共查询到20条相似文献,搜索用时 0 毫秒
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A high electron-density embedding medium was developed for SEM observation of inorganic constituents of organic or carbonaceous particles. The components used are a common epoxy resin in which iodoform is dissolved before the addition of the hardener. An iodoform content of 10% by weight proved satisfactory for obtaining excellent contrast between the matrix and embedded carbonaceous particles in the SEM. The system has been successfully applied in the preparation of polished specimens of coal particles. There is no interference between the iodine and any of the most abundant or most important coal mineral components, but it was found that the epoxy resin contained chlorine as a contaminant. 相似文献
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Geometric error calibration of multi-axis machines using an auto-alignment laser interferometer 总被引:6,自引:0,他引:6
This work will report the development and application of an auto-alignment laser interferometer system for the geometric error calibration of CNC multi-axis machines. The system is capable of a diagonal displacement measurement, where multiple machine axes are moved simultaneously, with automatic optic alignment. This capability provides a solution for quick evaluation of the overall volumetric error of a multi-axis machine tool. One application of the system is that the 21 geometric errors of a 3-axis machine can be quickly estimated from the displacement measurements of some determined diagonal lines in the working volume. Compared with a time of several days using a conventional laser interferometer system, it takes only 1 hour for the proposed system to complete the geometry calibration of a 3-axis machine. A method for the roll calibration of a vertical axis is also proposed and demonstrated in this work. 相似文献
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W. Senior 《Journal of microscopy》1970,91(3):207-210
The use of a commercially available polyester resin is described for the production of whole-mount preparations and as a mounting medium for histological sections. Any standard technique can be used which involves xylene as the clearing agent. It is considered that the slides produced are much stronger than those made with traditional mounting media and do not require long drying times before use. The method is particularly suitable for mounting thick specimens for teaching purposes. 相似文献
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Neefs E De Mazière M Scolas F Hermans C Hawat T 《The Review of scientific instruments》2007,78(3):035109
In order to make long-term monitoring of the atmospheric composition using commercial Bruker Fourier transform spectrometers more cost effective, a system called BARCOS has been developed. The system enables one to perform the operation of the spectrometric atmospheric observations in a remotely controlled or autonomous way, without human presence at the measuring site. Several observation geometries are foreseen, including solar and lunar absorption spectrometry. BARCOS is built using existing commercial hardware and software components, including the Bruker software for the operation of the spectrometer (OPUS) and runs in a personal computer (Microsoft) environment. It includes a small meteorological station. It is a flexible system, allowing manual interventions at any time. To run BARCOS effectively, the only prerequisite is that internet access is available at the site of operation. This article describes the BARCOS system hardware and software configurations. 相似文献
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We present a volumetric interferometer that has been specially designed to improve the measurement accuracy of the three-dimensional coordinate metrology by reducing excessive Abbe offsets. The interferometer is composed of two main parts; one is a three-dimensionally movable target and the other is a stationary two-dimensional array of photo-detectors. The target made of point diffraction sources emanates two spherical wavefronts, of which interference intensity is monitored by the photo-detectors. Applying phase shifting allows the phases of the photo-detectors to be precisely obtained, and the measured phases are fitted to a geometric model of multilateration so as to determine the xyz-location of the target by minimizing least square errors. A prototype built on a CMM demonstrates that the proposed interferometer is capable of measuring the xyz-coordinates of the probe with a volumetric uncertainty of less than 1.0 μm. 相似文献
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This report describes an interferometer recently developed and tested in prototype form. The device combines certain features of predecessor interometers but in a module which, subject to limitations on path-length and bandwidth, is simpler to use. 相似文献
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I. G. Palchikova V. I. Kovalevskii V. V. Shelkovnikov 《Optoelectronics, Instrumentation and Data Processing》2007,43(3):256-261
