Cracking in the stir zones of Mg-alloy friction stir spot welds

Liquid penetration induced (LPI) cracking is investigated during friction stir spot weld of AZ91, AZ31 and AM60 magnesium alloys. A combination of stir zone temperature measurement and detailed metallography has revealed differences in the cracking tendencies of different magnesium alloys when the dwell time during spot welding is varied. LPI cracking in AZ91 spot welds involves the following sequence of events: the formation of eutectic films in the thermo-mechanically affected zone (TMAZ) region immediately adjacent to the stir zone extremity, engulfment of melted eutectic films as the stir zone width increases during the dwell period, penetration of α−Mg grain boundaries and crack propagation when torque is applied by the rotating tool. Cracking occurs early in the dwell period during AZ91 spot welding and almost the entire stir zone is removed when the rotating tool is withdrawn. However, crack-free AZ31 and AM60 spot welds are produced when a dwell time of 4 s is used since the stir zone temperatures are much higher than the α-Mg + Mg₁₇Al₁₂ eutectic temperature (437 °C) and melted eutectic films dissolve rapidly following their engulfment by the growing stir zone. In contrast, the temperature during the dwell period in AZ91 spot welding is close to 437 °C and melted eutectic films are not completely dissolved so that spot welds produced using a dwell time of 4 s exhibit LPI cracking.     

Local melting and tool slippage during friction stir spot welding of Al-alloys

Local melting and tool slippage during friction stir spot welding of different Al-alloy base materials is examined using a combination of detailed microscopy and temperature measurement. The stir zone peak temperature during welding is limited by either the solidus of the alloy in question or by spontaneous melting of intermetallic particles contained in the as-received base material. When spontaneous melting occurs this facilitates tool slippage at the contact interface. Accurate stir zone temperature and grain size measurements are essential elements when estimating the strain rate using the Zener–Hollomon relation. In Al 2024 and Al 7075 spot welds spontaneous melting of second-phase particles produces a drastic reduction in strain rate values. In Al 5754 and Al 6061 spot welds there is a strong correlation between tool rotational speed and estimated strain values. Local melted films dissolve rapidly in the high temperature stir zone and when the spot weld cools to room temperature following welding. Evidence of local melting is observed in Al 7075 friction stir spot welded joints made using a combination of rapid quenching, high plunge rates, and extremely short dwell time settings.     

Microstructural evolution and its effect on Hall-Petch relationship in friction stir welding of thixomolded Mg alloy AZ91D

Microstructural evolution of a thixomolded magnesium (Mg) alloy AZ91D during friction stir welding was investigated. Friction stir welding resulted in a homogeneous microstructure consisting of fine recrystallised -Mg grains in the thixomolded material. The microstructural homogenisation and refinement was attributed to dynamic recrystallisation accompanied by the dissolution of the eutectic structure during the welding. The grain refinement in the stir zone was effective in increasing the hardness, as predicted by the Hall-Petch equation. The effect of grain size on hardness was smaller than that in conventional and rapidly solidified AZ91. This phenomenon may be explained as being due to the microstructure of the stir zone which consisted of fine equiaxed grains with a high density of dislocations.     

Tool penetration during friction stir spot welding of Al and Mg alloys

The mechanism of tool penetration during friction stir spot welding of Al-alloy and Mg-alloy sheet materials is investigated and is explained as a progression of wear events, from mild wear to severe wear and then to melt wear in material beneath the base of the rotating pin. Melt wear can also occur under the rotating tool shoulder provided that sufficient penetration of the upper sheet occurs during the spot welding operation. The highest temperatures attained during FSW spot welding of Al 6111 and AZ91 base materials are close to the solidus temperatures of each base material and correspond with 0.94T_s (Al 6111) and 0.99 T_s (AZ91) where T_s is the solidus temperature of the material in degrees Kelvin.     

Influence of tool geometry and process parameters on macrostructure and static strength in friction stir spot welded polyethylene sheets

The effect of important welding parameters and tool properties that are effective on static strength in friction stir spot welds of polyethylene sheets were studied. Six different tool pin profiles (straight cylindrical, tapered cylindrical, threaded cylindrical, triangular, square and hexagonal) with different shoulder geometries, different pin length, pin angle and concavity angle were used to fabricate the joints. The tool rotational speed, tool plunge depth and dwell time were determined welding parameters. All the welding operations were done at the room temperature. Welding force and welding zone material temperature measurements were also done. Lap-shear tests were carried out to find the weld static strength. Weld cross section appearance observations were also done. From the experiments, the effect of pin profile, pin length, pin angle, dwell time and tool rotational speed on friction stir spot welding formation and weld strength was determined.     

