The effects of texture and grain morphology on the fracture toughness and fatigue crack growth resistance of nanocrystalline platinum films

The fracture toughness and fatigue crack growth resistance of nanocrystalline materials are significantly affected by the thickness of the specimen. In this work we relate the mechanical properties of nanocrystalline platinum films to their texture and grain morphology. Tensile, creep and fatigue testing of annealed, ∼1 μm films resulted in mechanical properties similar to the as-received films (yield strength of ∼1.2 GPa, fracture toughness ∼17.8 MPa √m, and a fatigue crack growth power law exponent of ∼4.2). However, the breakdown of the initially columnar grain morphology had a marked effect on the transition point from an intergranular to transgranular fatigue cracking mode. Finite element modeling suggests that cyclic (fatigue) grain coarsening and the transition from inter- to transgranular cracking modes are a result of the relative importance of dislocation slip accommodation on in-plane and through-thickness oriented slip directions.     

Fatigue properties and fracture analysis of a SiC fiber-reinforced titanium matrix composite

Tension–tension fatigue properties of SiC fiber reinforced Ti–6Al–4V matrix composite (SiC_f/Ti–6Al–4V) at room temperature were investigated. Fatigue tests were conducted under a load-controlled mode with a stress ratio 0.1 and a frequency 10 Hz under a maximum applied stress ranging from 600 to 1200 MPa. The relationship between the applied stress and fatigue life was determined and fracture surfaces were examined to study the fatigue damage and fracture failure mechanisms using SEM. The results show that, the fatigue life of the SiC_f/Ti–6Al–4V composite decreases substantially in proportion to the increase in maximum applied stress. Moreover, in the medium and high life range, the relationship between the maximum applied stress and cycles to failure in the semi-logarithmic system could be fitted as a linear equation: S_max/μ = 1.381 − 0.152 × lgN_f. Fractographic analysis revealed that fatigue fracture surfaces consist of a fatigued region and a fast fracture region. The fraction of the fatigued region with respect to the total fracture surface decreases with the increase of the applied maximum stresses.     

Experimental investigation on low cycle fatigue of DZ125 with film cooling holes in different processes of laser drilling

Due to the different low cycle fatigue (LCF) properties and fatigue fracture behavior around film cooling holes on DZ125, the LCF tests are carried out using tension cycling under stress control conditions (stress ratio R = 0.1) at 900 °C. The specimens were designed as thin-wall plate with single hole and multi holes under picosecond and nanosecond laser drilling processes. Comparative analyses of the differences between fatigue life and microscopic fracture morphology are conducted. It is shown that under the same stress condition, the relationship between fatigue life is as follows: picosecond laser single-holed specimen > nanosecond laser single-holed specimens > picosecond laser multi-holed specimens > nanosecond laser multi-holed specimens. Scanning electron microscope (SEM) analyses of the fracture revealed that the crack initiates from the film cooling holes where fatigue source zone, fatigue crack propagation zone and fatigue fracture zone can be found. However, the different processes lead to slightly different fracture morphology: radial-type ridge centering on the fatigue source zone is more apparent and uniform in picosecond laser drilling specimens than in the nanosecond laser drilling ones. On the other hand, the radial-type ridge is biased toward large-aperture side with nanosecond laser drilling.     

The development of microstructural damage during high temperature creep–fatigue of a nickel alloy

Alloy 617 is the leading candidate material for an Intermediate Heat Exchanger (IHX) of the Very High Temperature Reactor (VHTR). To evaluate the behavior of this material in the expected service conditions, strain-controlled cyclic tests that include hold times up to 9000 s at maximum tensile strain were conducted at 950 °C. The fatigue resistance decreased when a hold time was added at peak tensile strain, owing to the mechanisms resulting in a change in fracture mode from transgranular in pure fatigue to intergranular in creep–fatigue. Increases in the tensile hold duration beyond an initial value were not detrimental to the creep–fatigue resistance. An analysis of the evolving failure modes was facilitated by interrupting tests during cycling for ex situ microstructural investigation.     

