异步轧制AZ31镁合金板材的孪晶组织及织构北大核心CSCD

采用异步轧制（AR）工艺和同步轧制（NR）工艺制备了AZ31镁合金板材,分析了AZ31镁合金板材的组织性能和力学性能,研究了轧制过程中孪晶组织和织构的演变规律,以及异步轧制工艺参数对镁合金板材组织、织构和力学性能的影响。结果表明,在压下量为3％～15％的范围内,异步轧制与同步轧制板材在晶粒尺寸以及均匀性上有相似的变化趋势。在变形初期,随压下量的增加,孪晶数量不断增加,孪晶使异步轧制与同步轧制板材中晶粒取向都发生偏转,即C轴趋向于垂直于法向（ND）,从而使初始挤压板材的丝织构强度减弱;当压下量达到24％时孪晶大量减少或消失。在压下量为3％～24％的范围内,同步轧制对板材力学性能的影响并不明显,峰值应变呈交替性变化,异步轧制板材在压下量达到24％时,表现出了良好的塑性变形能力,抗拉强度达到309MPa,峰值应变达到16．3％。     

异步冷轧压下量对AZ31镁合金板显微组织的影响

对AZ31镁合金板进行了5%、10%、15%压下量的异步冷轧,通过金相分析研究了不同的冷轧压下量对AZ31镁合金板材截面显微组织分布的影响。结果表明:随着压下量的增加,板材组织中孪晶和形变带增加。5%和10%压下量时,AZ31镁合金冷轧板的变形主要为孪生;压下量为15%时,变形主要为孪晶和形变带。当压下量较小时,孪晶在板材厚度方向的分布存在明显的不均匀,轧面附近的孪晶比板材心部多。随着变形逐渐深入到板材内部,剪切应变在板材厚度方向上各层的分布也逐渐趋于均匀。由于是异步轧制,板材上下轧面附近剪切应变分布不同,对应显微组织中的孪晶和形变带存在差异。     

初始取向对大应变轧制AZ31镁合金板材显微组织和力学性能的影响

采用大应变轧制技术对轧制面与挤压板材ED-TE面分别成90°、45°和0°的AZ31镁合金板材进行加工,研究初始取向对板材显微组织和力学性能的影响。结果表明:孪生诱发动态再结晶是大应变轧制过程中主要的再结晶机制,动态再结晶的发生使合金晶粒细化、力学性能大幅提高。轧制过程中孪生与板材初始取向密切相关,通过改变初始取向可控制板材晶粒细化和强度改善效果。0°轧制试样大应变轧制过程中,大部分晶粒的c轴受压,基面滑移启动难度增加,孪生的作用增强,压缩孪晶密度增大,进而通过孪生诱发动态再结晶获得更为细小的再结晶组织和更为优异的力学性能。压下量为80%时,0°轧制板材的平均晶粒尺寸为5μm,抗拉强度、屈服强度和伸长率分别为311.4 MPa、202.6 MPa和26.9%。     

不同轧制工艺参数条件下AZ31镁合金孪晶和织构的演变规律及其对力学性能的影响（英文）

为了考察轧制工艺参数对板材显微组织和力学性能的影响,通过不同温度和轧制变形量的热轧工艺得到具有不同晶粒尺寸、基面织构强度和孪晶类型的AZ31镁合金轧制板材。拉伸孪晶、压缩孪晶和双孪晶的体积分数与AZ31镁合金轧制板材的晶粒尺寸有关。当轧制温度为523 K、轧制变形量为10%时轧制得到的板材,三种类型孪晶的体积分数最高,此时晶粒尺寸最大。在轧制温度分别为523和473 K时,板材发生完全动态再结晶的临界变形量分别为30%和40%。拉伸实验结果表明:随着轧制变形量的增加,在第一阶段,轧制后板材屈服强度的提高主要依赖于晶粒细化强化和织构强化;当晶粒尺寸随变形量的增加不再发生明显的细化时,板材的屈服强度主要受织构弱化的影响。     