Effect of welding parameters on the strain rate and microstructure of friction stir spot welded 2024 aluminum alloy

The stir zone microstructure, crystallographic texture, temperature and strain rate in the stir zones produced during Al 2024 spot welding using different tool rotational speed settings are investigated. The calculated strain rate during spot welding decreases from 1600 to 0.6 s⁻¹ when the tool rotational speed increases from 750 to 3000 rpm. The low strain rate values are associated with tool slippage resulting from spontaneous melting of S phase particles at temperatures ≥490 °C. However, the calculated strain rate is 1600 s⁻¹ in Al 2024 spot welds made using tool rotational speed of 750 rpm since the temperature never reaches 490 °C. Material transfers downwards via that pin thread during the dwell period in Al 2024 spot welding. It is proposed that this downward transfer of material provides a continuous supply of undissolved S phase particles, which melt spontaneously when the welding parameter settings produce stir zone temperatures ≥490 °C. A weak crystallographic texture where the {100} planes are oriented at about 45° to the θ-direction exists in the stir zones of spot welds made using different tool rotational speeds (from 750 to 3000 rpm). Another crystallographic texture where the {100} planes are parallel to the Z-direction (to the tool axis) is stronger in spot welds made using higher tool rotational speed settings. Also, material located at the root of the pin thread has a quite different crystallographic texture from that in the bulk of the stir zone.     

Microstructural evolution in AZ91D magnesium alloy during electron beam welding

Vacuum electron beam welding can have a low heat input, which means there is a minimum heat affected zone during welding of AZ91D magnesium alloy. From the observed microstructure, the weld of the AZ91D magnesium alloy can be divided into four regions, which are the weld metal zone, a partially-melted zone adjacent to the fusion boundary, a partially-melted zone adjacent to the base metal and the base metal zone. A sharp transition from the fusion zone to the non-melted zone, especially the characteristic partial melting microstructure and nature of the alloy elements, was observed. It was found that significant partial melting had taken place in the very narrow region around the weld metal of the AZ91D magnesium alloy. The Al content of eutectic β-Mg₁₇Al₁₂ in the partially-melted zone adjacent to the fusion boundary was close to the content in the continuously precipitated eutectic β particles in the fusion zone and much lower than the eutectic β in the base metal. The fully melted eutectic β-phase coexisted with the partially melted eutectic β phase in the partially-melted zone adjacent to the base metal.     

Material flow and mechanical behaviour of dissimilar AA2024-T3 and AA7075-T6 aluminium alloys friction stir welds

The scope of this investigation is to evaluate the effect of joining parameters on the mechanical properties, microstructural features and material flow of dissimilar aluminium alloys (3 mm-thick AA2024-T3 and AA7075-T6 sheets) joints produced by friction stir welding. Mechanical performance has been investigated in terms of hardness and tensile testing. Material flow using the stop action technique has also been investigated in order to understand the main features of the mixing process. No onion ring formation has been observed; the boundary between both base materials at the stir zone is clearly delineated, i.e., no material mixing is observed. A non-stable rotational flow inside the threads has been identified due to the formation of a cavity on the rear of the pin. Microstructural observation has revealed the development of a recrystallised fine-grained stir zone, with two different grain sizes resulting from the two different base materials.     

