The Maia 384 detector array in a nuclear microprobe: A platform for high definition PIXE elemental imaging

Application of nuclear microprobe event-by-event data acquisition approaches to synchrotron elemental imaging is at the heart of the design of a large energy-dispersive detector array called Maia, under development by CSIRO and BNL for SXRF elemental imaging on the X-ray microprobe. A new project is aimed at harnessing this development to provide high throughput PIXE imaging on the CSIRO Nuclear Microprobe. Maia combines a 1.2 sr solid-angle 384 detector array, integrated scanning and real-time processing including spectral deconvolution of full-spectral data. Results using a Maia prototype demonstrate the potential using SXRF application data with elemental images of up 100 M pixels.     

Nanosecond pulsed proton microbeam

We show the preparation of a pulsed 20 MeV proton beam at the Munich tandem accelerator which offers a fluence of more than 1 × 10⁹ protons/cm² being deposited in a beam spot smaller than 100 μm in diameter and within a time span of 0.9 ns fwhm. Such a beam is produced by an ECR type proton source using charge exchange in cesium vapor to obtain a beam of negative hydrogen of high brightness that is bunched, chopped, accelerated and then focused by the superconducting multipole lens of the microprobe SNAKE. Single beam pulses are generated in order to irradiate cell samples or tissue and to measure their biological effect in comparison to continuous proton or X-ray irradiation.     

Mapping of ion beam induced current changes in FinFETs

We report on progress in ion placement into silicon devices with scanning probe alignment. The device is imaged with a scanning force microscope (SFM) and an aligned argon beam (20 keV, 36 keV) is scanned over the transistor surface. Holes in the lever of the SFM tip collimate the argon beam to sizes of 1.6 μm and 100 nm in diameter. Ion impacts upset the channel current due to formation of positive charges in the oxide areas. The induced changes in the source–drain current are recorded in dependence of the ion beam position with respect to the FinFET. Maps of local areas responding to the ion beam are obtained.     

Applications to cultural heritage diagnostics at the new nuclear microprobe beam line at CEDAD

A nuclear microprobe beam line has been installed at CEDAD (Centre for Dating and Diagnostics), University of Salento, Lecce, Italy. The beam line is connected to the ?30° port of the high energy switching magnet of a 3 MV HVEE 4130HC Tandetron accelerator. It is based on an Oxford Microbeam magnetic quadrupole triplet and its general features are presented. The results of functional tests are presented showing how a lateral spatial resolution as low as ～2 μm has been achieved in vacuum by analysing standard reference material. The results obtained in the analysis of ancient radiocarbon dated biological tissues are presented for the identification and distribution of toxic elements such as Pb.     

Determination of the local gold contact morphology on a photoactive polymer film using nanobeam GISAXS

Grazing incidence small-angle X-ray scattering is performed with a nanometer sized X-ray beam (nGISAXS) to probe the local gold contact morphology on a photoactive polymer film. By evaporation a 50 nm thick gold contact is installed on a diblock copolymer film, which consists of a non-conducting poly(styrene) (PS) and a semi-conducting poly(paraphenylene) (PPP) block. The region around the edge of the gold contact of 200 μm is probed with nGISAXS by scanning the sample position in steps of 1 μm with respect to the X-ray beam. The diblock copolymer film has a densely packed micellar structure with a characteristic distance between adjacent micelles of 19 nm which is unaffected by the gold deposition. The gold contact exhibits a tail region which extends its lateral dimension. For the full extended surface area of the gold contact with its tails an interdiffusion of gold into the diblock copolymer film is observed. For comparison imaging ellipsometry, atomic force microscopy and optical microscopy measurements are performed.     

Commissioning of the first KSTAR neutral beam injection system and beam experiments

The neutral beam injection (NBI) system was designed to provide plasma heating and current drive for high performance and long pulse operation of the Korean Superconducting Tokamak Advanced Research (KSTAR) device using two co-current beam injection systems. Each neutral beam injection system was designed to inject three beams using three ion sources and each ion source has been designed to deliver more than 2.0 MW of deuterium neutral beam power for the 100-keV beam energy. Consequently, the final goal of the KSTAR NBI system aims to inject more than 12 MW of deuterium beam power with the two NBI for the long pulse operation of the KSTAR. As an initial step toward the long pulse (～300 s) KSTAR NBI system development, the first neutral beam injection system equipped with one ion source was constructed for the KSTAR 2010 campaign and successfully commissioned. During the KSTAR 2010 campaign, a MW-deuterium neutral beam was successfully injected to the KSTAR plasma with maximum beam energy of 90 keV and the L-H transition was observed with neutral beam heating. In recent 2011 campaign, the beam power of 1.5 MW is injected with the beam energy of 95 keV. With the beam injection, the ion and electron temperatures increased significantly, and increase of the toroidal rotation speed of the plasma was observed as well. This paper describes the design, construction, commissioning results of the first NBI system leading the successful heating experiments carried in the KSTAR 2010 and 2011 campaign and the trial of 300-s long pulse beam extraction.     

