含铌微合金钢低温区静态软化行为

 通过两道次压缩变形实验对含Nb微合金钢静态软化行为进行了研究。结果表明：含Nb微合金钢静态再结晶临界温度随应变量增大而降低;随原始奥氏体晶粒尺寸增加而升高。温度高于静态再结晶临界温度时,含Nb微合金钢的静态再结晶激活能为常数(170589 kJ/mol);温度低于静态再结晶临界温度时,由于Nb的碳氮化物应变诱导析出,含Nb微合金钢的静态再结晶激活能为温度的函数,静态再结晶临界温度可通过再结晶激活能与温度倒数的关系曲线来确定。     

钒和铌-钒低碳微合金钢的静态再结晶行为

采用MMS-300热力模拟试验机研究了钒和铌-钒微合金钢的静态再结晶规律,绘制了试验钢的静态再结晶软化率曲线,计算出试验钢的静态再结晶激活能并建立了静态再结晶动力学模型,结合沉淀析出物的微观形貌观察,分析了铌对钒微合金钢静态再结晶行为的影响规律。结果表明,铌-钒钢的静态再结晶激活能要显著高于钒钢,在800~950℃变形保温60 s以上的试验条件下,铌-钒钢发生了形变诱导析出,细小的碳氮化物弥散分布在位错及晶界上,使得软化率曲线在此范围内出现"平台",说明铌既限制了静态再结晶的发生,又阻碍了软化行为的进行。     

一种钒氮微合金钢的静态再结晶行为

 通过双道次压缩试验,研究一种钒氮微合金钢道次间隔时间内在奥氏体区变形后的软化行为,采用应力补偿法计算静态再结晶的体积分数,并建立静态再结晶动力学模型。分析变形温度与间隔时间以及钒的析出物对静态软化行为的影响。结果表明,在高于900℃时进行第一道次变形,该钒氮微合金钢很快完成了静态再结晶;在850、800℃变形后的等温阶段,发生了形变诱导析出现象,使再结晶激活能增加,静态再结晶进程受到抑制,导致软化率曲线上出现了平台。     

两种同碳铌微合金化钢再结晶—析出沉淀交互作用的研究

本文绘制了碳氮含量相同、铌含量分别为0.024%和0.058%的两种微合金钢在应变分别为0.20和0.35条件下的再结晶-沉淀析出-时间-温度（RPTT）图。被称为“外推法”的方法被用来确定静态再结昌动力学曲线和绘制RPTT图。作为形变诱导析出行为的结果，在第一种钢的再结晶百分数-时间曲线图中观察到单个平台；第二种钢的这种曲线显示了双平台，以此的解释是用测热法来确认可能有两种形式的析出沉淀。本文使用透射电子显微技术显示在两种钢中形成的析出物形貌和最具有抑制再结晶能力的析出物尺寸。最后，对PRTT图的分析及其所具有的大量信息可提供用以设计一种更为合适的轧制制度，目的在于获得更细小的沉淀析出物和奥氏体→铁素体相变前更好的奥氏体显微组织。     

中碳铌微合金钢的应变诱导析出行为

通过应力松弛法验证了修正后的DS析出模型,得到了中碳铌微合金钢的应变诱导析出规律,结果表明:修改后的DS模型由于考虑了Si、Mn元素对碳氮化物应变诱导析出的影响,得到的PTT曲线与试验测得的曲线基本吻合,可用于Si、Mn含量较高的铌微合金钢应变诱导析出行为的预测;对于本试验用钢,PTT曲线具有典型的"C"型特征,鼻子温度在900℃左右,并且,随着应变速率的增大,PTT曲线左移,析出孕育期缩短。     

高Ti微合金钢热变形奥氏体的静态再结晶行为

在Gleeable-3800热/力模拟试验机上采用双道次压缩法,研究了一种高Ti微合金钢在奥氏体区变形后道次间隔时间内的静态软化行为,分析了变形温度和间隔时间对静态再结晶行为的影响规律,采用应力补偿法计算了静态再结晶分数。结果表明,变形温度、道次间隔时间对Ti微合金钢静态再结晶行为影响显著,变形温度越高,间隔时间越长,静态再结晶进行得越迅速;确定了Ti微合金钢的静态再结晶激活能为412.56 k J/mol,同时建立了静态再结晶动力学模型。     

