Structure, properties and fracture of friction stir welds in a high-temperature Al-8.5Fe-1.3V–1.7Si alloy (AA-8009)

Friction stir welds produced in a rapidly-solidified, powder metallurgy Al-8.5Fe-1.3 V-1.7 Si (wt.%) alloy were characterized in order to investigate the effects of deformation during welding on the weld zone microstructure, hardness, tensile properties, and fracture behavior. A weld produced using a tool rotational speed of 1200 rpm and a traversing rate of 4.3 mm/s exhibited a repetitive pattern of dispersoid-depleted bands that were attributed to the intense deformation that occurred in the vicinity of the tool. The significant softening associated with these regions, and the presence of occasional, irregularly-shaped voids near the boundary between the base metal and the weld zone on the advancing side of the weld, promoted a weld tensile strength of 60–70% of the base metal. The application of a lower tool rotational speed of 428 rpm and a lower traversing rate of 1.9 mm/s promoted fewer bands and a more uniform dispersoid distribution throughout the weld zone, and an absence of defects along the weld zone/base metal interface. Tensile strength of these welds approached 90% of the base metal. Fracture of the transverse-weld oriented tensile specimens for both weld types consistently occurred near the boundary between the weld zone and the base metal on the advancing side of the weld zone, with tensile specimen ductilities appreciably lower than that of the base metal.     

Effect of post-weld natural aging on mechanical and microstructural properties of friction stir welded 6063-T4 aluminium alloy

Influence of natural aging on mechanical and microstructural properties of friction stir welded 6063-T4 aluminium alloy plates was investigated through mechanical testing, X-ray diffraction studies, and transmission electron microscopy, for aging times up to 8640 h. Mg–Si co-clusters formed during the natural aging process resulted in an increase in strength, decrease in ductility, and occurrence of serrated plastic flow. Hardness increase from aging was fastest in welds obtained at higher tool rotational speeds due to greater amount of “quenched-in” vacancies from higher peak stir zone temperatures. Peak broadening analyses and classical Williamson–Hall plots were used to investigate the effect of friction stir welding and post weld natural aging on microstrain in different weld regions. Higher microstrain was found in stir zone as well as heat affected zone as compared to that for base metal, albeit for different reasons.     

R‐curve behaviour of friction stir welds in aluminium‐lithium alloy 2195

ABSTRACT The fracture resistance of friction stir welds in 2195‐T8 is described in this paper. R‐curves were produced for several crack planes, parallel to the welding direction and situated at varying distances from the weld centreline. The friction stir weld was also characterized by hardness and tensile testing. Fracture resistance of the friction stir weld is compared to the base metal and to a variable polarity plasma arc weld. Results show that the material in and around the friction stir weld is tougher than the base metal and the variable polarity plasma arc weld. The friction stir weld fracture performance is discussed in the light of the observed hardness and fractographic data presented.     

Thermal cycles and their effects during friction stir welding of AA7075 thicker plates with and without in-process cooling

Friction stir welding of AA 7075 plates in three different thicknesses such as 10, 16 and 25 mm at natural convection condition was carried out successfully without defects. Water cooled friction stir welds were also produced on 16 mm thick plates. The thermal cycles at different locations of the plate, during the friction stir welding process, were predicted using a three-dimensional thermal model. Mechanical properties of the welds were evaluated using tensile and hardness tests. Weld microstructures were also examined with optical and transmission electron microscopes. The weld hardness values and tensile properties were found to decrease with increase in plate thickness. The use of water cooling was found to improve the weld properties to some extent, although not to the level of base metal. The reasons for this behavior are discussed, correlating thermal cycles, mechanical properties, fracture locations and precipitate morphology.     