Microstructures and mechanical properties in dissimilar AZ91/AZ31 spot welds

The stir zone microstructures and mechanical properties of dissimilar AZ91/AZ31 friction stir spot welds made using different tool designs and tool rotational speed settings are investigated. Intermingled AZ91 and AZ31 lamellae are formed in the stir zones of dissimilar spot welds made using threaded, three-flat/0.7 mm/threaded and three-flat/no-thread tools and tool rotational speeds ranging from 1500 to 3000 rpm. The intermingled lamellae have chemical compositions, which are similar to those of the upper and lower sheets in the dissimilar sandwich. The flats on the rotating tool facilitate the downward transfer of upper and lower sheet materials in the location close to the pin periphery and therefore intermingled AZ91 and AZ31 lamellae are formed in the stir zones of dissimilar spot welds produced using a three-flat tool without a thread.The distance (Y) from the tip of the hook region to the keyhole periphery has a dominant influence on the mechanical properties of dissimilar AZ91/AZ31 spot welds, since the hook regions are curved inwards towards the axis of the rotating tool. The highest failure load properties and largest Y-values are found in dissimilar spot welds made using threaded and three-flat/0.7 mm/threaded tools and tool rotational speeds from 1500 to 3000 rpm. Dissimilar spot welds made using a rotational speed of 1000 rpm have the smallest Y-values and the lowest failure load properties.     

Local melting mechanism and its effects on mechanical properties of friction spot welded joint for Al-Zn-Mg-Cu alloy

Local melting and the eutectic film and liquation crack formation mechanisms during friction spot welding (FSpW) of Al-Zn-Mg-Cu alloy were studied by both experiment and finite element simulation. Their effects on mechanical properties of the joint were examined. When the welding heat input was high, the peak temperature in the stir zone was higher than the incipient melting temperature of the Al-Zn-Mg-Cu alloy. This resulted in local melting along the grain boundaries in this zone. In the retreating stage of the welding process, the formed liquid phase was driven by the flowing plastic material and redistributed as a “U-shaped” line in the stir zone. In the following cooling stage, this liquid phase transformed into eutectic films and liquation cracks. As a result, a new characteristic of “U” line that consisted of eutectic films and liquation cracks is formed in the FSpW join. This “U” line was located in the high stress region when the FSpW joint was loaded, thus it was adverse to the mechanical properties of the FSpW joint. During tensile shear tests, the “U” line became a preferred crack propagation path, resulting in the occurrence of brittle fracture.     

Microstructure and mechanical optimization of probeless friction stir spot welded joint of an Al-Li alloy

In this work, a third generation Al-Li alloy has been successfully spot welded with probeless friction stir spot welding (P-FSSW), which is a variant of conventional friction stir welding. The Box-Behnken experimental design in response surface methodology (RSM) was applied to optimize the P-FSSW parameters to attain maximum tensile/shear strength of the spot joints. Results show that an optimal failure load of 7.83 kN was obtained under a dwell time of 7.2 s, rotation speed of 950 rpm and plunge rate of 30 mm/min. Sufficient dwell time is essential for heat conduction, material flow and expansion of the stir zone to form a sound joint. Two fracture modes were observed, which were significantly affected by hook defect. In addition to mechanical testing, electron backscattering diffraction (EBSD) and differential scanning calorimetry (DSC) were used for microstructure evolution and property analysis. The precipitation of GP zone and Al₃Li as well as the ultrafine grains were responsible for the high microhardness in the stir zone.     

Microstructural characteristics and mechanical properties of non-combustive Mg–9Al–Zn–Ca magnesium alloy friction stir welded joints

Non-combustive Mg–9Al–Zn–Ca magnesium alloy was friction stir welded with rotation speeds ranging from 500 to 1250 rpm at a constant welding speed of 200 mm/min. Defect-free joints were successfully produced at rotation speeds of 750 and 1000 rpm. The as-received hot extruded material consisted of equiaxed α-Mg grains with β-Mg₁₇Al₁₂ and Al₂Ca compounds distributed along the grain boundaries. Friction stir welding produced much refined α-Mg grains accompanied by the dissolution of the eutectic β-Mg₁₇Al₁₂ phase, while Al₂Ca phase was dispersed homogeneously into the Mg matrix. An increase in rotation speed increased the α-Mg grain size but not significantly, while microstructure in the heat affected zone was almost not changed compared with the base material. The hardness tests showed uniform distributed and slightly increased harness in the stir zone. Results of transverse tensile tests indicated that the defect-free joints fractured at the base material, while longitudinal tensile tests showed that the strength of the defect-free welds was improved due to microstructural refinement and uniform distribution of intermetallic compounds.     

