状态转换时流动带电的实验研究

该文通过实验的方法,对液压系统中状态转换时的流动带电进行实验研究,得出在系统状态转换的过渡过程中,同产生压力冲击一样,会产生流动带电的冲击,其峰值是定常状态的160%,峰值的大小是与其状态转换时的阀开启速度和定常流速有关的结论。     

Inelastic electron holography

Coherence of inelastically scattered electrons was investigated by means of biprism interference experiments performed in a transmission electron microscope equipped with a highly coherent field emission gun and an imaging filter. The experimental results show that within the wave inelastically scattered at aluminium plasmons there is in fact an area of about 10 nm diameter with coherence sufficient to take electron holograms.     

Ferroelectric electron holography

Ferroelectrics are increasingly important as materials in semiconductor technology, e.g. for building non-volatile memory chips. For optimisation of the properties of such devices, there is an urgent need for methods, which analyse the ferroelectric properties at nanometer scale. Furthermore, the basic understanding of the interaction of ferroelectrics with electrons in the transmission electron microscopy is still incomplete. It is shown that electron holography offers a promising way to understand and investigate ferroelectrics in the electron microscope.     

Inelastic scattering and holography

The controversy about whether or not an inelastically scattered electron wave can still interfere with a reference wave is solved by treating the whole problem rigorously and describing electron, source and object in one Hamiltonian. It turns out that, in principle, interference can occur between an inelastically scattered wave and a reference wave from the incident beam spectrum provided the energy difference is smaller than about 10(-15) eV. However, it is argued that the density of states in source object and electron wave is much too small to make this effect observable.     

Performance limits of electron holography

Transmission electron microscopy is wave optics. The object exit wave contains the full object information. However, in the usual intensity images, recorded either in real space or in Fourier space, the phases are missing. In many applications at medium and at high resolution, electron holography has shown its unique ability of solving the “missing phase problem” and utilizing the recovered phase for complete interpretation of the object structure. The question is “What are the performance limits?” with respect to field of view, lateral resolution and signal resolution. In this article, the performance limits are derived and discussed.     

Energy-filtered electron-diffracted beam holography

A method of energy-filtered electron holography is described where any two electron-diffracted beams can be interfered using an electron biprism. A Gatan image filter is used to select the energy loss of the electrons produced in the holograms. Gallium arsenide is used as the TEM specimen. This method of microscopy confirms that fringes extending beyond a limiting aperture were due to inelastically scattered electrons and specifically electrons scattered from the bulk plasmon. The degree of coherence of the zero-loss and energy-loss electrons were high and measured to be approximately 0.3, which was maintained even for the high energy-loss electrons up to 100 eV. Future systematic studies using this method should help understand the Stobbs factor and contribute to the development of quantitative high-resolution electron microscopy.     

A source of a wide-aperture gas-discharge plasma flow

The described generator produces a wide-aperture flow of charged plasma particles (electrons, positive and negative ions) with a cross-sectional diameter of at least 120 cm, which propagates to a distance of 50 cm or more (depending on the operating mode and the geometric dimensions of the vacuum chamber). The uniform distribution of charged particles in the cross section of the plasma flow is at least 98%. The discharge current reaches 1 A or more at an accelerating voltage of 0.3–6 kV. The energy of particles in the plasma flow under such conditions was 10–6000 eV at current densities of up to 10 mA/cm². The generator structure contains coaxially positioned meshes of the anode grid and the cathode grid. The latter closes the cavity inside the cathode volume at a depth of 3–5 mean free paths of electrons in the gas-discharge plasma flow. The cathode is manufactured so that the cavity diameter exceeds the diameter of the through cavity in the cathode insulation, the latter being determined by the size of the plasma-flow cross section. The distance between the grid anode and the cathode grid is equal to the Aston dark space of a glow discharge, thus permitting the cathode lifetime to be increased to 3 years. It is shown that the duration of the cathode continuous operation is determined by the chosen values of its cavity depth and accelerating voltage.     

What acoustic holography can do

The history of development of acoustic holography in Russia is outlined. Examples of its efficient applications are given.     

Planar diffracted-beam interferometry/holography

A method to interfere planar electron diffracted beams that have been created by a primary electron beam passing through a crystal specimen has been invented and referred to as planar diffracted-beam interferometry/holography (planar DBI/H). Planar DBI/H is able to measure the intensity and coherence properties of the diffracted electron beams. When the diffracted electron beams are energy filtered, planar DBI/H is also able to measure the intensity and coherence properties of the zero-loss electrons, phonon-loss electrons and plasmon-loss electrons. These coherence properties are useful to help our understanding of the Stobbs factor and the properties of advanced materials, necessary for our understanding of nanoscience and the development of nanotechnology.     

基于数字全息技术的变形测量

全息技术在测量、防伪中有大量应用.数字全息技术采用数字记录和计算机处理,实现测量的方法上有其特点.本文重点对数字全息技术实现变形测量的方法和具体算法开展了研究.论文首先总结了数字全息技术应用中的基本问题,包括数字全息算法问题和噪声抑制问题等.叙述了基于数字全息技术的变形测量基本思想,及相位恢复算法,同时分析了几种变形测量的实现方法,并提出了"2+2"步变形测量方法.该方法相对于"1+1"步变形测量方法,提高了测量精度,同时比"4+4"步变形测量法提高了动态性.本文建立了实验系统,获得了硬币的数字全息图,实现了常用的"1+1"步变形测量方法、相移算法的变形测量方法以及"2+2"步变形测量方法,给出了"2+2"变形测量的实验结果.实验结果表明在数字全息技术中结合相移技术进行测量,可以提高物波再现精度,进而提高变形等的测量精度.     