Influence of tool geometries and process variables on friction stir butt welding of Al–4.5%Cu/TiC in situ metal matrix composites

Present work describes friction stir welding of in-house produced and hot rolled Al–4.5%Cu/TiC in situ metal matrix composites by using hardened bimetallic tool with varying shoulder surface geometries and other process variables. Joining of the said composite using friction stir welding process has been seen to provide beneficial effects such as grain refinement of the matrix and subsequent redistribution and refinement of reinforcements. A predictive model has also been developed to estimate the weld properties such as tensile strength and ductility with respect to the tool geometry used and input process variables. The X-ray diffraction analysis results of Al–4.5%Cu/TiC butt welds indicated formation of CuAl₂O₄ and CuAl₂ to some extent in the stir zone. Fractography of the weld samples revealed dimpled ductile nature of fracture. Through multi response optimization of the welding parameters and tool geometry, weld strength of 89% that of the base material was achieved.     

Joint properties of friction stir welded AZ31B– H24 magnesium alloy

Abstract

The weldability of friction stir welded hot rolled AZ31B-H24 magnesium alloy sheet, 4 mm in thickness, was evaluated, varying welding parameters such as tool rotation speed and travel welding speed. Sound welding conditions depended mainly on sufficient heat input during the welding process. Insufficient heat input, which was generated in the case of higher travel speed and lower rotation speed, caused an inner void or lack of bonding in the stir zone. The microstructure of the weld zone was composed of five regions: base metal, heat affected zone, thermomechanically affected zone, stir zone I and stir zone II. Unlike the general feature of friction stir welded aluminium alloys, the grain size of the weld zone was larger than that of the base metal. Stir zones I and II were characterised by partial dynamic recrystallisation and full dynamic recrystallisation, respectively. The hardness of the weld zone was lower than that of the base metal owing to grain growth. A wider range of defect free welding conditions was acquired at higher tool rotation speed and lower welding speed. The maximum tensile strengh was 240 MPa, which was ~85% of the base metal value of 293 MPa. The fracture location was close to the stir zone.     

Electron microscopy of inertia-friction weldments in a rapidly solidified Al-Fe-Mo-V alloy

The microstructures of inertia-friction weldments in a rapidly solidified, powder metallurgy Al-8.7Fe-2.8Mo-1V alloy were characterized using light and transmission electron microscopy. Extensive plastic deformation at the weld interface during the welding process was shown to fracture and disperse relatively coarse, spherical dispersoids present in the original base-metal microstructure, thereby resulting in a refined dispersoid size in this region. These fine dispersoids promoted an increase in hardness at the weld interface as compared to the unaffected base metal. Local regions of nonuniform interface deformation at the weld outer periphery resulted in a heterogeneous microstructure comprised of adjacent regions of high and low dispersoid density. The dispersoid-lean regions were characterized by appreciably coarsened alpha grains and a hardness well below that of the base metal. The greater extent of dispersoid-lean regions in welds produced with low axial force promoted preferential weld interface failure during three-point bend testing, while the near absence of these regions in welds produced with high axial force promoted failure in the unaffected base metal remote from the weld.     

The potential adaptation of stationary shoulder friction stir welding technology to steel

Stationary shoulder friction stir welding is a newly developed technique currently used for joining plates of relatively soft metals at different angular planes. The process is not currently applicable to steel, hence the present study was developed to investigate the theoretical and technical viability of stationary shoulder technology in DH36 steel. Aluminium welds were produced using both conventional rotating shoulder and stationary shoulder friction stir welding techniques, and steel welds were produced using only conventional friction stir welding techniques. The effects of stationary shoulder technology on both the microstructural evolution and resultant mechanical properties of aluminium have been evaluated so that the likely effects on steel could be predicted. In the aluminium welds, the stationary shoulder technique results in a distinct transition between stirred and unstirred material, contrasting to the gradual change typically seen in conventional friction stir welds produced with a rotating shoulder. An investigation of weld properties produced in DH36 steel has demonstrated that if the stationary shoulder weld technique was used, the microstructure likely to be formed, would be dominated by a bainitic ferrite phase and so would exhibit hardness and tensile properties in excess of the parent material. It is predicted that if the same abrupt transition between unstirred and stirred material observed in aluminium occurred in steel, this would lead to crack initiation, followed by rapid propagation through the relatively brittle weld microstructure. Hence, these findings demonstrate that without further design and process improvements, stationary shoulder friction stir welding is unlikely to be applicable to steel.     

