeZr)z的矫顽力机理，并探讨了高温永磁体Sm(CoCuFeZr)z今后的研究方向。     

高温氮化法制备z=3的β-Sialon材料

以Al2O3粉、Al粉和Si粉为主要原料,经高温氮化反应制备β-Sialon材料。研究了TiO2烧结助剂、烧结温度和保温时间对制备β-Sialon材料的影响。结果表明,添加TiO2作烧结助剂,在N2气氛中于1500℃保温5h后烧成的试样耐压强度达到76.94MPa、体积密度达到2.86g/cm3;试样以β-Sialon为主晶相,晶粒发育较好,呈棱柱状,直径约为1μm,长度约为2μm,且分布比较均匀,提高了材料的强度。     

Sm(CO,Fe,Cu,Zr)z(6.5≤z≤8.5)高温永磁合金的组织结构与性能

介绍了Sm（Co,Fe,Cu,Zr）z永磁合金的显微组织结构特点以及热处理工艺参数对组织结构的影响,讨论了Sm含量及合金元素对微观组织与性能的影响规律,并对合金的矫顽力随温度的反常变化现象、矫顽力增强机理和热稳定性研究进行了总结和讨论．     

Bond Angle Study of Self-compensating Y1−x Ca x Ba2−x La x Cu3O z System

Single-phase samples of a self-compensating Y_1?x Ca _x Ba_2?x La _x Cu₃O _z system were synthesized through a solid-state reaction method with x<0.4. The structure of all samples were characterized by X-ray diffraction and refined by the Rietveld method. Superconducting properties have been investigated by the DC magnetization measurement. The critical temperature (T _c ) decreases evidently with the increment of x although the carrier concentration remains constant in the samples for different doping level. Careful study of the chemical bonds in the crystalline lattice demonstrates that the T _c is closely correlated to four pairs of bond angles in the unit cell. The analysis indicates that crystalline structure is one of the important factors to high-T _c superconductivity, and its influence is independent of the carrier concentration.     

Determination of the Melt Undercooling Required for Producing Al x Ga y In1 – x – y Sb1 – z Bi z /InSb Heterostructures

Conditions for temperature-gradient epitaxial growth of Al _x Ga _y In_{1 – x – y} Sb_{1 – z} Bi _z /InSb heterostructures are examined. The factors are established which determine the initial melt undercooling required for preventing the thermal degradation of the substrate.     

硅微z轴谐振陀螺仪负电刚度效应分析及实验验证

介绍了在开环工作状态下硅微z轴谐振陀螺仪由于加工工艺缺陷所导致的误差机理。为减小陀螺仪初始电容差和抑制正交耦合误差，提出了一种闭环控制检测策略。重点分析了其力矩反馈器的电刚度效应并给出其线性数学模型表示式。通过对硅微z轴陀螺仪敏感模态的反馈力与谐振频率的关系分析，间接得出了在敏感方向上电负刚度与力矩器所施电压的内在联系，并在实验上进一步验证电刚度效应。这将为下一步闭环控制方案的设计奠定重要基础。     

硅微z轴谐振陀螺仪负电刚度效应 分析及实验验证

介绍了在开环工作状态下硅微z轴谐振陀螺仪由于加工工艺缺陷所导致的误差机理。为减小陀螺仪初始电容差和抑制正交耦合误差,提 出了一种闭环控制检测策略。重点分析 了其力矩反馈器的电刚度效应并给出其线性数学模型表示式。通过对硅微z轴陀螺仪敏 感模 态的反馈力与谐振频率的关系分析,间接得出了在敏感方向上电负刚度与力矩器所施电压的 内在联系,并在实验上进一步验证电刚度效应。这将为下一步闭环控制方案的设计奠定重要 基础。     

基于Euclidean距离的纸张z向截面中墨层图像分割

目的通过图像分割方法得到纸张z向截面中印刷墨层区域的图像,利于更好地分析研究油墨在纸张中的分布。方法利用物理切割方法和超景深显微镜拍摄,得到高分辨率的纸张z向截面彩色图像,将该图像从RGB颜色空间转换到HIS空间,采用欧式距离作为相似性度量,实现油墨层的分割。结果在HIS空间对油墨层图像进行分割时,分割阈值选取为3倍样本标准差最大值时,分割图像精确;当分割阈值取4倍或者2倍、1倍时,出现了过度分割或者欠分割。结论分割得到的油墨层图像有利于定量计算油墨的渗透深度及渗透分布,为进一步定量研究油墨与纸张的相互作用奠定了一定的基础。     

具有正温度系数的2:17型Sm(Co,Fe,Cu,Zr)z永磁体的研究现状

总结了矫顽力具有正温度系数的2:17型Sm(Co,Fe,Cu,Zr)z永磁体的研究现状;分析了成分与胞状显微组织对矫顽力正温度系数的影响,概括了目前解释矫顽力正温度系数的几种矫顽力机制模型,提出了对矫顽力正温度系数的研究是高温永磁体Sm(Co,Fe,Cu,Zr)z今后一个很有前景的新研究方向.