Experiments on inelastic electron holography

Using the combination of an electron biprism and an energy filter, the coherence distribution in an inelastically scattered wave-field is measured. It is found that the degree of coherence decreases rapidly with increasing distance between two superimposed points in the object, and with increasing energy-loss. In a Si sample, coherence of plasmon scattering increases in vacuum with the distance from the edge of the sample.     

Off-axis electron holography of patterned magnetic nanostructures

Magnetization reversal processes in lithographically patterned magnetic elements that have lateral dimensions of 70–500 nm, thicknesses of 3–30 nm and a wide range of shapes and layer sequences have been followed in situ using off-axis electron holography in the transmission electron microscope. This technique allows domain structures within individual elements and the magnetic interactions between them to be quantified at close to the nanometre scale. The behaviour of 30 nm-thick Co elements was compared with that of 10 nm-thick Ni and Co elements, as well as with Co/Au/Ni trilayers. The hysteresis loops of individual elements were determined directly from the measured holographic phase images. The reproducibility of an element's domain structure in successive cycles was found to be affected by the out-of-plane component of the applied magnetic field and by the exact details of its initial magnetic state. Close proximity to adjacent elements led to strong intercell coupling, and remanent states with the in-plane magnetic field removed included domain structures such as solenoidal (vortex) states that were never observed during hysteresis cycling. Narrow rectangular bars reversed without the formation of end domains, whereas closely separated magnetic layers within individual elements were observed to couple to each other during field reversal.     

全息学中计算机图像处理技术的应用研究

全息技术是物理学中的重大发现,随着计算机技术和相关设备的完备,数字全息术的研究应用得以飞速发展.CCD和计算机图像处理技术为全息技术的两个重要部分.本文将着重从计算机应用方面阐述图像处理技术在全息学的应用.     

Vacuum-ultraviolet Gabor holography with synchrotron radiation

We present the realization of high-resolution holographic microscopy using the original Gabor geometry and imaging with radiation in the vacuum-ultraviolet (VUV) spectral region. Synchrotron VUV radiation with a wavelength of 13.8 nm was focused on a small pinhole generating a highly divergent light cone suitable for digital in-line holography. Objects of different thickness and materials have been used to test the imaging properties of holographic microscopy in the VUV wavelength range. The effective numerical aperture was limited by the illuminated area of the detector, yielding a theoretical resolution below 1 microm and an experimental one of approximately 1 microm.     

Hologram simulation for off-axis electron holography

Hologram simulation for electron holography using an electron biprism is described. An electron hologram is superimposed by Fresnel fringes originating from the electron biprism, which affects both the amplitude and the phase of the object wave and the reference wave. In this simulation, we consider the effects of Fresnel diffraction as well as the electron-wave phase shift due to the electromagnetic field produced by the specimen. We also take into account the phase shift due to the inner potential of the specimen, the amplitude modulation due to the absorption of the incident electrons by the specimen, reference-wave distortion caused by the electromagnetic fields, coherency of the electron wave, and quantum noise of the detected electrons. Simulated and experimentally obtained holograms and reconstructed images are compared for the cases of a charged latex spherical particle and a single magnetic-domain spherical particle placed on a carbon film.     

Multiple scattering in low-energy electron holography

The theory of the low-energy electron point source (LEEPS) microscope is reformulated in matrix form to readily account for multiple scattering. An algorithm is developed for the storage of the structure matrix and an iterative method is used to solve the matrix equation for the structure factor. Examples of small and large clusters of atoms are given to compare single and multiple scattering. A Kirchhoff-Helmholtz transform is used for the reconstruction. We find that in some cases the multiple scattering is too strong and reconstruction is not possible. We give examples which show that, even when multiple scattering is important, one can still obtain reconstructions that reveal the atomic structure both along and lateral to the optical axis. We also compare our results with those found in LEED.     

CFD analysis of flow phenomena inside thermo vapor compressor influenced by operating conditions and converging duct angles

A thermo vapor compressor is simply a steam ejector employed in a multi effect desalination process. A greater understanding of flow phenomena inside an ejector plays an important role in its performance improvement. In this paper, CFD investigation has been carried out to study the flow structure inside a steam ejector. This research revealed the influence of operating pressures and ejector geometries on the flow structure and the performance of a steam ejector. The CFD results were verified with available experimental data. The angle of the converging duct as the geometry parameter was varied as 0°, 0.5°, 1°, 2°, 3.5° and 4.5°. The best performance was obtained by the ejector with converging duct angle of 1°.     

Specimen preparation for electron holography of semiconductor devices

A reliable and quick method of preparing specimens for electron holography of semiconductor devices is described in detail. The method is based on conventional mechanical grinding and polishing, and argon-ion milling, providing a large ( approximately 100 microm) area of electron transparency, no curtaining and thin dead layers on the surfaces of specimens. The vacuum area, necessary for the reference wave, is cut into the specimen by a focused ion beam. The advantages and disadvantages are discussed. The method has a yield greater than 90%, of tests of more than 20 specimens of MOS transistors.     

Past,present and future of electron holography

Electron holography, originally devised for improving the resolution of electron microscopes, progressed significantly with the advent of the ‘coherent’ field-emission electron beam. This permitted high-resolution microscopy (Lichte, 1986), and opened up such new fields as high-precision electron interferomentry. This paper briefly describes the developments in electron holography.