A first report on fracture toughness ofbcc iron alloys as influenced by solutes: opposite effects of silicon and cobalt

The effect of solutes on resistance to fracture of body centred cubic iron single-phase solid-solution alloys has been investigated. TheJ-integral method has been used for the measurement of ductile fracture toughness. TheJ _IC values so determined quantitatively indicate the extent of degradation in fracture toughness due to the addition of hardening solute silicon. Cobalt addition results in alloy softening. The measuredJ _IC values clearly demonstrate the toughening effect of cobalt addition as a solute, which result renders the case of Fe-Co solid-solution alloys interesting.     

Further developments in <Emphasis Type="Italic">J</Emphasis> evaluation procedure for growing cracks based on LLD and CMOD data

Laboratory testing of fracture specimens to measure resistance curves (J − Δa) have focused primarily on the unloading compliance method using a single specimen. Current estimation procedures (which form the basis of ASTM E1820 standard) employ load line displacement (LLD) records to measure fracture toughness resistance data incorporating a crack growth correction for J. An alternative method which potentially simplifies the test procedure involves the use of crack mouth opening displacement (CMOD) to determine both crack growth and J. However, while the J-correction for crack growth effects adopted by ASTM standard holds true for resistance curves measured using load line displacement (LLD) data, it becomes unsuitable for J-resistance measurements based upon the specimen response defined in terms of load-crack mouth opening displacement (CMOD). Consequently, direct application of the evaluation procedure for J derived from LLD records in laboratory measurements of resistance curves using CMOD data becomes questionable. This study provides further developments of the evaluation procedure for J in cracked bodies that experience ductile crack growth based upon the eta-method and CMOD data. The introduction of a constant relationship between the plastic components of LLD (Δ _p ) and CMOD (V _p ) drives the development of a convenient crack growth correction for J with increased loading when using laboratory measurements of P-CMOD data. The methodology broadens the applicability of current standards adopting the unloading compliance technique in laboratory measurements of fracture toughness resistance data (J resistance curves). The developed J evaluation formulation for growing cracks based on CMOD data provides a viable and simpler test technique to measure crack growth resistance data for ductile materials.     

Comparative studies of several methods to determine the dynamic fracture toughness of a nuclear pressure vessel steel A508 CL3 with Charpy-size specimen

In this investigation, five estimation methods have been adopted to estimate the dynamic fracture toughness of a nuclear pressure vessel steel A508 CL3 by using pre-cracked Charpy-size specimens on an instrumented impact test machine. Furthermore, the merits and the demerits of the five methods have also been compared. The experimental results indicate that the maximum load energy method based on the curve of load versus load-point displacement overestimates the dynamic fracture toughness J _Id , especially above room temperature. The method of compliance changing rate underestimates the dynamic fracture toughness. The method of measuring the critical stretch zone width (SZW _c ) at the crack tip by means of SEM fractography and then converting the SZW _c into J _Id has a relatively large error. In addition, it is expensive and difficult to measure the SZW _c . The method of energy revised at the maximum load may be considered a better single-specimen method for determining the dynamic fracture toughness. Furthermore, the results indicate that although the dynamic resistance curve method can exactly estimate the dynamic fracture toughness of the material, this method needs several specimens. Moreover, the test procedure is complicated. Thus, it is not suitable for nuclear reactor pressure vessel embrittlement surveillance.     

DAMAGE MECHANICS APPROACH TO REMOVE THE CONSTRAINT DEPENDENCE OF ELASTIC–PLASTIC FRACTURE TOUGHNESS

It is now generally agreed that the applicability of a one-parameter J-based ductile fracture approach is limited to so-called high constraint crack geometries, and that the elastic-plastic fracture toughness J_1c, is not a material constant but strongly specimen geometry constraint-dependent. In this paper, the constraint effect on elastic-plastic fracture toughness is investigated by use of a continuum damage mechanics approach. Based on a new local damage theory for ductile fracture(proposed by the author) which has a clear physical meaning and can describe both deformation and constraint effects on ductile fracture, a relationship is described between the conventional elastic-plastic fracture toughness, J_1c, and crack tip constraint, characterized by crack tip stress triaxiality T. Then, a new parameter J_dc (and associated criterion, J_d=J_dc) for ductile fracture is proposed. Experiments show that toughness variation with specimen geometry constraint changes can effectively be removed by use of the constraint correction procedure proposed in this paper, and that the new parameter J_dc is a material constant independent of specimen geometry (constraint). This parameter can serve as a new parameter to differentiate the elastic-plastic fracture toughness of engineering materials, which provides a new approach for fracture assessments of structures. It is not necessary to determine which laboratory specimen matches the structural constraint; rather, any specimen geometry can be tested to measure the size-independent fracture toughness J_dc. The potential advantage is clear and the results are very encouraging.     