钒微合金化对高锰TWIP钢热加工行为的影响

重点研究钒微合金化高锰(20%~30%)TWIP钢的静态软化和应变诱导析出行为,考察了不同钒含量(0.1%、0.2%)和碳含量(0.2%、0.6%、1%)的影响,目标是确定钒在热轧后还能有进一步析出强化作用的条件(如:成分、热加工参数)。在700~1100℃温度范围内进行了双道次扭转试验,还对卷取进行了模拟(从700℃到550℃)。采用先进的分析方法,如通过EBSD来确定晶粒尺寸和再结晶分数,采用TEM来分析析出物。结果表明,在热加工温度范围内,钒的析出相对迟缓,而且只在20%Mn-0.6%C-0.2%V或30%Mn-1%C-0.1%V的成分条件下发生。将碳含量降低到0.2%时,只在650℃和700℃模拟卷取后才能观察到析出物。另外,在有应变诱导析出发生的情况下,回复、再结晶和应变诱导析出之间有着复杂的相互影响。静态再结晶被明显推迟,导致回复对软化动力学具有重要影响。     

钒微合金钢中形变奥氏体的静态再结晶和诱导析出动力学

采用扭转试验和外推法，研究了三种不同含钒量的微合金钢形变奥氏体的静态再结晶动力学，建立了静态再结晶临界温度（ＳＲＣＴ）以上及其以下的温度模型。业已发现，ＳＲＣＴ是应变、奥氏体晶粒尺寸和现合金含量的函数，这里的微合金即指Ｎ和Ｖ。还对三种钢的应变诱导析出动力学进行了研究，测定了它们的析出－时间－温度（ＰＴＴ）曲线。测定了未再结晶温度（Ｔｎｒ），并得出结论，Ｔｎｒ和ＳＲＣＴ之间差异主要是由于奥氏体晶粒尺     

WNQ570桥梁钢的静态再结晶行为

 为了研究轧制工艺对WNQ570桥梁钢再结晶行为的影响,采用Gleeble-3500热模拟试验机模拟了其双道次热变形过程,测试了试验钢的应力-应变曲线,建立了静态再结晶晶粒体积分数随变形温度和道次间隔时间变化的关系模型,分析了应变诱导析出抑制对静态软化行为的影响。研究结果表明：静态再结晶体积分数随变形温度的提高或道次间隔时间的延长而增大,应变诱导析出抑制静态再结晶的进行;静态再结晶激活能为240.47kJ/mol。研究结果为制订试验钢二阶段控轧工艺提供了依据。     

微合金钢中微合金碳氮化物在奥氏体中的沉淀问题

微合金碳氮化物在奥氏体中的沉淀析出行为将对形变奥氏体的再结晶行为、奥氏体晶粒粗化行为以及在一定程度上对钢的沉淀强化行为产生显著的影响。本文探讨了微合金钢中M(CN)相析出的热力学、形核长大动力学、M(CN)相析出与晶体缺陷关系等重要基本理论问题,进行了系统的试验研究和     

铌钛复合微合金化对含磷冷轧结构钢板组织性能的影响

以低碳含磷钢为研究对象,通过分析不同卷取温度（600、650、700℃）时热轧态和冷轧退火态的显微组织、力学性能及退火再结晶动力学行为,对比研究了微铌（0．02％）处理和铌钛复合微合金化（0．02％Nb＋0．012％Ti）对钢的组织和性能的影响。研究结果表明,与微铌处理钢相比,铌钛复合微合金化钢在600℃卷取时析出物数量更多,在更高温度卷取时熟化速度更快,650℃卷取时即熟化到一定程度。低温（600℃）卷取时,铌钛复合微合金化钢的退火再结晶更难,800℃×30s连续退火可以保证完全再结晶。将温度继续升高至800℃以上,会导致强度下降,在一定程度上影响板卷之间的性能稳定性。     

Dynamic and Static Recrystallization Behavior of Low Carbon High Niobium Microalloyed Steel

 The recrystallization behavior of a low carbon high Nb microalloyed steel was investigated using Continuous and interrupted hot compression tests. The results showed that the onset of dynamic recrystallization (DRX) could be detected from inflection in the plot of the strain hardening rate θ against stress σ regardless of whether the stress peak appears or not. According to Zener-Hollomon parameter the activity energy of DRX (Qdef) was obtained, and a new modified expression calculating Qdef was proposed in consideration of the chemical composition of experimental steel. Applying the 2% offset method the static softening fraction was determined. The graphic representation of the softening fraction vs. interrupt time gave the information of the non-static recrystallization temperature (about 1000℃)and the relationship of precipitation-time-temperature. Static recrystallization kinetics follow Avrami’s law in high deformation temperature, and different values of the exponent n were given to illustrate the different effects of Nb element on static recrystallization at different deformation temperature.     

