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1.
硫酸预氧化难处理金矿石的工艺研究   总被引:2,自引:1,他引:1  
李德良  王淀佐 《黄金》1998,19(11):35-37
研究探讨了硫酸作为氧化剂,分解细粒浸染型含砷难处理金矿石的技术可能性。试验结果表明,硫酸可以有效地氧化砷黄铁矿而实现金的单体解离,适宜的分解条件为:硫酸与矿粉质量比=3,采用机械搅拌,反应温度240 ̄260℃,分解时间2 ̄3h,分解渣采用硫脲浸出时,浸金率高于95%。浸金条件为:硫脲质量分数1%,三价铁作氧化剂,OX/L(氧化剂与络合剂比值)=0.04 ̄0.06,浸出时间6h。  相似文献   

2.
原子吸收分光光度法测定粗铜中的金银   总被引:1,自引:0,他引:1  
试样经硝酸和王水溶解,在含HNO3的硫脲介质中直接喷测银。金则在2NHCI介质中用MIBK萃取,并经含(NH4)2HPO4的HCI溶液洗涤除铁后喷测。该法灵敏度高、准确性好.适用于粗铜中金银的测定。回收率金为95.0%~99.8%,银为98.6%~105%,结果令人满意,  相似文献   

3.
用螯合树脂回收铅阳极泥中的金   总被引:3,自引:0,他引:3  
何喜知  曹瑰华 《黄金》1998,19(5):34-36
对金含量较低(0 ̄100g/t)的铅阳极泥,用SO2直接从其金浸出液中还的金,回收率和纯度均较低。本文用螯合树脂吸附法富集微量金(0 ̄46mg/L)效果很好。吸附后溶液中金的浓度降至≤0.1mg/L,金的吸附率为99.7%。经解吸与还原,金的真收率为98% ̄99%。此外,从负阳极泥中回收银、锑、铋也取得较好结果。  相似文献   

4.
加温硫脲炭浸法提金新工艺研究   总被引:6,自引:1,他引:5  
张清波 《黄金》1993,14(12):23-27
广西龙水金矿浮选金精矿采用加温硫脲炭浸法提金新工艺处理,精矿金品位45.33g/t,硫脲用量6kg/t,金浸出率可达94。26%,金总回收率达90.28%.降低硫脲用量,提高金浸出率的重要条件是适当的温度,氧化剂,保护剂,吸附剂等诸因素的有机结合。  相似文献   

5.
刘虎生  李林荣 《黄金》1994,15(2):50-52
ICP-AES法测定矿渣中痕量金。称样5.000g于650℃灼烧后,用王水溶解,滤液通过TBP萃取树脂色谱柱吸附,0.1mol/LHC1+0.1mol/L硫脲混合淋洗液解脱。本法分析0.051g/t含量的金标样,结果与推荐值吻合。六次分析结果的相对标准偏差(RSD)<5%。回收率为96%~104%。方法简便,快速和准确。  相似文献   

6.
ICP-AES法测定矿渣中痕量金   总被引:1,自引:1,他引:0  
ICP-AES法测定矿渣中痕量金。称样5.0000g于650℃灼烧后,用王水溶解,滤液通过TBP萃取树脂色谱柱吸附,0.1mol/LHCl+0.1mol/L硫脲混合淋洗液解脱。本法分析0.051g/t含量的金标样,结果与推荐值吻合。六次分析结果的相对标准偏差(RSD)<5%。回收率为96%~104%。方法简便,快速和准确。  相似文献   

7.
本文研究硫脲法提金浸取液中连续测定硫脲(TU)与Fe(Ⅱ)离子的适宜浓度范围,酸度影响及指示剂使用量与校正等工作条件,建立了简便,快速,准确的连续测定方法,3~4min,完成两个元素次的分析,相对标准偏并分别低于0.1%与0.3%。  相似文献   

8.
本文介绍了采用非氰化浸出一特种树脂吸附湿法新工艺从硫酸浇渣中回收金的工业实践结果。采用简单设备,在矿浆浓度60%、温度60℃、〔h2SO4〕为1mol/L、〔NaClO3〕为5g/L、Eh保持在600 ̄700mV条件下进行搅拌浸出、用R410特种树脂进行吸附。饱和树脂用H2SO4溶液(0.1mol/L)洗涤、酸性硫脲溶液解吸,电解沉积Au,所得Au粉纯度〉99%,Au的总回收率达94%。该工艺流程  相似文献   

9.
含硫金矿的焙烧处理及硫脲浸金研究   总被引:6,自引:1,他引:5  
研究了含硫金矿经焙烧预处理后,以酸性硫脲溶液浸金的条件。结果表明,在助溶剂Re 1存在下,低品位的原生硫化金矿及高品位的浮选金精矿均可得到高于95 % 的金浸出率。得到了焙烧预处理、硫脲浸出难处理金矿的完整工艺,并试图解释硫化矿物的成分和结构是影响硫脲浸金效率的重要因素  相似文献   

10.
陈小燕  邵从和 《黄金》2000,21(2):46-47
含稀有贵金属铜料经高温焙烧后,混酸分解。在稀王水介质中,经聚氨脂泡沫塑料流动吸附,硫脲解脱后,于原子吸收光谱仪波长242.8nm处,以空气-乙炔火焰测量金的吸光度,按标准曲线法计算金量。该方法相对标准偏差为1.73%~6.85%,标准加入回收率为97.0%~101.7%。  相似文献   

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根据深云立交桥梁的检测结果,对该桥目前的整体状况、工作状态,及其使用情况做出综合评价,对桥的病害原因进行了分析,并提出合理的加固方案。  相似文献   