Fatigue behavior and modeling of short fiber reinforced polymer composites including anisotropy and temperature effects

Effects of anisotropy and temperature on cyclic deformation and fatigue behavior of two short glass fiber reinforced polymer composites were investigated. Fatigue tests were conducted under fully-reversed (R = −1) and positive stress ratios (R = 0.1 and 0.3) with specimens of different thicknesses, different fiber orientations, and at temperatures of −40 °C, 23 °C, and 125 °C. In samples with 90° fiber orientation angle, considerable effect of thickness on fatigue strength was observed. Effect of mold flow direction was significant at all temperatures and stress ratios and the Tsai–Hill criterion was used to predict off-axis fatigue strengths. Temperature also greatly influenced fatigue strength and a shift factor of Arrhenius type was developed to correlate fatigue data at various temperatures, independent of the mold flow direction and stress ratio. Micromechanisms of fatigue failure at different temperatures were also investigated. Good correlations between fatigue strength and tensile strength were obtained and a method for obtaining strain–life curves from load-controlled fatigue test data is presented. A fatigue life estimation model is also presented which correlates data for different temperatures, fiber orientations, and stress ratios.     

Fatigue lifetime and tearing resistance of AA2198 Al–Cu–Li alloy friction stir welds: Effect of defects

The fatigue strength and failure mechanisms of defect-free (“sound”) and flaw bearing friction stir butt-welds of 3.1 mm-thick AA2198-T8 Al–Li–Cu alloy have been investigated via S–N curves at R = 0.1 using cross weld specimens. The fatigue strength of sound welds is only reduced by 10–15% at the aimed lifetime of 10⁵ cycles compared to the base material. Joint Line Remnant (JLR) bearing welds have a similar fatigue strength as sound welds and the JLR is not the crack initiation site. Kissing Bond (KB) bearing welds that have undergone a weld root polishing show a reduction in fatigue strength by 17% compared to sound welds. For specimens loaded at or above yield strength of the weld nugget the crack systematically initiates from the KB during the first cycle, which is interpreted further using fracture mechanics. The strongest reduction, about 28% in fatigue strength, is found for welds with an initial gap between the parent sheets (GAP welds) along with initiation at intergranular surface microcracks. Kahn tear tests show a reduction in tearing resistance for the flaw bearing welds with a similar ranking as for the fatigue strength.     

Effect of stress ratio on VHCF behavior for a compressor blade titanium alloy

Effect of stress ratio on fatigue properties of a titanium alloy (TC-17) in the high cycle fatigue (HCF) and very high cycle fatigue (VHCF) were investigated by electromagnetic and ultrasonic fatigue testing. The S–N curves at R = −1, 0.1, 0.5 and 0.7 at 110 Hz and 20 kHz were obtained and discussed. The effects of frequency on fatigue strength was also investigated. It was concluded that the fatigue strength with 50% fatigue failure probability at R = 0.1, 0.5 and 0.7 is lower to the Goodman line and shows a bilinear decreasing trend. Cleavage fracture of primary grains in the surface and interior initiation zone were observed. The formation of the facets induced by the basal or prismatic slips of the H.C.P grains decreased the fatigue strength with variation in mean stress.     

The role of oxidation damage in fatigue crack initiation of an advanced Ni-based superalloy

The effects of prior oxidation on the room temperature fatigue life of coarse-grained Ni-based superalloy, RR1000, have been investigated. High cycle fatigue tests were conducted, on both machined and pre-oxidised testpieces, at room temperature at an R ratio of 0.1. The oxidation damage was produced by pre-exposures at 700 °C for either 100 or 2000 h. Pre-oxidised testpieces tended to fail with shorter fatigue lives than those obtained from the as-machined testpieces although they were also observed to outperform the as-machined test pieces at peak stress levels around 900 MPa. The chromia scale and intergranular alumina intrusions formed during pre-oxidation are prone to crack under fatigue loading leading to early crack nucleation and an associated reduction in fatigue life. This has been confirmed to be the case both below and above a peak stress level of ∼900 MPa. The better fatigue performance of the pre-oxidised specimens around this stress level is attributed to plastic yielding of the weaker γ′ denuded zone, which effectively eases the stress concentration introduced by the cracking of the chromia scale and intergranular internal oxides. This γ′ denuded zone is also a product of pre-oxidation and develops as a result of the selective oxidation of Al and Ti. Over a limited stress range, its presence confers a beneficial effect of oxidation on fatigue life.     