Evaluation of the ISO <Emphasis Type="Italic">J</Emphasis> initiation procedure using the EURO fracture toughness data set

The multiple specimen J _0.2/BL initiation fracture toughness test procedure from the ISO standard, ISO 12135:2002, is evaluated using the EURO fracture toughness data set. This standard is also compared with the ASTM standard, ASTM E 1820, multiple specimen J _Ic procedure. The EURO round robin data set was generated to evaluate the transition fracture toughness methods for steels. However, many of the tests resulted in ductile fracture behavior giving final J versus ductile crack extension points. This is the information that is measured in a multiple specimen J initiation fracture toughness test. The data set has more than 300 individual points of J versus crack extension with four different specimen sizes. It may be the largest data set of that type produced for one material. Therefore, its use to determine J initiation values can provide an important evaluation of the standard procedures. The results showed that a J _0.2/BL value could be determined from the ISO standard for three of the four specimen sizes, the smallest size did not meet the specimen size requirement on J. The construction line slopes in this method are very steep compared with the ASTM construction line slopes. This resulted in low J initiation values, about a factor of two lower than the one from the ASTM method. Of the various criteria imposed to determine a valid J _0.2/BL value, the one limiting the maximum J value was the most questionable. It had an effect of eliminating small specimen data that was identical to acceptable large specimen data.     

A direct estimate of JIc from the load versus load-line displacement record

The purpose of this study is to examine the current standard fracture toughness test procedure to determine if there could be an easier method to get a J_Ic value from the test record. The current method for determining J_Ic involves a detailed computational and construction procedure. The objective in this study is to simplify the analysis for the determination of J_Ic. The results of this study show that the load and displacement record for a fracture toughness test can be used to directly estimate a J_Q value, a provisional value for fracture toughness, J_Ic. The J value taken at the maximum load point can be used along with an adjustment factor to estimate a J_Q value. This J_Q estimate is close to the one obtained from the construction procedure of ASTM Standard E 1820. When a unit‐sized specimen is tested, that is, a specimen with a width of 50 mm and a thickness of 25 mm the maximum load point provides a direct estimate of J_Q. Other sizes require a size adjustment factor, which is simply a square root relationship between the width of the test specimen and a unit width. The proposed new method of estimating J_Q is simple in concept and requires a minimum number of calculations. It appears to produce values of J_Q which are comparable to those obtained from the ASTM E1820 construction procedure and may produce less scatter.     

Assessment of the fracture toughness of cast steels

Estimates of the fracture toughness in terms of the critical stress intensity factorsK _C andK _IC are made for a 1Cr steel, a 1/2Cr-1/2Mo-1/4V steel, a 1 1/2Mn-Ni-Cr-Mo steel and a 1 1/2 Ni-Cr-Mo steel all in cast form. The methods used are linear elastic fracture mechanics,J-integral and crack opening displacement methods. The last two methods are applied in combination with an electrical potential method to detect the initiation of fracture.     

A new method to estimate the plane strain fracture toughness of materials

Although the testing method for fracture toughness K_IC has been implemented for decades, the strict specimen size requirements make it difficult to get the accurate K_IC for the high‐toughness materials. In this study, different specimen sizes of high‐strength steels were adopted in fracture toughness testing. Through the observations on the fracture surfaces of the K_IC specimen, it is shown that the fracture energy can be divided into 2 distinct parts: (1) the energy for flat fracture and (2) the energy for shear fracture. According to the energy criterion, the K_IC values can be acquired by small‐size specimens through derivation. The results reveal that the estimated toughness value is consistent with the experimental data. The new method would be widely applied to predict the fracture toughness of metallic materials with small‐size specimens.     