贝氏体非调质紧固件用钢静态再结晶行为分析

为分析贝氏体非调质紧固件用钢的静态再结晶行为,在Gleeble 3500热模拟试验机上进行了双道次压缩试验,并计算了静态再结晶软化率。研究表明,所研究钢种的奥氏体在1 050℃以上易于发生静态再结晶,在850℃以下静态再结晶发生困难;所确定的再结晶模型1可用于预测所研究钢种的静态再结晶的发生情况;利用道次间的静态再结晶细化奥氏体,适宜的轧制温度应控制在950~1 050℃,热机轧制温度应控制在850℃左右。     

Determination of Optimal Recrystallization Annealing Temperature of Nb-Ti Microalloyed High Strength IF Steel

The Nb-Ti microalloyed high strength IF steel sheet was used to study the effect of annealing temperature on the microstructures,mechanical properties and textures.The experimental results show that experimental steel is incomplete recrystallization at 750℃ annealing,but complete recrystallization from 780℃ to 870℃ under experimental conditions.When the annealing temperature was increased,the yield strength and tensile strength would gradually reduce,the plastic strain ratio and yield point elongation would gradually increase.The yield strength,tensile strength,elongation,the plastic strain ratio and the strain hardening exponent were approximate 300MPa,410MPa,36.5%,1.7 and 0.22 respectively under annealing temperature 810℃ to 840℃.When the annealing temperature was increased,the α-textures and γ-textures were gradually weakened,and the α-textures have a trend to {111} texture.Therefore,the suggestion of the optimal recrystallization annealing temperature is about 810℃ to 840℃ in industrial production.     

Dynamic and Static Recrystallization Behaviour of Coarse-grained Austenite in a Nb-V-Ti Microalloyed Steel简

The dynamic recrystallization （DRX） and static recrystallization （SRX） behaviour of coarse-grained aus- tenite in a Nb-V-Ti microalloyed steel were studied by using a Gleeble thermomechanical simulator. Continuous and interrupted compression tests of coarse-grained austenite were performed in the temperature range of 1000-1 150 ℃ at a strain rate of 0. 1- 5 s 1. The peak and critical strains for the onset of DRX were identified with strain hardening rate analysis, and the ratio of critical strain to peak strain was found to be consistent with the one reported for fine- grained austenite. An equation of the time for 50% softening was proposed by considering the activation energy of steel without microalloying elements and the solute drag effect of microalloying elements. Strain-induced precipitation may not take place at the deformation temperature above 1000 ℃, which indicates that SRX of coarse-grained aus- tenite is mainly retarded by coarse grain size and Nb in solution during rough rolling.     

热连轧生产船板钢E36静态再结晶行为研究

基于热模拟双道次压缩试验,研究了热连轧生产过程中船板钢E36奥氏体变形区不同变形温度、变形间隙时间内的软化行为,分析了变形温度和轧制变形间隙时间对静态再结晶软化率的影响,结果表明：变形温度是影响再结晶的最主要因素,在达到轧制变形温度时,随着轧制间隙时间的延长,再结晶软化率呈现逐步递增的趋势。通过金相分析,得出了最佳轧制...     

Recrystailization Behavior of Deformed Austenite in High Strength Microalloyed Pipeline Steel

Using methods of single-hit hot compression and stress relaxation after deformation on a Gleeble 1500D thermomechanical simulator,the curves of flow stress and stress relaxation,the microstructure and the recrystallization behavior of Nb-V-Ti high strength microalloyed low carbon pipeline steel were studied,and the influence of the thermomechanical treatment parameters on dynamic and static recrystallization of the steel was investigated.It was found that microalloying elements improved the deformation activation energy and produced a retardation of the recrystallization due to the solid solution and precipitation pinning.The deformation conditions such as deformation temperature,strain,and strain rate influenced the recrystallization kinetics and the microstructure respectively.Equations obtained can be used to valuate and predict the dynamic and static recrystallizations.     

Recrystallization Behavior of Deformed Austenite in High Strength Microailoyed Pipeline Steel

Using methods of single-hit hot compression and stress relaxation after deformation on a Gleeble 1500D thermomechanical simulator, the curves of flow stress and stress relaxation, the microstructure and the recrystallization behavior of Nb-V-Ti high strength microalloyed low carbon pipeline steel were studied, and the influence of the thermomechanical treatment parameters on dynamic and static recrystallization of the steel was investigated. It was found that microalloying elements improved the deformation activation energy and produced a retardation of the recrystallization due to the solid solution and precipitation pinning. The deformation conditions such as deformation temperature, strain, and strain rate influenced the recrystallization kinetics and the microstructure respectively. Equations obtained can be used to valuate and predict the dynamic and static recrystallizations.