稀土Y对AZ61镁合金微观组织和力学性能的影响

研究了稀土钇含量对AZ61镁合金显微组织和室温及高温力学性能的影响。实验结果表明：加入稀土钇可使AZ61合金铸态组织中的β相数量减少、铸态晶粒细化;大部分钇与铝结合生成高熔点、高热稳定性的稀土相A12Y3;固溶处理后,β相完全溶解而稀土相则以块状或杆状存在于晶界周围;适量的稀土钇可以提高AZ61合金的室温及高温强度、硬度和延伸率;而过量的稀土钇则会导致AZ61合金的性能下降;稀土钇的含量为1．0％时合金可得到较佳的力学性能。     

热处理对AZ61A镁合金显微组织及力学性能的影响

采用光学显微镜(OM)、场发射扫描电镜(FESEM)、X射线衍射(XRD)及拉伸试验等研究了热处理对铸态AZ61A镁合金显微组织及力学性能的影响.结果表明,分布在铸态AZ61A镁合金晶界的粗大网状β-Mg17Al12相在T4热处理过程中几乎全部溶解,使合金的硬度和屈服强度下降,而抗拉强度和伸长率升高;T6热处理后,合金组织中出现不连续析出与连续析出的β-Mg17Al12相,使得合金的抗拉强度、屈服强度略有提高,硬度有明显提高,而伸长率明显降低;不同的热处理使合金的断口形貌发生明显变化.     

稀土铈对AZ61镁合金显微组织和力学性能的影响

在AZ61合金中添加0％、0.5％、1％和1.5％(质量分数)的铈(Ce)制备了4种合金,研究了Ce含量和合金变形状态对其力学性能和显微组织的影响.实验表明,添加Ce元素后,形成的Al4Ce对合金有强化作用,但其铸态组织仍然粗大,需要经过轧制及退火,合金组织才能得到改善.力学性能测试结果表明,随Ce含量的增加,轧制态合金强度上升,伸长率有所提高.300℃退火1h后,强度比轧制态有所降低,但伸长率提高较大.含1.0％Ce的3#合金具有最好的综合力学性能,挤压+轧制加工态其抗拉强度、屈服强度和伸率长分别为350 MPa、274MPa和6.2％；300℃×lh退火后,分别为306 MPa、201MPa和18.7％.     

稀土对AZ61镁合金组织及室温力学性能的影响

以AZ61镁合金为基础合金,研究了镁合金中不同稀土含量对其组织及室温力学性能的影响,并通过SEM对断口形貌的观察分析了稀土对合金断裂机制的影响。结果表明：加入1%-4％的稀土后,铸态AZ61合金组织中的母相明显变少,形成粗大针状或者棒状甚至块状AhCe或Al3Nd稀土相,造成合金成分的不均匀,使晶界脆化,同时在拉伸过程中易在粗大稀土相的尖角处形成应力集中,降低了镁合金室温力学性能;另外,由于稀土含量偏高,AZ6l合金中β-Mg177Al12相由连续网状、块状变为断续的网状或粒状,分布在合金基体中,同时沿晶界或晶内分布的粗大或团簇的Al4Ce或Al3Nd强化相,造成一定的品格畸变,阻碍位错的运动,使含稀土合金的室温力学性能有所提高,但仍低于AZ61合金的力学性能;通过SEM对断口观察发现所有试验合金的断裂方式均为解理断裂。     

Sn对AZ61镁合金组织和力学性能的影响

通过合金制备、微观分析和力学性能测试等方法研究了Sn对AZ61镁合金微观组织和力学性能的影响.结果表明,当加入Sn后,在铸态及热处理态合金中均发现了球形颗粒状的Mg2Sn相;0.5%的Sn可以明显提高合金在20℃、150℃、175℃的抗拉强度.合金力学性能的提高一方面是固溶强化,另一方面是高熔点的Mg2Sn相的弥散强化.     