Grain size effects in a Ni-based turbine disc alloy in the time and cycle dependent crack growth regimes

The fatigue crack growth (FCG) behaviour in a Ni-based turbine disc alloy with two grain sized variants, in a low solvus high refractory (LSHR) superalloy has been investigated under a range of temperatures (650–725 °C) and environments (air and vacuum) with trapezoidal waveforms of 1:1:1:1 and 1:20:1:1 durations at an R = 0.1. The results indicate that a coarse grained structure possesses better FCG resistance due to the enhanced slip reversibility promoted by planar slip as well as the reduction in grain boundary area. The fatigue performance of the LSHR superalloy is significantly degraded by the synergistic oxidation effect brought about by high temperature, oxidising environment and dwell at the peak load, associated with increasingly intergranular fracture features and secondary grain boundary cracking. Secondary cracks are observed to be blocked or deflected around primary γ′, carbides and borides, and their occurrence closely relates to the roughness of the fracture surface, FCG rate and grain boundary oxidation. The apparent activation energy technique provides a further insight into the underlying mechanism of the FCG under oxidation–creep–fatigue testing conditions, and confirms that oxidation fatigue is the dominant process contributing to the intergranular failure process. At high enough crack growth rates, at lower temperatures, cycle dependent crack growth processes can outstrip crack-tip oxidation processes.     

Characterisation of fatigue fracture surfaces of friction stir channelling specimens tested at different temperatures

The fatigue fracture surfaces of friction stir channelling specimens tested at room temperature, 120 °C and 200 °C were observed in a scanning electron microscope (SEM) in order to analyse their morphology and the crack propagation mechanisms. Three different friction stir channelling conditions were tested and analysed. For all specimens tested the developing fatigue-crack has always initiated at the advancing side, namely on the boundary between the nugget and the thermo mechanically affected zone (TMAZ) into the interior of the specimen. The crack has propagated through the channel nugget with a path tangential to the advancing side. After the crack has reached the processed surface, a second crack initiated at the channel bottom. The fracture surfaces have shown a semi-elliptical shape crack front. This second crack has propagated uniformly through the base material. Fatigue crack propagation on the TMAZ was mainly characterised by fatigue striations. It was found, on most of the surfaces observed, a clear coexistence of the intergranular fracture mode and the transgranular fracture mode. A relationship between the fatigue testing temperature and the roughness of the fracture surfaces was found. The fracture surfaces roughness was considerably lower at a testing temperature of 200 °C for the three friction stir channelling conditions analysed.     

Cyclic torsion very high cycle fatigue of VDSiCr spring steel at different load ratios

Cyclic torsion fatigue tests with superimposed static torsion loads are performed with VDSiCr spring steel with shot-peened surface in the high cycle fatigue (HCF) and very high cycle fatigue (VHCF) regime. Fatigue properties are investigated at load ratios R = 0.1, R = 0.35 and R = 0.5 up to limiting lifetimes of 5 × 10⁹ cycles with a newly developed ultrasonic torsion testing method. Increasing the load ratio reduces the shear stress amplitude that the material can withstand without failure. Fatigue cracks are initiated at the surface in the HCF regime. In the VHCF regime, cracks are preferentially initiated internally in the matrix, below the surface layer with compression residual stresses, and less frequently at the surface. Cyclic and mean shear stresses with 50% survival probability in the VHCF regime are presented in a Haigh diagram. Linear line approximation delivers a mean stress sensitivity of M = 0.33 for load ratios between R = −1 and R = 0.5.     