Non-linear fracture mechanics

The fracture of solids is analyzed using the formalism of equilibrium mechanics. A partially cracked, mechanically loaded reversible system is considered. A stability criteria is formulated. The equilibrium theory is valid for non-linear load deflection relationships and is applied to linear elastic fracture mechanics, the Hertz test and J _IC tests.

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Résumé La rupture des solides est analysée en utilisant le formalisme de la mécanique de l'équilibre. On considère un système partiellement fissuré réversible et chargé mécaniquement. On formule un critère de stabilité. La théorie de l'équilibre est valide pour des relations non linéaires charge déflection et est appliquée à la mécanique de la rupture élastique, à l'essai de Hertz et aux essais J _IC.

     

Comparison of mode I and mode II elastic-plastic fracture toughness for two low alloyed high strength steels

In the present work, mode I and mode II tests were carried out on two low alloyed high strength steels. An asymmetrical four point bend specimen and J _II-integral vs. crack growth resistance curve technique were used for determining the mode II elastic-plastic fracture toughness, J _IIc · J _II-integral expression of the specimen was calibrated by finite element method. The results indicate that the present procedure for determining the J _IIc values is easy to use. Moreover, the mode I fracture toughness J _Ic is very sensitive to the rolling direction of the test steels, but the mode II fracture toughness J _IIc is completely insensitive to the rolling direction of the steels, and the J _IIc /J _Ic ratio is not a constant for the two steels, including the same steel with different orientations. Finally, the difference of the fracture toughness between the mode I and mode II is discussed with consideration of the different fracture mechanisms.     

High rate toughness of ductile polymers

Impact toughness of two highly ductile polymers: acrylonitrile-butadiene-styrene (ABS) terpolymer and polypropylene block copolymer (PPBC) - was evaluated using the essential work of fracture (EWF) - and a J-R resistance single specimen curve - S_pb techniques. The EWF has proved to be capable of determining toughness from the total fracture energy of several samples differing in initial ligament length and the linear regression of the data. On the other hand, the S_pb method, which is based on the load separation principle, is able of constructing J-R curves by inferring instantaneous crack growth length from the sole comparison between one sharp and one blunt-notched load-displacement traces. Results show that both methodologies can be used under impact conditions when evaluating ABS polymers. However, ABS impact fracture toughness value yielded by the EWF method, w_Ie, was larger than the J_0.2 value obtained from the S_pb method. This difference was imputed to the more progressive development of the necking zone in front of the crack tip under plane strain conditions. On the contrary, for very ductile fracture behavior like that demonstrated by PPBC in which J-controlled conditions were not achieved and hence J-R curves could not be built the EWF appeared as a valuable alternative to characterize impact toughness.     

Constraint-modified J−R curves and its application to ductile crack growth

The concept of J-controlled crack growth is extended to J–A ₂ controlled crack growth using J as the loading level and A ₂ as the constraint parameter. It is shown that during crack extension, the parameter A ₂ is an appropriate constraint parameter due to its independence of applied loads under fully plastic conditions or large-scale yielding. A wide range of constraint level is considered using five different types of specimen geometry and loading configuration; namely, compact tension (CT), three-point bend (TPB), single edge-notched tension (SENT), double edge-notched tension (DENT) and centre-cracked panel (CCP). The upper shelf initiation toughness J _IC, tearing resistance T _R and J–R curves tested by Joyce and Link (1995) for A533B steels using the first four specimens are analysed. Through finite element analysis at the applied load of J _IC, the values of A ₂ for all specimens are determined. The framework and construction of constraint-modified J–R curves using A ₂ as the constraint parameter are developed and demonstrated. A procedure of transferring the J–R curves determined from standard ASTM procedure to non-standard specimens or practical cracked structures is outlined. Based on the test data, the constraint-modified J–R curves are presented for the test material of A533B steel. Comparison shows the experimental J–R curves can be reproduced or predicted accurately by the constraint-modified J–R curves for all specimens tested. Finally, the variation of J–R curves with the size of test specimens is produced. The results show that larger specimens tend to have lower crack growth resistance curves.     