13.
劳伦斯小说《儿子与情人》一个鲜明的语言特色就是标准英语和当地方言频繁的语码转换。莫瑞尔用方言来对抗妻子,而妻子坚持用标准英语,偶尔也用方言来讽刺、挖苦丈夫。语码转换反映了劳伦斯男女二元对立的哲学思想。  相似文献   

14.
摘要:在第4次工业革命浪潮的推动下,钢铁科学与技术正在经历数字化、智能化转型。钢铁行业全流程各工序均为“黑箱”,为多场、多相、多变的巨系统,具有复杂相关关系和遗传效应等。这些不确定性带来了巨大的挑战。挑战和机遇并存。这些不确定性提供了智能化和数字化技术的应用场景资源;钢铁行业极为丰富的大数据提供了挖掘其中蕴含客观规律的数据资源;现代的数据科学、智能技术为解决不确定性问题提供了强大的手段。以数据为中心,以工业互联网为载体,以实验工具、数字数据、计算工具为支撑,建设钢铁企业材料创新基础设施,将可以大幅度提高研发效率,降低研发成本,有力地支撑钢铁材料科学与技术的转型发展。实验工具平台除了传统的实验室仪器装备和中试装备之外,实际生产线被作为主要的实验工具。这些实验工具提供丰富、精准、写实的历史数据和现实生产数据,特别是生产线装备提供实际生产大数据,蕴含着生产过程中的全部规律,是极宝贵的数据资源。利用机器学习、深度学习等现代数据挖掘技术为计算工具,对这些数据资源进行处理、分析、计算,将数据转换为高保真度模型,可以得到具有“原位分析能力”的数字孪生。在工业互联网的总体架构下,以数字孪生为核心,组成信息物理系统,构建起基于数据自动流动的状态感知、实时分析、科学决策、精准执行的闭环赋能体系,解决生产制造、应用服务过程中的复杂性和不确定性问题,提高资源配置效率,实现资源优化,对材料行业转型发展提供关键技术支撑。虚实映射、实时交互、精准控制的信息物理系统与材料创新基础设施合二为一,以材料创新基础设施为基盘,形成具有“原位分析能力”的数字孪生,建设钢铁生产全流程、一体化的信息物理系统,必将推进钢铁行业智能制造蓬勃开展和数字化、智能化转型。  相似文献   

15.
Social comparison involves positioning the self relative to others on a vertical or status dimension (ranging from upward to downward comparisons) and a horizontal or solidarity dimension (ranging from contrastive to connective comparisons). Across 3 studies in which 389 undergraduates recorded everyday social comparisons (n = 4,417), downward and connective comparisons were rated as more helpful and mood enhancing than upward and contrastive comparisons. The effects of horizontal comparisons were greater for people for whom solidarity was an important value; however, the effects of vertical comparisons were not greater for people who valued status. The roles of the comparison target, topic, and situation were also explored; for example, noticing undesirable features of the target enhanced status but undermined solidarity. (PsycINFO Database Record (c) 2010 APA, all rights reserved)  相似文献   

16.
Daniel Robinson suggests that much of the civil and criminal law "serves as the institutionalized form of praise and blame". Indeed it does. Pulling at this thread of Robinson's tapestry leads the reader straightaway to a host of truths about how law and morality not only intersect, but work together in harmony. "[L]aw", Robinson says, is a "vivid expression of deeper and impenetrably complex moral theories". This essay explores several of these harmonies, but focuses on two. One is that political society must be seen as the cooperation of free persons according to law, which persons hold common moral understandings. The second has to do with retribution as the moral justifying aim of punishing criminals. The author goes beyond Robinson's limited praise of retribution, and shows that some central features of our practice of punishment are understandable only within the retributive framework. (PsycINFO Database Record (c) 2010 APA, all rights reserved)  相似文献   

17.
Two studies investigated the role of expressive vocal behavior (specifically, speech rate and loudness) in fear and anxiety and in sadness and depression. In the 1st study, participants spoke about personally experienced fear and anxiety-arousing and neutral events using 3 different voice styles: fast and loud, normal, and slow and soft. In the 2nd study, participants spoke about personally experienced sad or depressing and neutral events using the same 3 voice styles. In both studies, the participants' highest levels of subjective affective and cardiovascular (CV) arousal occurred when they spoke about the emotional events in a mood-congruent voice style: fast and loud in the case of fear and anxiety, and slow and soft in the case of sadness or depression. Mood-incongruent voice styles canceled the heightened levels of CV arousal normally associated with these negative emotions. The voice-style manipulation had no significant effect on the participants' levels of CV arousal during the neutral discussions. (PsycINFO Database Record (c) 2010 APA, all rights reserved)  相似文献   

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为解决单个企业的信息化投资风险、从整体上降低企业信息化投入,针对大邱庄钢铁产业的类型特点,设计了一种新型信息化公共服务平台。详细阐述了钢铁产品展示及交易平台的建设内容及系统开发技术。该平台集产品展示、信息查询、用户管理功能于一体,实现了全自动、全智能的在线管理和维护,适用于中小型企业。该平台的应用最大化地发挥了大邱庄的产业优势,对大邱庄工业园区的宣传和市场开拓起到了一定的作用。  相似文献   

20.
The relationship between aging and negative affect is dynamic and complex. Although prior studies have often cited lower prevalence rates of anxiety and mood disorders among older individuals, these studies may miss the dynamic relationship between symptoms and aging. To evaluate a nonlinear model of the relationship between aging and negative affect, the author examined measures of neuroticism, anxiety, and depression symptoms in a cross-sectional, community sample (N = 335), ages 18 to 93. Results indicated a curvilinear relationship, with mean symptom levels increasing during early adulthood (until the mid-30s) and then showing a small decline until older adulthood (the mid-70s), when symptoms again increase with age. (PsycINFO Database Record (c) 2010 APA, all rights reserved)  相似文献   

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