An assessment of microstructure,hardness, tensile and impact strength of friction stir welded ferritic stainless steel joints

Microstructure and mechanical characterization of friction stir welded 409M ferritic stainless steel joint were carried out. Single pass welds free of volumetric defects were produced at a welding speed of 50 mm/min and rotation speed of 1000 rpm. Optical microscopy, microhardness testing, transverse tensile, impact and bend tests were performed. The coarse ferrite grains in the base material are changed to very fine grains consisting duplex structure of ferrite and martensite due to the rapid cooling rate and high strain induced by severe plastic deformation caused by frictional stirring. Tensile testing indicates overmatching of the weld metal relative to the base metal. The joints are also exhibited acceptable ductility and impact toughness.     

Effect of welding speed on microstructural and mechanical properties of friction stir welded Inconel 600

In order to evaluate the properties of a friction stir welded Ni base alloy, Inconel 600 (single phase type) was selected. Sound friction stir welds without weld defect were obtained at 150 and 200 mm/min in welding speed, however, a groove like defect occurred at 250 mm/min. The electron back scattered diffraction (EBSD) method was used to analyze the grain boundary character distribution. As a result, dynamic recrystallization was observed at all conditions, and the grain refinement was achieved in the stir zone, and it was gradually accelerated from 19 μm in average grain size of the base material to 3.4 μm in the stir zone with increasing the welding speed. It also has an effect on the mechanical properties so that friction stir welded zone showed 20% higher microhardness and 10% higher tensile strength than those of base material.     

Microstructural characteristics and mechanical properties of friction stir welded joints of Ti–6Al–4V titanium alloy

The α + β titanium alloy, Ti–6Al–4V, was friction stir welded at a constant tool rotation speed of 400 rpm. Defect-free welds were successfully obtained with welding speeds ranging from 25 to 100 mm/min. The base material was mill annealed with an initial microstructure composed of elongated primary α and transformed β. A bimodal microstructure was developed in the stir zone during friction stir welding, while microstructure in the heat affected zone was almost not changed compared with that in the base material. An increase in welding speed increased the size of primary α in the stir zone. The weld exhibited lower hardness than the base material and the lowest hardness was found in the stir zone. Results of transverse tensile test indicated that all the joints had lower strength and elongation than the base material, and all the joints were fractured in the stir zone.     

Friction stir welding characteristics of different heat-treated-state 2219 aluminum alloy plates

Friction stir welding (FSW) of 2219-O and 2219-T6 aluminum alloys was performed to investigate the effects of the base material conditions on the FSW characteristics. The experimental results indicated that the base material condition has a significant effect on weld morphologies, weld defects, and mechanical properties of joints. In the 2219-O welds, no discernible interface exists between the stir zone (SZ) and the thermal-mechanically affected zone (TMAZ), and weld defects are liable to form in the lower part of the weld. In the 2219-T6 welds, there is visible interface between the SZ and the TMAZ, and a weld nugget with an “onion ring”-like morphology clearly exists. The defects are liable to form in the upper part of the weld. The strength efficiency of 2219-O joints is 100%, while that of 2219-T6 joints is only up to 82%. In addition, the two types of joints have different fracture location characteristics.     