The relationship between Palmqvist indentation toughness and bulk fracture toughness for some WC-Co cemented carbides

The Palmqvist indentation toughness (W) has been determined for a series of WC-Co hardmetals containing up to 10 wt % cobalt. Using a correlative parameter (the cobalt mean-free path) the Palmqvist toughness has been compared with true fracture toughness data (G _IC values) for similar materials, obtained by conventional testing techniques. It has been shown that a linear relationship betweenW andG _IC can be predicted, on the basis of a recent theory of the fracture process in hardmetals. The validity of such a relationship has been experimentally confirmed, over a limited range of hardmetal compositions and microstructures. The experimental difficulties and expense associated with fracture toughness determination for brittle materials such as hardmetals, by quasi-conventional techniques, are well known. It is concluded that the Palmqvist test provides a useful method of measuring fracture toughness on a routine basis, since it is simple to perform, non-destructive, and does not require a specialized testpiece geometry. Its application in hardmetal quality control is, therefore, indicated.     

Specimen Size Requirements for Two-parameter Fracture Toughness Testing

Using a single parameter fracture mechanics theory, a minimum specimen size requirement of min(a, b, B) >200J/σ₀ in tension and min(a, b, B) >25J/σ₀ in bending, where B is the thickness, b the remaining ligament and a is the crack length of the specimen, were derived [Shih and German (1981), International Journal of fracture 17, 27–43] which have provided the basis for modern fracture toughness testing procedures. Two-parameter fracture toughness testing including the constraint, on the other hand, is desirable since it offers a solution to the transferability issue. A size requirement for a valid two-parameter fracture toughness testing based on the J-A₂ three-term solution was determined as min(a, b, B) > 11J/σ₀ [Chao and Zhu (1998), International Journal of fracture 89, 285–307] in which the limiting case is bend specimens under large scale yielding (LSY). Recent work by Chao et al. (2004, International Journal of fracture, 27, 283–302) has shown that the J-A₂ dominance at a crack tip can be significantly enhanced for bending specimens under LSY if a modified J-A₂ solution is adopted. This current paper further studies the size of the J-A₂ dominant zone using the modified J-A₂ solution for deep bend specimens with hardening from low to high and loading from SSY to LSY using finite element analysis. Based on the results, a rather relaxed specimen size requirement min(a, b, B) >6J/σ₀ is developed and recommended for a valid two-parameter fracture toughness testing using the J-A₂ fracture criterion. Validity of the size requirement is demonstrated by using the experimental J-R curves from non-standard bending specimens for A285 steel.     

Correction methods of an apparent negative crack growth phenomenon

It often occurs in J–R testing that some initial crack extension (a) data points have anomalous negative values. The reason for the apparent negative crack growth is due to the analysis method. The phenomenon as a possible source of error in determining J _IC or J–R curve from partial unloading compliance experiments may be eliminated by the compliance correction equation or the offset technique. In this study, new correction methods based on compliance correction and blunting behavior are proposed and verified by the measurement of the actual crack length and J _IC analysis.     

Study of the relationship between fracture toughness (J IC) and bulge ductility

A theoretical model relating fracture toughness expressed as J _IC and bulge ductility {ie71-1} for a material exhibiting linear elastic behavior at low temperature and elastic-plastic behavior at higher temperatures is proposed. This model shows a variation of J _IC with {ie71-2} for linear elastic behavior and J _IC with {ie71-3} for elastic-plastic behavior. The model contains three constants to be determined experimentally for a given material, specimen geometry and testing conditions. A case study on 1045 steel in the temperature range ?60 to 25°C confirms the validity of the model. The experimental results help in determining the size of the fracture zone ahead of the crack as well as the mechanisms for crack blunting and crack growth.     

A study on the ASTM E1921 standard in determining the fracture toughness of ferritic steels

One of the most important aims of the fracture mechanics is to determine the fracture toughness of a material. Various methods were developed for this purpose and have been still used nowadays. In the J‐integral method that is one of them, providing of a dominant linear elastic condition on the specimen is not required. However, in ferritic steels, the fracture toughness values (K_JC) obtained by the J‐integral method show some inconsistencies. Therefore, the ASTM E1921 standard was developed on ferritic steels, which are instabilities in the values of elastic or elastoplastic fracture toughness. In this study, a new method was used to determine the fracture toughness (K_IC) of ferritic steels, and it was compared with the standard. Three steels with different mechanical properties and average grain size were investigated in this study.     