Design of a beam dump for the IFMIF-EVEDA accelerator

The IFMIF-EVEDA accelerator will be a 9 MeV, 125 mA cw deuteron accelerator prototype for verifying the validity of the accelerator design for IFMIF. A beam stop will be used for the RFQ and DTL commissioning as well as for the EVEDA accelerator tests. Therefore, this component must be designed to stop 5 MeV and 9 MeV deuteron beams with a maximum power of 1.13 MW.The first step of the design is the beam-facing material selection. The criteria used for this selection are low neutron production, low activation and good thermomechanical behavior. In this paper, the mechanical analysis and radioprotection calculations that have led to the choice of the main beam dump parameters will be described.The present design is based on a conical beam stop (2.5 m length, 30 cm diameter, and 3.5 mm thickness) made of copper plus a cylindrical 0.5 m long beam scraper. The cooling system is based on an axial high velocity flow of water. This design is compliant with the mechanical design rules during full power stationary operation of the accelerator. The radioprotection calculations performed demonstrate that, with an adequate local shielding, doses during beam on/off phases are below the limits.     

Design of neutral beam injection system for KSTAR tokamak

The neutral beam injection (NBI-1) system has been designed for providing a 300 s deuterium beam of 120 kV/65 A as an auxiliary heating and current drive system of the KSTAR (Korea Superconducting Tokamak Advanced Research) tokamak. The deuterium beam is produced from a long pulse ion source composed of a bucket-type plasma generator and a multi-aperture tetrode accelerator with the help of discharge power supplies and high voltage (HV) power supplies. The beamline components (BLCs) include a neutralizer with an optical multi-channel analyzer (OMA) section, a bending magnet (BM), an ion dump assembly, a movable calorimeter, beam scrapers, and a cryo-sorption pump system in a rectangular vacuum tank. A beam duct equipped with bellows and a voltage break is placed between the NBI vacuum tank and the KSTAR vacuum vessel. All data and parameters of the NBI system are controlled by a control and data acquisition (CODAQ) system through the EPICS based Ethernet interface.     

Negative ion beam extraction in ROBIN

The RF based single driver ?ve ion source experiment test bed ROBIN (Replica Of BATMAN like source in INDIA) has been set up at Institute for Plasma Research (IPR), India in a technical collaboration with IPP, Garching, Germany. A hydrogen plasma of density 5 × 10¹² cm^?3 is expected in driver region of ROBIN by launching 100 kW RF power into the driver by 1 MHz RF generator. The cesiated source is expected to deliver a hydrogen negative ion beam of 10 A at 35 kV with a current density of 35 mA/cm² as observed in BATMAN.In first phase operation of the ROBIN ion source, a hydrogen plasma has been successfully generated (without extraction system) by coupling 80 kW RF input power through a matching network with high power factor (cos θ > 0.8) and different plasma parameters have been measured using Langmuir probes and emission spectroscopy. The plasma density of 2.5 × 10¹¹ cm^?3 has been measured in the extraction region of ROBIN. For negative hydrogen ion beam extraction in second phase operation, extraction system has been assembled and installed with ion source on the vacuum vessel. The source shall be first operated in volume mode for negative ion beam extraction. The commissioning of the source with high voltage power supply has been initiated.     

Safety managements of the linear IFMIF/EVEDA prototype accelerator

On the Linear IFMIF/EVEDA Prototype Accelerator (LIPAc), the validation up to 9 MeV deuteron beam with 125 mA continuous wave is planned in Rokkasho, Aomori, Japan. Since the deuteron beam power exceeds 1 MW, safety issue related to γ-ray and neutron production is critical. To establish the safety management indispensable to reduce radiation exposure for personnel and activation of accelerator equipment, Personnel Protection System (PPS) of LIPAc control system, which works together with Radiation Monitoring System and Access Control System, was developed for LIPAc. The management of access to the accelerator vault by PPS and the beam duty management of PPS are presented in details.     