Strain path and microstructure evolution during severe deformation processing of an as-cast hypoeutectic Al–Si alloy

Microstructure evolution in an as-cast Na modified Al–7%Si (wt. pct.) alloy was examined during redundant and monotonic straining by repetitive equi-channel angular pressing (ECAP) under ambient temperature conditions, and during friction stir processing (FSP). Redundant straining during repetitive ECAP was accomplished by processing following route B_C while monotonic straining employed route A. Single- and multi-pass FSP was conducted on this same as-cast material using an FSP tool having a threaded pin. The as-cast microstructure comprises equiaxed primary α dendrite cells embedded in the Al–Si eutectic constituent. The evolution of this microstructure during repetitive ECAP can be described by idealized models of this process. The primary and eutectic constituents can still be discerned and the Si particle distribution is not homogenized even during ambient temperature processing involving von Mises strains >9.0. In contrast, the primary and eutectic constituents cannot be distinguished in the stir zone after even a single FSP pass. Strain estimates based on the shape change of the primary α constituent indicate that the Si particle distribution has become homogeneous at local von Mises strains of 2.5–3.0 during the FSP thermomechanical cycle. Mechanical property data are consistent with strain path during SPD processing by repetitive ECAP and FSP.     

Defect features and mechanical properties of friction stir lap welded dissimilar AA2024–AA7075 aluminum alloy sheets

5 mm-Thick dissimilar AA2024-T3 and AA7075-T6 aluminum alloy sheets were friction stir lap welded in two joint combinations, i.e., (top) 2024/7075 (bottom) and 7075/2024. The influences of process conditions (welding speed and joint combination) on defects (hook and voids) features and mechanical properties of joints were investigated in detail. It was found that the hook deflects largely upwards into the stir zone (SZ) at lower welding speeds (50, 150 mm/min) in both combinations. The process conditions significantly affect the hook geometry which in return affects the lap shear strength. In all 2024/7075 joints, voids appear and the joints fracture from the tip of hook on AS along the SZ/TMAZ (thermomechanically affected zone) interface in lap shear test (tensile fracture mode). In 7075/2024 joints, the hook on RS horizontally extends a large distance into the bottom stir zone at higher welding speeds (225, 300 mm/min). The joints fracture in three modes: shear fracture along the lap interfaces, tensile fracture and the mix fracture of both. In both joint combinations, the lap shear strength generally increases with the increase of welding speed. 7075/2024 Joints show higher failure load than 2024/7075 joints at lower welding speeds while the opposite result appears at higher welding speeds.     

Identification of the pin offset effect on the friction stir welding (FSW) via Taguchi – Grey relational analysis: A Case study for AA 7075 – AA 6013 alloys

The aim of this work is to present a case study relating to the dissimilar friction stir welding (FSW) ability of AA 7075‐T651 and AA 6013‐T6 by applying pin offset technique. An orthogonal array L18 was conducted to perform the overlapped weld seams using three different values of pin offset, welding speed and tool rotational speed along with two different pin profiles determine the impact of welding parameters on the tensile properties of friction stir welded joints. The nugget zone for each of overlapped weld seams exhibited a complex structure and also, the pin offset and profile also were found to have a great impact on the microstructural evolution of the nugget zone. The ultimate tensile strength, elongation at the rapture and bending strength of welded joints were measured in the ranges of 194–215 MPa, 1.79–3.34 % and 203–352 MPa. From the Taguchi based Grey relational analysis, the optimum welding condition was determined for the welded joint performed using a single fluted pin profile with the zero pin offset, tool rotational speed of 630 min^?1 and welding speed of 63 mm/min. Microstructural and macro‐structural observations revealed that welded joints exhibiting lower tensile strength are consistent of various types of defects (e. g. cracks, tunnels and cavities). The fracture location of welded joints was found to be on the heat affected zone and between the heat affected zone and AA 6013‐base metal. The tool and pin wear was not observed during the welding applications     

The time–temperature–corrosion susceptibility in a 7050-T7451 friction stir weld

The temperature gradient occurring for a short time during friction stir welding greatly affects the localized corrosion properties of welded 7050-T7451 plates. An immersion experiment in a salty solution was carried out in order to verify the influence of short-term post-weld heat treatments at temperatures similar to those taking place during friction stir welding on the corrosion behaviour of friction stir welded 7050-T7451. The experiment consisted of inserting thermocouples at different weld regions for the registration of the temperature development with time, and partially immersing the welded plate in a salty solution at 480 °C. In this manner, the weld experienced different temperature expositions at different locations. It was found that a temperature exposition above 180 °C for 20 min significantly increases the general corrosion resistance of friction stir welded 7050-T7451. The re-exposition of 7050-T7451 friction stir weld to a time–temperature combination similar to that occurring during the welding process on the thermomechanically heat affected zones of the weld, significantly improves the corrosion properties and the environmental cracking resistance. After the short-term temperature exposition, the fracture location of samples tested in a 3.5 wt.% NaCl solution moved from the corrosion susceptible thermomechanically affected zone to the heat affected zone.     