Fatigue of 2024-T351 aluminium alloy at different load ratios up to 1010 cycles

Fatigue properties of 2024-T351 aluminium alloy are investigated in the high cycle fatigue (HCF) and very high cycle fatigue (VHCF) regime. Endurance tests are performed with ultrasonic equipment at 20 kHz cycling frequency at load ratios of R = −1, R = 0.1 and R = 0.5 up to 10¹⁰ cycles. Additional servo-hydraulic tests between 8 and 10 Hz at R = 0.1 show no frequency influence on fatigue lifetimes. Linear lines in double logarithmic S–N plots are used to approximate data. Slope exponents of approximation lines increase with increasing numbers of cycles for all load ratios. Failures above 5 × 10⁹ cycles (R = −1 and R = 0.1) or 10¹⁰ cycles (R = 0.5) occur, and no fatigue limit is found. Fatigue cracks leading to failures above 10⁹ cycles are initiated at the surface or slightly below at broken constituent particles or at agglomerations of fractured particles, which are probably Al₇Cu₂(Fe, Mn). Specimens stressed with more than 10¹⁰ cycles at R = −1 without failure show several cracks starting at constituent particles. Maximum crack lengths are 30 μm, which is considerably below grain size.     

Loading frequency and microstructure interactions in intergranular fatigue crack growth in a disk Ni-based superalloy

The paper examines the role of the loading frequency on the dwell fatigue crack growth mechanism in the super-solvus nickel-based superalloy, ME3. This is accomplished by carrying out a set of crack growth experiments in air and vacuum at three temperatures; 650 °C, 704 °C and 760 °C using a dwell loading cycle with hold time periods up to 7200 s imposed at the maximum load level. Results of these tests show that the transitional transgranular/intergranular loading frequency is 0.1 Hz, and are used to determine the apparent activation energy of the time-dependent crack growth process. Analysis of this energy in both air and vacuum showed that the intergranular cracking is governed by a mechanism involving grain boundary sliding. This mechanism is explained in terms of absorption of dissociated lattice dislocations into grain boundary dislocations. The gliding of these dislocations under shear loading is assumed to cause grain boundary sliding. A condition for this mechanism to occur, is that a critical minimum distance exists between slip bands impinging the affected grain boundary. This condition is examined by correlating the slip band spacing (SBS) and loading frequency using a model based on minimum strain energy accumulation within slip bands and that a unique configuration of number and spacing of bands exists for a given plastic strain. The model outcome expressed in terms of SBS as a function of loading frequency is supported by experimental measurements at both high and low loading frequencies. Results of the model show that a saturation of SBS, signifying a condition for intergranualr cracking, is reached at approximately 3 μm which is shown to coincide with the transitional loading frequency of 0.1 Hz.     

Fatigue assessment of root failures in HSLA steel welded joints: A comparison among local approaches

Fatigue tests were performed on welded joints made of high-strength, low-alloy steel (S690). Different welding processes were tested, resulting in welds with different defects essentially consisting in lack of penetration. Fatigue tests were run with both constant and variable amplitude loading. The experimental results were compared to predictions obtained by applying local approaches (local stress and local strain) and the concepts of fracture mechanics. The local stress approach allowed the fatigue strength of joints in constant amplitude loading (for fatigue above 2 × 10⁶) to be predicted, but the assumption of a constant value of the slope k = 3 for all S–N curves led to non-conservative predictions of shorter lives. The local strain approach allowed the fatigue strength of the joints under constant amplitude to be predicted. Although, these predictions matched the experimental data well for both small and large defects in the entire cycle number range, they failed to predict the behaviour of joints under variable amplitude loading. Conversely, the fracture mechanics approach proved to be more efficient in predicting the fatigue behaviour of welded joint under variable amplitude loading.     

