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探讨了对纤维素酶法提取南瓜果胶效果有影响的两个杀青条件———温度和时间,并研究了优化工艺条件的放大过程。结果表明:杀青温度为85℃,杀青时间为20 min为最佳提取工艺,提取得率为14.3%。在放大15倍的实验中,提取得率为21.4%,这可能是由于放大实验中的测量误差减少所致。实验所得到的最佳果胶提取条件可以为综合利用南瓜提供一定的实验依据。 相似文献
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玉米芯中水溶性膳食纤维的微波预处理-超声波碱解法提取工艺研究 总被引:1,自引:0,他引:1
《应用化工》2017,(3)
采用正交实验对玉米芯中水溶性膳食纤维(SDF)的微波预处理-超声波碱解法提取工艺进行优化,以SDF得率为考察指标。结果表明,最佳微波预处理工艺超声波碱解法提取工艺条件为:原料粉碎粒度60目,解吸剂比7∶1 m L/g,微波功率560 W,微波时间150 s,Na OH浓度0.8%,液料比30∶1 m L/g,超声波功率200 W,提取温度50℃,提取时间35 min。该工艺条件下,SDF得率为4.75%。与超声波提取法相比,采用微波预处理并结合碱解法,可有效提高玉米芯中SDF的超声波提取效率。微波预处理-超声波碱法提取技术具有省时高效的特点,特别适用于玉米芯SDF的提取。 相似文献
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《应用化工》2022,(3)
采用正交实验对玉米芯中水溶性膳食纤维(SDF)的微波预处理-超声波碱解法提取工艺进行优化,以SDF得率为考察指标。结果表明,最佳微波预处理工艺超声波碱解法提取工艺条件为:原料粉碎粒度60目,解吸剂比7∶1 m L/g,微波功率560 W,微波时间150 s,Na OH浓度0.8%,液料比30∶1 m L/g,超声波功率200 W,提取温度50℃,提取时间35 min。该工艺条件下,SDF得率为4.75%。与超声波提取法相比,采用微波预处理并结合碱解法,可有效提高玉米芯中SDF的超声波提取效率。微波预处理-超声波碱法提取技术具有省时高效的特点,特别适用于玉米芯SDF的提取。 相似文献
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以荠菜为原材料,采用化学法制备不溶性膳食纤维和氨基酸。用酸水解法提取氨基酸,然后用碱提取法提取IDF,通过单因素实验和正交实验确定了不溶性膳食纤维制备的最佳工艺。提取荠菜IDF时,最适提取条件是碱液浓度为6%,碱浸温度为25℃,碱提取时间为20min,在此条件下提取荠菜IDF得率为71.6%,产品的持水力为658%、膨胀力为5.62mL/g。 相似文献
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超临界CO2和微波辅助萃取辽细辛挥发油 总被引:3,自引:0,他引:3
通过超临界CO2萃取辽细辛挥发油均匀设计实验和微波诱导萃取的正交实验比较,考察了影响提取的主要因素,得到了最佳萃取工艺. 超临界CO2萃取最佳工艺条件为:压力16 MPa,温度32oC,CO2流量20 kg/h和时间80 min,得率为3.78%;微波萃取最佳工艺条件为:辐射功率720 W,辐射时间50 s,溶剂用量300 ml,洗涤溶剂用量30 ml,得率为5.46%. 水蒸馏法提取率为1.62%. 结果表明,超临界CO2和水蒸馏法萃取辽细辛挥发油品质最好;微波萃取收率最高,但品质较差. 相似文献
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黑种草籽油的超临界CO_2萃取及其GC-MS分析 总被引:1,自引:0,他引:1
以新疆瘤果黑种草籽为原料,采用超临界CO2萃取技术(SFE-CO2)研究了瘤果黑种草籽油的萃取工艺,并对其化学成分进行了GC-MS分析。得到瘤果黑种草籽油较适宜的工艺条件为:萃取压力20 MPa,萃取温度35℃,萃取时间2 h,CO2流量20 kg/h。在该工艺条件下,黑种草籽油的得油率达36.33%。GC-MS检测出6种脂肪酸成分,主要为不饱和脂肪酸,其中,亚油酸质量分数60.95%,油酸质量分数20.54%,8,11-二十碳二烯酸质量分数2.43%,不饱和脂肪酸的质量分数近84%。 相似文献
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超临界CO_2萃取青皮挥发油的工艺研究 总被引:1,自引:0,他引:1
采用正交实验法对超临界CO2萃取中药青皮挥发油的最佳工艺条件进行优选。以挥发油得率为考察指标,探讨了萃取压力、萃取温度、萃取时间三因素在不同水平下对青皮挥发油得率的影响,并与水蒸气蒸馏法进行了比较。研究表明,萃取压力对挥发油得率有显著影响,萃取温度及时间影响不显著,各因素作用主次关系为:压力>温度>时间。优选得到的最佳工艺为:萃取压力25 MPa,萃取温度35℃,萃取时间1.5 h,得率为1.3197%,比水蒸气蒸馏法提高2.4倍,时间减少78.57%。超临界CO2萃取收率高、耗时短、品质好。 相似文献
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Extraction of essential oil from geranium (Pelargonium graveolens) with supercritical carbon dioxide
Amelia Peterson Siti Machmudah Bhupesh C Roy Motonobu Goto Mitsuru Sasaki Tsutomu Hirose 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》2006,81(2):167-172