钕对AZ61镁合金铸态显微组织和力学性能的影响

主要研究了Nd对AZ61合金铸态组织和力学性能的影响。研究结果表明Nd元素对AZ61镁合金有明显的细化作用,当加入1．0％Nd时,细化效果最为显著,而且有最佳的力学性能。经分析,Nd与合金中的镁铝元素形成热稳定性较高的金属间化合物,在α-Mg晶粒内和晶界均有分布。     

稀土元素对AZ31镁合金组织和力学性能的影响

向AZ31镁合金中添加稀土Ce和复合添加Ce与Sb,测试和分析了合金的力学性能和组织。研究表明:合金相组成主要为α-Mg、CeSb以及Mg_(17)Al_(12);复合添加Ce和Sb可细化晶粒和有助于形成CeSb第二相,从而有效提高AZ31镁合金的力学性能。当Ce为1.5%,Sb为1.5%时,铸态合金室温抗拉强度为201.4 MPa,伸长率为12.6%,冲击韧度值为8.1 J·cm~(-2);经385℃热挤压成型后,合金室温抗拉强度为325.6 MPa,伸长率为22.3%,冲击韧度值为15.8 J·cm~(-2)。     

稀土铈对AZ61变形镁合金组织和力学性能的影响

研究了不同稀土铈含量对AZ61合金显微组织和力学性能的影响.实验发现:加入稀土铈后,AZ61合金铸态组织的β相变少、变细,铸态晶粒细化;大部分铈与铝结合生成高熔点、高热稳定性的稀土相Al4Ce;在热挤压和退火过程中,Al4Ce能够阻碍晶粒或亚晶粒的长大,使晶粒细化.适量的稀土铈提高了挤压态合金的强度、延伸率和显微硬度;而过量的稀土铈则会导致AZ61合金的性能下降;含1.0%稀土铈的挤压态合金可得到最高的抗拉强度308.1MPa、最高屈服强度180.1MPa、最大的显微硬度HV80.5和最高的延伸率14.2%;所有试验合金的断裂方式是解理断裂.     

La对AZ61镁合金组织及性能的影响

研究添加稀土La含量为(0,0.5,1.0,1.5)％对AZ61合金的微观组织及室温力学性能的影响.结果表明:加入0.5％ ～1.5％的稀土后,铸态AZ61合金组织中的β-Mg17Al12相明显变得细小,形成了针状的Al11La3相.当稀土含量超过1.0％时,针状的Al11 La3相开始粗化长大,β-Mg17 Al12相的网状结构开始分离,变得细小;La的加入可以提高AZ61合金力学性能,当加入的La含量为1.0％时,AZ61合金的力学性能最好.因此,AZ61合金中加入La的质量分数为1.0％时,为合金化的最佳值.     

CaC2对电磁-悬浮铸造AZ61合金组织和力学性能的影响

利用电磁搅拌技术,结合悬浮铸造方法,在浇铸AZ61镁合金的过程中加入微纳米颗粒CaC2,使CaC2弥散分布于母相金属液中,促进合金形核,改善合金铸造组织形态和分布,提高合金的力学性能.结果表明:利用电磁一悬浮铸造制备的镁合金,其显微组织细化,晶间β相细小并且网状结构减少,当CaC2悬浮剂加入量(质量分数)为0.36%时,镁合金的细化效果最佳,其晶粒最小尺寸为75 μm,抗拉强度为211.4 Pa,伸长率为8.5%,与普通金属型铸造制备的镁合金相比,晶粒尺寸减小64.3%;抗拉强度提高约24.2%;伸长率提高46.6%.     

Effect of yttrium on microstructures and mechanical properties of hot rolled AZ61 wrought magnesium alloy

1 Introduction Magnesium alloys are attractive materials due to their good specific properties such as low density, good damping characteristics, good thermal conductivity and high elastic modulus[1,2]. Recently, there has been significant increase in the…     

Effects of Ce addition on microstructure,mechanical properties and corrosion resistance of as-cast AZ80 magnesium alloy

In this study, Ce was introduced into the AZ80 alloy and the effects of Ce addition on the microstructure, mechanical properties and corrosion resistance of the as-cast AZ80 magnesium alloy were investigated. The results show that the addition of Ce into the AZ80 alloy can not only refine the microstructure, but also result in the formation of the needle-like Al4Ce phase. These tiny Al4Ce phases are homogeneously distributed at grain boundaries and within grains. An appropriate Ce addition can also change the β-Mg17Al12 phase at the grain boundaries from continuous network to small island-like. At the same time, with the increase of Ce content from 0 to 2.0wt.%, the macro-hardness of the as-cast alloy is enhanced linearly, while impact toughness, tensile strength and elongation all firstly increase and then decrease. The AZ80 alloy containing 1.0wt.% Ce exhibits the optimal properties. Its macro-hardness, impact toughness, tensile strength and elongation are 61.90 HB, 15.50 J·cm^-2, 171.80 MPa and 3.35%, increase by 9.95%, 63%, 13.3% and 36.7%, respectively compared with the base alloy. In addition, Ce can enhance the corrosion resistance of the AZ80 magnesium alloy.     