Experimental investigation of R-ratio effects on fatigue crack growth of adhesively-bonded pultruded GFRP DCB joints under CA loading

A series of fatigue experiments was performed in order to investigate the effect of the R-ratio on the fatigue/fracture behavior of adhesively-bonded pultruded GFRP double cantilever beam joints. Constant amplitude fatigue experiments were carried out under displacement control with a frequency of 5 Hz in ambient laboratory conditions. Three different R-ratios were applied: R = 0.1, R = 0.5 and R = 0.8. The crack length was determined by means of crack gages and a dynamic compliance method. The dominant failure mode was a fiber-tear failure that occurred in the mat layers of the pultruded laminates. The depth of the crack location significantly affected the energy dissipated for the fracture under cyclic loading. Short-fiber and roving bridging increased the fracture resistance during crack propagation. Fatigue crack growth curves were derived for each R-ratio and each observed crack path location. The fatigue threshold and slope of the fatigue crack growth curve significantly increased with increased R-ratio.     

Fatigue behavior of friction stir weld joints of Al–Zn–Mg alloy AA7039 developed using base metal in different temper condition

This paper presents the influence of base metal temper conditions (O, W and T6) on fatigue behavior of friction stir weld joints of Al–Zn–Mg alloy AA7039. Fatigue tests were performed at stress ratio of 0.1 and tensile to tensile stress in the range of 85–215 MPa to develop S–N curves. Fractured surfaces were investigated by SEM to determine the mode of fracture. On the basis of this study, friction stir welding of Al–Zn–Mg alloy AA7039 is recommended to be performed in W temper condition because of better tensile properties and superior fatigue strength.     

Research on fatigue behavior and residual stress of large-scale cruciform welding joint with groove

Fatigue fracture behavior of the 30 mm thick Q460C-Z steel cruciform welded joint with groove was investigated. The fatigue test results indicated that fatigue strength of 30 mm thick Q460C-Z steel cruciform welded joint with groove can reach fatigue level of 80 MPa (FAT80). Fatigue crack source of the failure specimen initiated from weld toe. Meanwhile, the microcrack was also found in the fusion zones of the fatigue failure specimen, which was caused by weld quality and weld metal integrity resulting from the multi-pass welds. Two-dimensional map of the longitudinal residual stress of 30 mm thick Q460C-Z steel cruciform welded joint with groove was obtained by using the contour method. The stress nephogram of Two-dimensional map indicated that longitudinal residual stress in the welding center is the largest.     

Effect of frequency on very high cycle fatigue behavior of a low strength Cr–Ni–Mo–V steel welded joint

Axially fully-reversed fatigue test of a low strength Cr–Ni–Mo–V steel welded joint was conducted up to the very high cycle fatigue regime under the frequency of 110 Hz and 20 kHz. The S–N curve shows a duplex shape at low frequency while decreases continuously at high frequency. Sites of crack initiation and fracture of the welds depend on stress level and loading frequency, hence leading to changed fatigue strength. In addition, frequency effect varies among different parts of the welded joint and fatigue lifetime.     

Fatigue behavior and failure mechanism of basalt FRP composites under long-term cyclic loads

This paper studies the fatigue behavior of basalt fiber reinforced epoxy polymer (BFRP) composites and reveals the degradation mechanism of BFRP under different stress levels of cyclic loadings. The BFRP composites were tested under tension–tension fatigue load with different stress levels by an advanced fatigue loading equipment combined with in-situ scanning electron microscopy (SEM). The specimens were under long-term cyclic loads up to 1 × 10⁷ cycles. The stiffness degradation, S–N curves and the residual strength of run-out specimens were recorded during the test. The fatigue strength was predicted with the testing results using reliability methods. Meanwhile, the damage propagation and fracture surface of all specimens were observed and tracked during fatigue loading by an in-situ SEM, based on which damage mechanism under different stress levels was studied. The results show the prediction of fatigue strength by fitting S–N data up to 2 × 10⁶ cycles is lower than that of the data by 1 × 10⁷ cycles. It reveals the fatigue strength perdition is highly associated with the long-term run-out cycles and traditional two million run-out cycles cannot accurately predict fatigue behavior. The SEM images reveal that under high level of stress, the critical fiber breaking failure is the dominant damage, while the matrix cracking and interfacial debonding are main damage patterns at the low and middle fatigue stress level for BFRP. Based on the above fatigue behavior and damage pattern, a three stage fracture mechanism model under fatigue loading is developed.