Electron beam emission and interaction of double-beam gyrotron

This paper presents the numerical simulation of a double-beam magnetron injection gun (DB-MIG) and beam-wave interaction for 60 GHz, 500 kW gyrotron. The beam-wave interaction calculations, power and frequency growth estimation are performed by using PIC code MAGIC. The maximum output power of 510 kW at 41.5% efficiency, beam currents of 6 A and 12 A, electron beam velocity ratios of 1.41 and 1.25 and beam voltage of 69 kV are estimated. To obtain the design parameters, the DB-MIG with maximum transverse velocity spread less than 5% is designed. The computer simulations are performed by using the commercially available code EGUN and the in-house developed code MIGANS. The simulated results of DB-MIG design obtained by using the EGUN code are also validated with another trajectory code TRAK, which are in good agreement.     

Progress in development and design of the neutral beam injector for JT-60SA

Neutral beam (NB) injectors for JT-60 Super Advanced (JT-60SA) have been designed and developed. Twelve positive-ion-based and one negative-ion-based NB injectors are allocated to inject 30 MW D⁰ beams in total for 100 s. Each of the positive-ion-based NB injector is designed to inject 1.7 MW for 100 s at 85 keV. A part of the power supplies and magnetic shield utilized on JT-60U are upgraded and reused on JT-60SA. To realize the negative-ion-based NB injector for JT-60SA where the injection of 500 keV, 10 MW D⁰ beams for 100 s is required, R&Ds of the negative ion source have been carried out. High-energy negative ion beams of 490–500 keV have been successfully produced at a beam current of 1–2.8 A through 20% of the total ion extraction area, by improving voltage holding capability of the ion source. This is the first demonstration of a high-current negative ion acceleration of >1 A to 500 keV. The design of the power supplies and the beamline is also in progress. The procurement of the acceleration power supply starts in 2010.     

External scanning micro-PIXE for the characterization of a polycapillary lens: Measurement of the collected X-ray intensity distribution

We developed a PIXE detection system for the analysis of medium-light elements which exploits a weakly focusing polycapillary lens for the transmission of the X-rays emitted from the target material to a Silicon Drift Detector. The polycapillary lens efficiently collects X-rays, while prevents back-scattered protons from impinging on the detector chip, thus avoiding electronics perturbation and consequent quality loss of PIXE spectra. The system is optimized for the detection of X-rays in the energy range 1–10 keV, when the emission from the target is induced by MeV proton beams with size of the order of a few hundreds of micrometers.This work reports the results of the lens characterization in terms of X-ray collection spot, i.e. the area of the sample actually “seen” by the lens, and its dependence on the X-ray energy. The lens properties have been measured using the external scanning microbeam facility of the Tandetron accelerator at LABEC-INFN in Florence. The detection system was used to detect X-rays from a set of pure elemental standards with an incident 3 MeV proton beam focused to a size of about 30 μm scanning an area of 1.9 × 1.6 mm². By measuring the spatial distribution of characteristic X-rays from each given material, the collection profile of the lens at the corresponding X-ray energy was obtained. Using several standards, the behaviour throughout the range 1–10 keV was examined. The sensitivity of the lens collection profile on the lens-sample out-of-focus distance was also investigated.     

Time Resolved Ion Beam Induced Current measurements on MOS capacitors using a cyclotron microbeam

As overlayers on electronic devices become progressively thicker, radiation effects microscopy using traditional microbeams (with ion energies up to a few tens of MeVs) is becoming less and less viable. To penetrate to the sensitive regions of these devices, much higher energies, several hundreds of MeVs are necessary. These high energies are available only from cyclotrons. A nuclear microprobe has been developed on the AVF cyclotron of the Takasaki Ion Accelerators for Advanced Radiation Applications (TIARA) facility. In this paper we will present the first results using 260 MeV Ne and 520 MeV Ar microbeams to perform Time Resolved Ion Beam Induced Current (TRIBIC) measurements on Metal-Oxide-Semiconductor (MOS) capacitors. The results will be compared to data taken with a traditional 15 MeV O microbeam.     

Corrosion of Fe9Cr1Mo steel in stagnant liquid lead–lithium eutectic

The corrosion behaviour of Fe9Cr1Mo steel samples in a static Pb₈₃Li₁₇ eutectic melt at 823 K in a specially designed necked quartz capsule is investigated. The samples are kept isothermally for 500, 1000, 1500 and 2000 h. The changes in microstructure and depletion of alloying components of the sample kept for 2000 h have been studied using scanning electron microscope (SEM), energy disperses X-rays (EDS) and electron probe beam microanalysis (EPMA). Weight loss and thinning of the walls has been calculated by gravimetric analysis method for all the samples. Using this data the change in thickness per year is calculated. Preferential dissolution of major constituent elements namely iron and chromium from the samples with the formation of a ferritic–martenstic layer is observed. Percentage mass loss with respect to time follows a parabolic curve which indicates non linear mechanism of corrosion.     