This study investigated the supercritical fluid extraction (SFE) of geranium essential oil from geranium (Pelargonium graveolens) using supercritical carbon dioxide solvent. The extraction yield was measured as a function of pressure, temperature and carbon dioxide flow rate. At low pressure (10 MPa) and high temperature (343 K), waxes were co‐extracted with the essential oil, resulting in artificially elevated essential oil extraction yields as no method was available with the SFE apparatus used to separate co‐extracted waxes and oil. At high pressure (30 MPa) and low temperature (313 K), the amount of wax co‐extracted decreased. Under these ‘optimum’ conditions, the extraction yield increased with decrease in flow rate giving a maximum extraction yield of 2.53%. All samples were analyzed by gas chromatography–mass spectrometry and the effect of pressure and extraction time on oil composition was studied. The percentage compositions of terpene hydrocarbons, terpenols, geraniol and geranyl esters were significantly affected by pressure and extraction time. The oil samples obtained by SFE were also compared with commercially obtained steam distilled samples. All major components of the commercially obtained oils were present in the SFE‐obtained oils; however, the percentage composition of the major components differed greatly between steam distilled and SFE oils. Copyright © 2005 Society of Chemical Industry 相似文献
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Laboratory-Scale Optimization of Roasting Conditions Followed by Aqueous Extraction of Oil from Wild Almond
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Hooman Chodar Moghadas Karamatollah Rezaei 《Journal of the American Oil Chemists' Society》2017,94(6):867-876
The effects of roasting and aqueous extraction conditions for oil recovery from wild almond were optimized using response surface methodology (RSM). Optimum conditions for oil extraction were obtained at 142 °C roasting temperature, 16.5 min roasting time, 5.67 extraction pH and 4.6 h extraction time. Under these conditions, the extraction yield of 34.5% (w/w, based on the original weight of the sample) was obtained, which is equivalent to 80.0% of the total oil in the kernel. This was lower than that obtained by hexane Soxhlet (HS) extraction (43.1%, w/w, considered as 100% of total oil) but higher than that of cold pressing (CP) (18.5%, w/w; i.e., 42.9% of total oil). The refractive indices and saponification values of the oils were not affected by the extraction method. However, fatty acid and tocopherol compositions and DPPH radical scavenging capacities as well as unsaponifiable matter, iodine, peroxide and acid values of the obtained oils were impacted by the extraction method. The results showed that the quality attributes (omega-6 fatty acid content, peroxide and acid values, total tocopherol contents and antioxidant activity) of the oil obtained by AEP were somewhat similar to those of the oil extracted by CP and much superior to those of the oil obtained by HS. 相似文献