Effect of La and Nd on microstructures and mechanical properties of AZ61 wrought magnesium alloy

Effects of La and Nd addition on the microstructure and mechanical properties of the AZ61 alloy have been investigated. The results show that when La and Nd are added into the AZ61 alloy respectively, the β(Mg17-Al12) phase is refined and granulated, and new phases are formed in the form of small rod-like shape, which are verified as La3 Al12 and Nd3Al11 phase by X-ray diffraction and TEM observation. Microstructure observations show that the effective efficiency of La addition is higher than that of Nd addition, thus the sizes of β(Mg17 Al12) and La3Al11 phase are relatively smaller than those of β(Mg17 Al12 ) and Nd3 Al11 phases in both AZ61 alloy and Nd-containing alloy. The increase of the tensile strength and elongation of AZ61 alloy refers to the existence of small rod-like La3Al11 and Nd3Al11 phases, and fine granulated β(Mg17 Al12 ) phase.     

轴向力对搅拌摩擦焊接AZ61A镁合金拉伸性能的影响(英文)

研究轴向力对搅拌摩擦焊接AZ61A镁合金拉伸性能的影响。在3～7kN范围内选择5个不同大小的轴向力制备接头。测试接头的拉伸性能,并研究其与搅拌区显微组织和硬度的相关性。结果表明,与其他轴向力下的接头相比,轴向力为5kN时制备的接头具有最好的拉伸性能。搅拌区生成的细晶组织和高硬度是获得高拉伸强度的主要原因。     

离心压力对AZ31镁合金的组织和力学性能的影响

通过XRD、压缩试验等方法研究了不同离心压力对AZ31镁合金组织演变和力学性能的影响。结果表明,随着离心压力的增大,离心铸造AZ31镁合金的晶粒明显细化,平衡凝固的共晶转变被抑制,第二相β-Mg17Al12析出量减少,由粗大的“骨骼”状分布转变成弥散分布在晶界,形成以过饱和初生相ɑ-Mg为主相的凝固组织。XRD分析表明,离心压力的增大引起X射线衍射峰向高角度方向偏移,α-Mg的晶格常数减小。随着离心压力的增大,合金力学性能得到明显改善,抗压强度从199 MPa提高到256 MPa,而伸长率变化不明显。     

YAG脉冲激光焊接AZ61镁合金薄板对接接头的组织与性能

采用YAG脉冲激光焊方法对AZ61镁合金薄板进行焊接．利用光学显微镜、x射线能谱分析仪等手段分析焊接接头的宏观形貌、显微组织和化学成分,并对焊接接头的显微硬度和拉伸强度进行了测试．结果表明,焊缝正面有轻微塌陷,反面成形良好．焊缝表面圆滑、连续、鱼鳞纹细密均匀,接头成形良好．母材为粗大的等轴晶,焊缝区的晶粒比母材细小．焊缝区的显微硬度比母材区域明显提高,焊接接头的抗拉强度与母材相当,约为250MPa,焊接接头具有良好的力学性能;焊缝表面由于Mg元素的大量蒸发使铝的含量升高,而焊缝表面zn元素含量很低．     

Effect of Pr addition on microstructure and mechanical properties of AZ61 magnesium alloy

To improve the strength, hardness and heat resistance of Mg-6Al-1Zn(AZ61) alloy, the effects of Pr addition on the as-cast microstructure and mechanical properties of AZ61 alloy were investigated at room and elevated temperatures by means of Brinell hardness measurement, optical microscope(OM), scanning electron microscope(SEM), energy dispersive spectroscopy(EDS), X-ray diffractometer(XRD) and DNS100 electronic universal testing machine. The results show that the microstructures of Pr-containing AZ61 alloys were refined, with primary β-Mg17Al12 phase distributed homogeneously. When the addition of Pr is up to 1.2wt.%, the β phase becomes fi ner, and new needle-like or short-rod shaped Al11Pr3 phase and blocky AlPr phase appear. As a result, optimal tensile properties are obtained. However, greater than 1.2wt.% Pr addition leads to poorer mechanical properties due to the aggregation of the needle-like phase and large size of grains. The present research fi ndings provide a new way for strengthening of magnesium alloys at room and elevated temperatures, and a method of producing thermally-stable AZ61 magnesium alloy.