Viscoelasticity of ceramics at high temperatures

The dependence of the fracture toughness, K _IC, on the loading rate has been calculated. On the basis of linear elastic fracture mechanics (LEFM) a strong dependence of the fracture toughness on the loading rate is obtained if subcritical crack growth is taken into account. If the subcritical crack growth parameters n and B are sufficiently small, which correspond to a high velocity of crack extension, the fracture toughness should decrease at lower loading rates. This behaviour is similar to the well-known decrease of bending strength. The experimental results for alumina containing glassy phase as a model material, however, show a maximum in a certain regime of loading rates. A model is established, which combines LEFM and the viscoelasticity, and leads to a maximum of K _IC at a certain loading rate dependent on the viscosity of the glassy phase.     

Limitations of elastic definitions in Al-Si-Mg cast alloys with enhanced plasticity: linear elastic fracture mechanics versus elastic-plastic fracture mechanics

Linear elastic fracture mechanics describes the fracture behavior of materials and components that respond elastically under loading. This approach is valuable and accurate for the continuum analysis of crack growth in brittle and high strength materials; however it introduces increasing inaccuracies for low-strength/high-ductility alloys (particularly low-carbon steels and light metal alloys). In the case of ductile alloys, different degrees of plastic deformation precede and accompany crack initiation and propagation, and a non-linear ductile fracture mechanics approach better characterizes the fatigue and fracture behavior under elastic-plastic conditions.To delineate plasticity effects in upper Region II and Region III of crack growth an analysis comparing linear elastic stress intensity factor ranges (ΔK_el) with crack tip plasticity adjusted linear elastic stress intensity factor ranges (ΔK_pl) is presented. To compute plasticity corrected stress intensity factor ranges (ΔK_pl), a new relationship for plastic zone size determination was developed taking into account effects of plane-strain and plane-stress conditions (“combo plastic zone”). In addition, for the upper part of the fatigue crack growth curve, elastic-plastic (cyclic J based) stress intensity factor ranges (ΔK_J) were computed from load-displacement records and compared to plasticity corrected stress intensity factor ranges (ΔK_pl). A new cyclic J analysis was designed to compute elastic-plastic stress intensity factor ranges (ΔK_J) by determining cumulative plastic damage from load-displacement records captured in load-control (K-control) fatigue crack growth tests. The cyclic J analysis provides the true fatigue crack growth behavior of the material. A methodology to evaluate the lower and upper bound fracture toughness of the material (J_IC and J_max) directly from fatigue crack growth test data (ΔK_FT(JIC) and ΔK_FT(Jmax)) was developed and validated using static fracture toughness test results. The value of ΔK_FT(JIC) (and implicitly J_IC) is determined by comparing the plasticity corrected elastic fatigue crack growth curve with the elastic-plastic fatigue crack growth curve. A most relevant finding is that plasticity adjusted linear elastic stress intensity factor ranges (ΔK_pl) are in remarkably good agreement with cyclic J analysis results (ΔK_J), and provide accurate plasticity corrections up to a ΔK corresponding to J_IC (i.e. ΔK_FT(JIC)). Towards the end of the fatigue crack growth test (above ΔK_FT(JIC)) when plasticity is accompanied by significant tearing, the cyclic J analysis provides a more accurate way to capture the true behavior of the material and determine ΔK_FT(Jmax). A procedure to decouple and partition plasticity and tearing effects on crack growth rates is given.Three cast Al-Si-Mg alloys with different levels of ductility, provided by different Si contents and heat treatments (T61 and T4) are evaluated, and the effects of crack tip plasticity on fatigue crack growth are assessed. Fatigue crack growth tests were conducted at a constant stress ratio, R = 0.1, using compact tension specimens.     

Temperature dependence of fracture toughness J IC and ductility for BCC materials in the transition region

The temperature dependence of ductility, strength and fracture toughness for a BCC material undergoing predominantly linear elastic behavior at low temperatures and elastic-plastic behavior at higher temperatures is examined. A model, based on ductile fracture mechanisms involving void nucleation followed by cavity growth and void coalescence, is developed to relate the fracture toughness parameter J _IC with temperature. Two general equations for linear elastic and elastic plastic regimes of J _IC versus temperature T, are obtained. Applications of this model to experimental data obtained on a carbon steel show that J IC varies with T ² at low temperatures and with T at higher temperatures, thus defining a transition temperature.