Effects of microstructure and residual stress on fatigue crack growth of stainless steel narrow gap welds

The effects of weld microstructure and residual stress distribution on the fatigue crack growth rate of stainless steel narrow gap welds were investigated. Stainless steel pipes were joined by the automated narrow gap welding process typical to nuclear piping systems. The weld fusion zone showed cellular–dendritic structures with ferrite islands in an austenitic matrix. Residual stress analysis showed large tensile stress in the inner-weld region and compressive stress in the middle of the weld. Tensile properties and the fatigue crack growth rate were measured along and across the weld thickness direction. Tensile tests showed higher strength in the weld fusion zone and the heat affected zone compared to the base metal. Within the weld fusion zone, strength was greater in the inner weld than outer weld region. Fatigue crack growth rates were several times greater in the inner weld than the outer weld region. The spatial variation of the mechanical properties is discussed in view of weld microstructure, especially dendrite orientation, and in view of the residual stress variation within the weld fusion zone. It is thought that the higher crack growth rate in the inner-weld region could be related to the large tensile residual stress despite the tortuous fatigue crack growth path.     

Evaluation of the microstructure and mechanical properties of friction stir welded 6005 aluminum alloy

Abstract

The microstructural change related with the hardness profile has been evaluated for friction stir welded, age hardenable 6005 Al alloy. Frictional heat and plastic flow during friction stir welding created fine and equiaxed grains in the stir zone (SZ), and elongated and recovered grains in the thermomechanically affected zone (TMAZ). The heat affected zone (HAZ), identified only by the hardness result because there is no difference in grain structure compared to the base metal, was formed beside the weld zone. A softened region was formed near the weld zone during the friction stir welding process. The softened region was characterised by the dissolution and coarsening of the strengthening precipitate during friction stir welding. Sound joints in 6005 Al alloys were successfully formed under a wide range of friction stir welding conditions. The maximum tensile strength, obtained at 507 mm min^-1 welding speed and 1600 rev min^-1 tool rotation speed, was 220 MPa, which was 85% of the strength of the base metal.     

An outlook on comparison of hybrid welds of different root pass and filler pass of FCAW and GMAW with classical welds of similar root pass and filler pass

In the present study, gas metal arc welding and flux cored arc welding were applied on SA516 Gr70 carbon steel material. Two different hybrid passes were applied, wherein flux cored wire and solid wire were applied to root pass and filler pass one by one and vice versa. Besides, two more welds of similar electrode root pass and filler pass of flux cored arc welding and gas metal arc welding were acquired. The comparative analysis was carried out in terms of macrostructure and microstructure examination, tensile testing, hardness variations, and impact testing for these classical welds and hybrid welds. The results reveal that, hybrid welds lead to better impact properties relative to classical welds. Maximum angular distortion of 2.66° was reported with classical weld of gas metal arc welding with solid wire root pass and same filler pass. The maximum impact toughness of 49 J/m³ was reported for flux cored root pass and solid wire filler pass at the weld zone. Maximum tensile strength of 596 MPa was reported for hybrid weld of solid root pass and flux cored filler pass. Microstructures are reported with the presence of different acicular ferrite and grain boundary ferrite. Maximum acicular ferrite of 61% was reported with classical weld of flux cored arc welding.     

Fracture toughness and fatigue crack growth in Ti‐6Al‐4V friction stir welds

Friction stir welding of titanium holds the promise for producing joints with microstructures and mechanical properties that are more comparable to wrought material than traditional fusion welding processes. Extensive data exist on the microstructure and static mechanical properties of titanium friction stir welds, but very little are available on the durability (fatigue) and even less on the damage tolerance (fracture toughness and fatigue crack growth). This paper presents the results of an investigation into the damage tolerance of friction stir welds made in 6 mm thick Ti‐6Al‐4V after a post‐weld heat treatment. It was found that the apparent fracture toughness was lower than the wrought base material, 7–25% depending on the crack orientation relative to the weld, but the crack growth performance (ΔK vs. da/dN) of the weld in the absence of weld‐induced residual stresses was identical to the base material.     