异步轧制AZ31镁合金的微观组织与室温成形性能

探讨采用小异速比多道次异步轧制技术提高AZ31镁合金板材室温成形性能的可行性,研究异步轧制板材微观组织的特点、形成机理及其与成形性能间的内在联系。结果表明:多道次异步轧制所累积的剪切应变能有效促进压缩孪晶的交互作用,细化合金晶粒组织,削弱(0002)基面的织构强度;异步轧制AZ31镁合金板材后续退火处理后的室温伸长率和Erichsen值分别可达32%和6.14mm;(0002)基面织构减弱和塑性应变比的降低是板材室温成形性能提高的根本原因。     

异步轧制硅钢的表面纳米化及轧制参数的影响

对硅钢板材分别进行异步和同步轧制,研究了轧制参数包括速比、压下量和道次对板材表面显微组织的演变的作用.结果表明,异步轧制硅钢板材表面形成了晶粒尺寸为10~50 nm,取向接近随机分布的纳米晶,而同步轧制板材的表面只形成了位错胞,证明异步轧制可以诱发表面纳米化.异步轧制板材表面纳米晶的形成过程为:在剪切力的反复作用下,高密度位错形成、滑移、湮灭和重组形成亚微米尺度的亚微晶/位错胞.随着压下量和轧制道次增加,高密度位错重复以上过程使晶粒尺寸减小、取向差增大,最终形成取向接近随机分布的纳米晶组织.大压下量和多道次是异步轧制诱发板材表面纳米化的关键,而速比的增加可以加快纳米化进程.     

异步轧制对AZ31镁合金板材组织和性能的影响

对不同轧制温度、道次压下量以及轧制路径等工艺条件下所制备的AZ31镁合金板材的组织和性能进行了研究。结果表明,当温度由623K升到723K时,晶粒发生长大,孪晶消失,板材的抗拉强度由275MPa降到250MPa,伸长率则由14.5%增加到18%;当道次压下量从5%增加到20%时,晶粒逐渐得到细化,板材的抗拉强度由道次压下量为5%时的265MPa增加到20%时的300MPa,伸长率则由18%降到15%;轧制路径的改变,使不同板材中孪晶的数量产生改变,路径A中的孪晶较多,伸长率较低,强度较高,路径D中的孪晶较少,伸长率较高,强度较低。     

交叉轧制对ZK60镁合金组织演变和性能的影响

研究了轧制方式对ZK60镁合金组织与织构的影响规律,同时通过对退火后板材进行室温拉伸试验研究了其力学性能。经过交叉轧制的镁合金板材由于二次孪晶的生成及非基面滑移系的启动促使再结晶程度增大,晶粒细化效果显著,退火后平均晶粒尺寸达到6.43μm。同时交叉轧制会迫使晶粒向TD方向旋转,从而降低织构强度,改变织构类型。相比于单向轧制,交叉轧制后板材的平均抗拉强度和伸长率分别提高到321 MPa和25.7%,伸长率提高了近50%;塑性应变比、平面各向异性指数、屈强比等指标也得到了改善。结果表明,交叉轧制可有效调控镁合金板材组织及其均匀性、提高力学性能和成形性能。     

异步热轧对钛合金Ti-6Al-4V微观组织及力学性能的影响

通过异步/同步热轧实验研究了异步热轧工艺对钛合金显微组织和力学性能的影响。实验表征了试样的显微组织、力学性能、断口形貌和微观取向。实验结果表明,复杂应变路径较之简单应变路径能更好的细化晶粒及同时提高强度和塑性,并且表层晶粒小于中心晶粒。异步轧制工艺相比同步轧制能更好获得细小晶粒。异步轧制试样的强度及塑性值高于同步轧制试样相应值,提高异步速比可提高强度及塑性值。异步轧制试样的塑性变形机制可能是滑移,而同步轧制试样塑性变形机制为滑移或孪晶。     

异步热轧对钛合金Ti-6Al-4V微观组织及力学性能的影响（英文）

通过异步/同步热轧实验研究了异步热轧工艺对钛合金显微组织和力学性能的影响。实验表征了试样的显微组织、力学性能、断口形貌和微观取向。结果表明,复杂应变路径较之简单应变路径能更好地细化晶粒,同时提高强度和塑性,并且表层晶粒小于中心晶粒。异步轧制工艺相比同步轧制能更好地获得细小晶粒。异步轧制试样的强度及塑性值高于同步轧制试样相应值,提高异步速比可提高强度及塑性值。异步轧制试样的塑性变形机制可能是滑移,而同步轧制试样塑性变形机制为滑移或孪晶。     