Role of plunge depth on the joint formation and mechanical behavior of Al6063-AZ91 dissimilar lap joint produced by friction stir welding

Dissimilar lap joint of Al6063 aluminium and AZ91 magnesium alloys was successfully produced by friction stir welding. Three different plunge depths (3.2 mm, 3.25 mm, and 3.3 mm) were adopted during welding. Similar Al6063–Al6063 lap joints were also produced along with the dissimilar Al6063–AZ91 joints for the purpose of comparing the joint formation. With the increased plunge depth, the width of the similar Al6063 - Al6063 lap joint was increased. On the contrary, joint width was decreased for the dissimilar joint with increased plunge depths. The dissimilar joint was formed with a strong metallurgical bonding between the Al6063 and AZ91 alloys, which is attributed to the mechanical mixing of these alloys in the nugget zone. Additionally, the formation of intermetallics was also observed from the x-ray diffraction analysis. The variations within the measured hardness values were higher at the joint interface due to the mixing of aluminium and magnesium alloys in the nugget zone. From the tensile shear tests, increased strength and decreased elongation were measured with the increased plunge depth. The results demonstrate the importance of the plunge depth on the lap joint formation between dissimilar Al6063–AZ91 alloys during friction stir welding.     

6082-T6回填式搅拌摩擦点焊热-流耦合分析

为了解释了回填式搅拌摩擦点焊的连接机理,本文根据6082-T6铝合金回填式搅拌摩擦点焊焊接过程的特点,建立了简化的热源模型,利用有限元分析软件ANSYS模拟出焊接过程中的温度场,进而耦合得到其应力场.结果表明:随着焊接过程的进行,铝合金6082-T6最高温度分布在袖筒1/2处,焊点处粘塑性金属的最大流动速度出现在铝合金上表面袖筒内侧区域;通过分析模拟过程中流体流动的流线与试验测量所得接头形貌照片,得到流场的分布规律.     

率相关材料在搅拌摩擦焊接过程中的行为分析

为研究金属粘性效应时的搅拌摩擦焊接材料流动行为,采用率相关本构描述搅拌摩擦焊接过程中的材料行为,并与非率相关材料模型的计算结果进行了对比.结果显示,由于考虑了金属的粘性效应.用率相关材料模型模拟搅拌摩擦焊接过程能更好地反映材料流动行为的本质.在搅拌摩擦焊接中,材料沿搅拌头切向方向的运动构成了搅拌摩擦焊接构件材料流动的主要形式.焊接构件-搅拌头接触面上的接触压力在搅拌头前方较大,在搅拌头后方较小,这一规律在率相关模型中更为明显.搅拌头前方材料在搅拌头的挤压之下向远离搅拌头的方向运动,而搅拌头后方的材料要填充由于搅拌头的移动而留下的空间,这一过程是保证搅拌摩擦焊接顺利完成的一个主要因素.因此,用率相关模型模拟搅拌摩擦焊接过程中的材料力学行为更为接近真实情况.     

Microstructure and tensile properties of friction welded aluminum alloy AA7075-T6

Solid-state welding processes like friction welding and friction stir welding are now being actively considered for welding aluminum alloy AA7075. In this work, friction welding of AA7075-T6 rods of 13 mm diameter was investigated with an aim to understand the effects of process parameters on weld microstructure and tensile properties. Welds made with various process parameter combinations (incorporating Taguchi methods) were subjected to tensile tests. Microstructural studies and hardness tests were also conducted. The results show that sound joints in AA7075-T6 can be achieved using friction welding, with a joint efficiency of 89% in as-welded condition with careful selection of process parameters. The effects of process parameters are discussed in detail based on microstructural observations.