Comparative experimental study on the modification of microstructural and mechanical properties of friction stir welded and gas metal arc welded EN AW‐6061 O aluminum alloys by post‐weld heat treatment

In this paper, the effects of post‐weld heat treatment on modification of microstructures and mechanical properties of friction stir welded and gas metal arc welded AA6061‐O plates were compared with each other. Gas metal arc welding and friction stir welding were used as the applicable welding processes for AA6061‐O alloys. The applied post‐weld heat treatment consisted of solution heat treatment, followed by water quenching and finally artificial aging. The samples were classified as post‐weld heat treated and as‐welded joints. The microstructural evolution, tensile properties, hardness features and fracture surfaces of both as‐welded and post‐weld heat treated samples were reported. The results clearly showed that friction stir welding process demonstrated better and more consistent mechanical properties by comparison with the gas metal arc welding process. The weld region of as‐welded samples exhibited a higher hardness value of 80 HV0.1 compared to the base material. In addition, the feasibility of post‐weld heat treatment in order to enhance the mechanical properties and to obtain more homogeneous microstructure of 6061‐O aluminum alloys was evaluated.     

Establishing relationship between the base metal properties and friction stir welding process parameters of cast aluminium alloys

In friction stir welding (FSW), the material under the rotating action of non-consumable tool has to be stirred properly to get defect free welds in turn it will improve the strength of the welded joints. The welding conditions and parameters are differing based on the mechanical properties of base materials such as tensile strength, ductility and hardness which control the plastic deformation during friction stir welding. The FSW process parameters such as tool rotation speed, welding speed and axial force, etc. play a major role in deciding the weld quality. FSW Joints of cast aluminium alloys A319, A356, and A413 were made by varying the FSW process parameters and the optimum values were obtained. In this investigation, empirical relationships are established and they can be effectively used to predict the optimum FSW process parameters to fabricate defect free joints with high tensile strength from the known base metal properties of cast aluminium alloys.     

Defect tolerance of friction stir welds in DH36 steel

Friction stir welding of steel is in the early stages of development. The aim to commercialise this process creates a trade-off between welding time, cost and quality of the joint produced. Therefore, it becomes critical to analyse the lower quality bound of steel friction stir welds in conventional square edge butt welding configuration. Work has been undertaken to evaluate the microstructure and fatigue performance of 6 mm thick DH36 steel plates friction stir welded with sub-optimal process conditions, resulting in the development of embedded and surface breaking flaws. The defective weldments were characterised to understand the nature of the flaws and a programme of mechanical testing was undertaken (including fatigue assessment) to determine the relationship between the flaw geometry, location and weld quality. A number of characteristic flaws were identified and seen to interact with the samples' fatigue fracture mechanisms. Samples with wormholes at the weld root produced the lowest fatigue performance. Fracture from incomplete fusion paths at the retreating side of the welds' top surface was seen to correspond to the highest recorded fatigue lives. The work provides an insight into the complex nature of characteristic flaws in steel friction stir welds and their interaction with fatigue behaviour.     

Correlation between precipitate microstructure and mechanical properties in AA7075‐T6 aluminum alloy friction stir welded joints

Microstructural evolution and mechanical properties of friction stir welded AA7075‐T6 aluminum alloy were examined. Grain structure and precipitate evolution in the stir zone and heat‐affected zone were evaluated using optical microscope and differential scanning calorimetry. A significant grain refinement and dissolution of η′ precipitates in the stir zone were found, but chromium‐bearing dispersoids remained nearly unchanged. The main particles in the stir zone and heat‐affected zone were η precipitates as well as Guinier‐Preston zones formed during post‐weld natural aging. The small recrystallized grains were observed in the thermo‐mechanically affected zone next to the stir zone. A W‐shaped hardness distribution where soft region was produced in the heat‐affected zone at a short distance from the stir zone were obtained. Hardness profiles of the welds were explained by precipitate distributions. Friction stir welding resulted in the reversion and coarsening of η′ precipitates. The formation of Guinier‐Preston zones in the stir zone and some parts of the heat‐affected zone during post‐weld natural aging increased the hardness. In transverse tensile specimens, fracture occurred in a location with the minimum hardness at either advancing or retreating side randomly. Further, influences of welding parameters on mechanical properties were investigated.