轧制工艺对AZ31B镁合金薄板组织与性能的影响

研究了轧制温度和轧制速度对AZ31B镁合金薄板微观组织演变和力学性能的影响。结果表明,轧辊加热有利于镁合金薄板成型;AZ31B镁合金在低温或低速轧制时薄板纵向组织为大量的切变带,切变带区域包含大量孪晶组织,横向组织为含极少量孪晶的等轴晶组织;在轧制温度为400℃和轧制速度为16m/min轧制时,由于动态再结晶,横纵截面组织均为等轴晶。AZ31镁合金薄板的最佳轧制制度为轧辊温度为70℃、轧制温度为400℃、轧制速度为6m/min,此工艺轧制的薄板横向抗拉强度、屈服强度和伸长率分别为350MPa、300MPa和12%,纵向为345MPa、290MPa和11.2%,纵向与横向性能差别明显减小。     

Microstructure and mechanical properties of a basal textured AZ31 magnesium alloy cryorolled at liquid-nitrogen temperature

A strongly basal textured AZ31 magnesium alloy were cryorolled at liquid-nitrogen temperature at various strains. The microstructure and texture of the rolled sheets have been investigated using electron backscatter diffraction (EBSD) and X-ray diffraction. The microstructural and textural evolutions of the AZ31 magnesium alloy during cryorolling have been discussed. A lot of twins were observed in the rolled sheets. The influence of strain on the twin types and variant selection during cryorolling for the magnesium alloy has been discussed quantitatively based on the orientation data collected using EBSD. The influence of the twins on the microstructural and textural evolutions for the AZ31 magnesium alloy during cryorolling has also been discussed. The mechanical properties of the cryorolled sheets were tested by uniaxial tensile tests at the ambient temperature with a strain rate 10^-3s^-1 in the tensile direction respectively along the rolling and transverse directions of the rolled sheets. The relationships between the mechanical properties and microstructure of the cryorolled sheets have been discussed in the present work. The active twinning during rolling at that cryogenic temperature has been found to play an important role in influencing the microstructure, texture, as well as the mechanical properties of the AZ31 magnesium alloy.     

轧制温度对AZ31镁合金轧制板材中的{1011}-{1012}双孪生行为的影响

在150-350℃温区内不同温度下轧制AZ31镁合金板,观察了不同温度下轧制变形量为9%的AZ31镁合金板材的显微组织,研究分析了轧制温度对轧制板材中{1011}-{1012}双孪晶的含量、类型以及高温轧制过程中双孪晶中的动态再结晶行为的影响,讨论了板材中的孪晶对其力学性能的影响.研究结果表明:在150-300℃温区内轧制时,板材组织中均有含量不等的{1011}-{1012}双孪晶,随着轧制温度的升高,孪晶含量下降.250℃以上轧制的板材中单片一次孪晶中出现的双孪晶类型较为单一,仅出现共面型双孪晶.在250℃以上轧制板材中的双孪晶晶界处中可以观察到明显的动态再结晶现象,这些动态再结晶晶粒对孪晶界和孪晶起到消除和吞噬的作用.350℃下轧制的AZ31镁合金板材中未观察到{1011}-{1012}双孪晶.随着轧制温度的升高,镁合金轧制板材的强度减弱而塑性增强.     

Effect of plane strain on microstructures and texture, through the reduction ratio of AZ31 Mg alloy

Structural evolution of warm-rolled AZ31 alloy sheets was investigated with respect to various reduction ratios. In order to examine the effect of rolling pass on deformation of the sheet, one-pass rolling was applied to the AZ31 alloys for various 6/1/2011reduction ratios. When the applied reduction ratio was ∼85% of the initial thickness, significant grain refinement and texture development were achieved with dynamic recrystallization. Moreover, with the increase of the rolling reduction ratio from 30% to 85%, the warm rolled sheets exhibit plane strain mode displaying uniform 〈0 0 0 1〉//ND basal textures throughout the whole sheet thickness. The two-dimensional finite element method simulation showed that the current lubrication rolling results in a uniform plane strain deformation through the whole warm rolled sheet.     