An experimental assembly is created and a method for simultaneous studying dynamics of phototransformation of holographic photopolymer materials by spectrophotometric and interferometric methods is elaborated. A special diffraction interferometer with combined branches is developed. The interferometer ensures the sensitivity to the change in the refractive index Δn ~ 10?3 for ~100 μm specimens. 相似文献
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The scheme and the main elements of an interferometer simultaneously operating at frequencies of the 8-and 4-mm ranges are presented. To combin e two radiations in a common waveguide section and separate them by sending to the corresponding receivers, a special separation filter has been developed. A homo-dyne technique for transferring phase measurements to an intermediate frequency is employed in the interferometer. The range of unambiguously measured phase shifts is 1.5°—360°, and the phase-shift measurement error is within 5%. 相似文献
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A polarized light interferometer, suitable for the high-speed photography of microscopic objects in laser fusion experiments, is described. Based on a Wollaston prism as beam splitter, its main advantages are its relative simplicity, the absence of alignment and stability problems, and the extended spectral range down to 0.18 mum wavelength. The interferometer has been successfully applied in CO(2) and neodymium laser plasma interaction studies with laser illumination at 0.694 mum (ruby laser) and 0.265 mum (4th harmonic of the Nd(3+) laser) wavelength. 相似文献
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The nonlinear errors of high-precision linear encoders were calibrated by using a nanometer-length calibrator that was based on the optical-zooming laser interferometer with an optical frequency comb. A transmission-type linear encoder and a reflection-type linear encoder were calibrated, and the cyclic nonlinear errors were evident. The magnitudes of the observed cyclic errors were 0.1 nm and 0.2 nm, respectively, and the best calibration uncertainties were 0.55 nm (k = 2). A traceable calibration service for linear encoders with the best calibration uncertainty in the sub-nanometer range has started based on this work. 相似文献
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We report a simple scheme for stabilizing and tuning the length of a conventional piezo-driven optical cavity against the resonant transmission of a master laser. In contrast with other schemes, we drive the piezo at its mechanical resonance of 5 kHz over an amplitude equivalent to one free spectral range and use a feedback circuit that incorporates phase-sensitive detection of the master-laser transmission. The bandwidth of our cavity-lock circuit is limited only by the resonance frequency of the cavity piezo and is 1.4 kHz. The stabilized mean cavity length reaches in 30 s a minimum Allan deviation of approximately 10 kHz (a length stability of 20 parts per trillion) equaling that of the polarization-stabilized He-Ne we use as our master laser. Here, we investigate the mechanical characteristics of the cavity, describe the lock circuit and its measured performance, and provide simple analytical relations between the phase-sensitive signal and cavity displacement. Our setup economizes the cost and amount of equipment necessary for stabilizing multiple continuous-wave lasers operating at different wavelengths. 相似文献
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Differential heterodyne interferometer is applied for measuring spatial thickness variations across glass panels of liquid-crystal displays. This system uses the Zeeman laser as a source of two-frequency shifted orthogonally linearly polarized probe waves, passing through the glass in two spatially separated points. These waves are then recombined in a single beam to produce the intermediate frequency signal with the phase proportional to the thickness gradient of a glass sample. The phase of the intermediate signal is measured against the laser reference by means of a lock-in amplifier, and finally real-time integration provides the thickness variation. Since spatial separation of the probe beams is only 1.35 mm good approximation for the thickness gradient is achieved. Detailed design of the interferometer and experimental results on real samples are presented. 相似文献
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D. A. Nagornyi A. G. Nagornyi V. I. Voznyi 《Instruments and Experimental Techniques》2005,48(2):225-227
An interferometer for a wavelength of 8 mm, capable of homodyne frequency conversion for measuring the electron density of a steady-state plasma from a high-frequency ion source, is described. An original method for generating a reference intermediate-frequency signal using a cavity resonator is applied in the interferometer. The unambiguously measured phase shifts range from 1.5° to 360°, and the error in measuring the phase shift is 5%.__________Translated from Pribory i Tekhnika Eksperimenta, No. 2, 2005, pp. 98–100.Original Russian Text Copyright © 2005 by D. Nagornyi, A. Nagornyi, Voznyi. 相似文献