Mechanical design for modification of a neutral beam for off-axis injection

DIII-D is planning to implement off-axis neutral beam current drive by neutral beam injection through a midplane port at angles up to 15° from horizontal. To accommodate the beam-line tilting, the following modifications are planned: (1) move the beam line away from the tokamak by 0.39 m to allow for a 0.68 m inside diameter welded bellows of necessary length to provide 15° of vertical motion between the vessel port and the beam line; (2) reduce the vertical height of the injected beam from 0.48 m to 0.43 m to provide clearance for the inclined beam as it passes through the length of the vessel port; (3) add a linkage system between the front of the beam line and the tokamak to restrain the NB against the vacuum loading from the bellows while maintaining zero roll about the axis of the beam line as it is moved about a virtual pivot axis; (4) add a forward and two rear vertical actuators for raising and lowering the beam line (These actuators require coordinated position control to rotate the NB about a virtual pivot axis.); (5) incorporate lateral restraint to comply with seismic requirements.     

Recent status of the Kiev nuclear probe

The modified Van de Graaff accelerator with proton beam energy W ? 3 MeV has been installed and put into operation at the TMM laboratory in Kiev. The laboratory incorporates the nuclear probe (NP) beam line, coupled to this accelerator. A short version of an optimized probe-forming system (PFS) has been developed for the Kiev NP. The system is based on divided triplet of the magnetic quadrupole lenses (MQLs). This PFS has two working regimes for the probe operations. The results of numerical calculations of the geometrical and ion-optical parameters of the PFS are presented. It is shown that this versatile PFS is a promising design for a modern nuclear nano-probe. A new precision adjustable MQL has been designed. Three lenses, the slit systems and target chamber are manufactured and installed at the Kiev probe beam line. Also a new data acquisition system for the Kiev NP is being developed.     

A bulk tungsten tile for JET: Heat flux tests in the MARION facility on the power-handling performance and validation of the thermal model

In the frame of the ITER-like Wall (ILW) for the JET tokamak, a divertor row made of bulk tungsten material has been developed for the position where the outer strike point is located in most of the foreseen plasma configurations. In the absence of active cooling, this represents a formidable challenge when one considers the temperature reached by tungsten (T_W,surf > 2000 °C) and the vertical gradient ?T/?z = 5 × 10⁴ K/m.As the development is drawing to an end and most components are in production, actual 1:1 prototypes are exposed to an ion beam with a power density around 7 MW/m² on the plasma-facing surface. Advantage is taken of the flexibility of the Marion facility to bombard the tungsten stack under shallow angles of incidence (～6°) with a powerful beam of ions and neutrals (>70 MW/m² on axis). The shallow angles are important, with respect to the toroidal wetted surface, for properly simulating the expected performance under actual tokamak conditions. The Marion tests have been used to validate for a few typical cases the thermal calculations that were steadily developed along with the tungsten tile and, at the same time, to gather information on the actual temperatures of individual components. The latter is an important factor to a finer estimation of the power handling capabilities.     

Manufacturing prototypes for LIPAC beam dump

The purpose of the research is to define the most adequate manufacturing process for the dump of a linear deuteron accelerator. The deuteron beam can be pulsed as well as continuous with energies up to 9 MeV. The maximum beam power is 1.12 MW corresponding to a beam current of 125 mA.The requirements on the surface on which the deuterons will be stopped are quite demanding and the length and slenderness of the cone poses a considerable difficulty in the manufacturing process.The design of the beam dump is based on a copper cone 2500 mm long, 300 mm aperture and 5 to 6.5 mm thickness.Basically only two technologies were found feasible for the manufacturing of the cone: Electroforming and Electron Beam Welding (EBW).The article shows the main results found when manufacturing different prototypes.     

Design and analysis of the IFMIF–EVEDA beam dump cooling system

The IFMIF–EVEDA beam dump is designed to stop a 9 MeV, 125 mA continuous wave deuteron beam that deposits along its surface a total of 1.125 MW. The beam dump design is based on a 2.5 m long copper cone whose inner surface absorbs the beam. This piece is cooled by water flowing at high velocity through the annular channel formed between it and a second piece (shroud) made of four truncated cones of slightly different slopes.In this paper the beam dump cooling system will be briefly described, and the relevant 1D and 3D results will be presented paying especial attention to the computational fluid dynamics results.