脉冲电流轧制对AZ31镁合金微观组织与力学性能的影响

对比研究脉冲电流轧制工艺与温轧工艺对AZ31镁合金板材的力学性能、织构、微观组织与沉淀相等方面的影响。结果表明：脉冲电流具有促进冷轧AZ31镁合金低温再结晶能力的作用。脉冲电流轧制后的镁合金板材组织由细小的等轴再结晶粒与析出相构成,没有发现孪晶组织,并且完全再结晶,原始晶粒均被细小的再结晶晶粒取代,再结晶晶粒内的位错密度低。而温轧镁合金组织则由稍拉长变形孪晶、粗大的再结晶晶粒和析出相构成,再结晶的晶粒内位错密度高。两种轧制方式下的镁合金析出相均为Mg17Al12。脉冲电流轧制后镁合金的织构具有典型基面织构的特征,而脉冲电流轧制镁合金的织构则出现横向偏转;脉冲电流轧制后镁合金的屈服强度与伸长率均比温轧镁合金的大,但抗拉强度正好相反。     

Improving single pass reduction during cold rolling by controlling initial texture of AZ31 magnesium alloy sheet

The AZ31 magnesium alloy sheets obtained by multi-pass hot rolling were applied to cold rolling and the maximum single pass cold rolling reduction prior to failure of AZ31 magnesium alloy was enhanced to 41%. Larger single pass rolling reduction led to weaker texture during the multi-pass hot rolling procedure. The sheet obtained showed weak basal texture, while the value was only 1/3–1/2 that of general as-rolled AZ31 Mg alloy sheets. It was beneficial for the enhancement of further cold rolling formability despite of the coarser grain size. The deformation mechanism for the formation of texture in AZ31 magnesium alloy sheet was also analyzed in detail.     

Influence of rolling route on microstructure and mechanical properties of AZ31 magnesium alloy during asymmetric reduction rolling

Four different routes of asymmetric reduction rolling were conducted on AZ31 magnesium alloy to investigate their effect on the microstructure evolution and mechanical properties. Route A is the forward rolling; while during routes B and C the sheets are rotated 180° in rolling direction and normal direction, respectively; route D is the unidirectional rolling. The strain states of rolled sheets were analyzed by the finite element method, while the microstructure and texture were observed using optical microscopy, X-ray diffraction and electron back-scattered diffraction techniques, and the mechanical properties were measured by tensile test. The results show that route D produced the largest effective strain. Compared with other samples, sample D exhibited a homogeneous microstructure with fine grains as well as a weak and tilted texture, in corresponding, it performed excellent tensile properties, which suggested that route D was an effective way to enhance the strength and plasticity of AZ31 sheet.     

Microstructure and texture evolution of AZ31 magnesium alloy during rolling

The production of magnesium alloy sheets normally involves several processing stages including hot rolling,cold rolling and intermediate annealing.The microstructure and texture evolution of AZ31 magnesium alloy sheets in different processing states were investigated by optical microscopy and X-ray diffraction technique.It is found that the microstructure of hot-rolled sheets is dominated by recrystallized equiaxed grains,while that of cold-rolled sheets is dominated by deformation twins.With final annea...     

AZ31镁合金轧制板材退火后的组织与力学性能

采用单向轧制和交叉轧制工艺分别进行了AZ31镁合金板材轧制实验,分析了轧制板材经退火处理后的组织与力学性能。结果表明:采用单向轧制工艺,当板材最终变形量相等时,经退火处理后的板材大压下量比小压下量得到的微观组织更为细小;交叉轧制得到轧制板材可以缓解镁合金轧制板材在室温下的各向异性,其微观组织较单向轧制均匀,具有更好的冲压成形性能;交叉轧制和单向轧制两种工艺得到的板材微观组织细化效果相似。     

异步轧制对AZ31镁合金板材组织和性能的影响

对不同轧制温度、道次压下量以及轧制路径等工艺条件下所制备的AZ31镁合金板材的组织和性能进行了研究。结果表明．当温度由623K升到723K时，晶粒发生长大，孪晶消失，板材的抗拉强度由275MPa降到250MPa，伸长率则由14．5％增加到18％；当道次压下量从5％增加到20％时，晶粒逐渐得到细化，板材的抗拉强度由道次压下量为5％时的265MPa增加到20％时的300MPa，伸长率则由18％降到15％；轧制路径的改变，使不同板材中孪晶的数量产生改变，路径A中的孪晶较多，伸长率较低，强度较高，路径D中的孪晶较少，伸长率较高．强度较低。