Liquid–vapor structure near heating surface at high heat flux in subcooled pool boiling

Liquid–vapor behavior close to a heating surface was measured using two conductance probes with tip diameters smaller than 5 μm. Measurements were carried out for water boiling on an upward-facing copper surface under subcooling from 0 to 30 K. The probe signals and the void fraction distributions showed that there is little difference in the liquid–vapor structure beneath large vapor masses in saturated and subcooled boiling, that a macrolayer remains on the heating surface, and that in subcooled boiling it does not dry out even at heat fluxes far higher than CHF for saturated boiling. The thickness of the macrolayer forming beneath large vapor masses was determined from the location where the probe signals corresponding to the large vapor masses disappear. It was found that the thicknesses of the macrolayer formed in subcooled boiling are comparable to or thicker than those near the CHF in saturated boiling, and it is considered that this is most likely to be one of the causes why the CHF increases with the increasing subcooling.     

Temperature measurements near a heating surface at high heat fluxes in subcooled pool boiling

In previous papers (Int J Heat Mass Transfer, 2008;50:3481–3489, 2009;52: 814–821), the authors conducted measurements of liquid–vapor structures in the vicinity of a heating surface for subcooled pool boiling on an upward‐facing copper surface by using a conducting probe method. We reported that the macrolayer dryout model is the most appropriate model of the CHF and that the reason why the CHF increases with increasing subcooling is most likely that a thick macrolayer is able to form beneath large vapor masses and the lowest heat flux of the vapor mass region shifts towards the higher heat flux. To develop a mechanistic model of the CHF for subcooled boiling, therefore, it is necessary to elucidate the effects of local subcooling on boiling behaviors in the vicinity of a heating surface. This paper measured local temperatures close to a heating surface using a micro‐thermocouple at high heat fluxes for water boiling on an upward‐facing surface in the 0 to 40 K range of subcooling. A value for the effective subcooling, defined as the local subcooling during the period while vapor masses are being formed was estimated from the detected bottom peaks of the temperature fluctuations. It was established that the effective subcooling adjacent to the surface remains at considerably lower values than the bulk liquid subcooling. This suggests that, from nucleation to coalescence, the subcooling of a bulk liquid has a smaller effect on the behavior of primary bubbles than the extent of the subcooling would appear to suggest. An empirical correlation of the effective subcooling is proposed to provide a step towards quantitative modeling of the CHF for subcooled boiling. © 2009 Wiley Periodicals, Inc. Heat Trans Asian Res; Published online in Wiley InterScience ( www.interscience.wiley.com ). DOI 10.1002/htj.20277     

A new mechanistic model for pool boiling CHF on horizontal surfaces

This work proposes a new mechanistic model for predicting the critical heat flux (CHF) in horizontal pool boiling systems. It is postulated that when the vapor momentum flux is sufficient to lift the liquid macrolayer from the heating surface, wetting is no longer feasible, and a transition from nucleate to film boiling occurs. This is the same mechanism that has found success in predicting CHF in flow boiling systems. An experimental investigation of CHF with pentane, hexane, and FC-72 in saturated horizontal pool boiling with chamber pressures of 150, 300, and 450 kPa provides evidence that the new model captures the variation of CHF with pressure reasonably well compared with other well known models. The new model is also compared with existing data from the literature over a reduced pressure range of 2 × 10^?5–2 × 10^?1. The mean deviation between the predicted and measured CHF is typically within 20% over the parameter space covered.     

Boiling behaviors and critical heat flux on a horizontal plate in saturated pool boiling of water at high pressures

Observations of boiling behaviors and measurements of critical heat flux (CHF) were carried out for saturated water boiling on a horizontal, upward-facing plate at pressures from atmospheric to 7 MPa. The primary bubbles diminish in size almost in inverse proportion to pressure and commence to coalesce in the very low heat flux region. The diameter of detached coalesced bubbles increases with increases in the heat flux and reaches about 10 mm even at a pressure of 5 MPa. Detachment frequency of the coalesced bubbles was unaffected by the heat flux and pressure. The CHF predicted based on the macrolayer dryout model agrees well with the measured data.     

Non-linear dynamical analyses of transient surface temperature fluctuations during subcooled pool boiling on a horizontal disk

The class of dynamics in pool boiling on a large-size heater is assessed under subcooled pool boiling conditions. Transient surface temperature measurements are obtained using surface micro-machined K-type thin film thermocouples (TFT) in 10 °C subcooled pool boiling experiments on a 62.23 mm diameter silicon wafer using PF-5060 as the test liquid. Surface temperature data is obtained at each steady state condition to generate the boiling curve. The fraction of false-nearest neighbors, recurrence plots and space–time separation plots are obtained using the TISEAN package. The correlation dimension is then estimated from the re-constructed phase space data using a naïve algorithm. The correlation dimension varies from ～11.2 to 11.5 near onset of nucleate boiling (ONB), to ～7–10 in fully developed nucleate boiling (FDNB) ～7–9 near critical heat flux (CHF) condition, and from ～6.6 to 7.7 in film boiling. False-nearest neighbor estimates and recurrence plots show that nucleate boiling may be dominated by statistical processes near ONB and in partial nucleate boiling (PNB). In contrast, FDNB, CHF and film boiling seem chaotic and governed by deterministic processes.     

Macrolayer formation and mechanisms of nucleate boiling,critical heat flux,and transition boiling

The drying process of a macrolayer on a 15 mm diameter boiling surface was observed with high speed video in the region of nucleate and of transition boiling close to the critical heat flux (CHF). It was found that the macrolayer rests beneath a large vapor mass. It partially dries in nucleate boiling and completely dries in transition boiling at the detachment of the vapor mass. The macrolayer thickness at CHF and in transition boiling was determined on the basis of the energy balance relation proposed by Katto and Yokoya. The macrolayer thickness at low heat flux was obtained by decreasing CHF with downward-facing heating surfaces and agreed well with the correlation proposed previously by the present authors. The macrolayer thickness in transition boiling with a vertical surface also agrees fairly well with the correlation, when the heat flux at macrolayer formation, given on the nucleate boiling curve, is extrapolated to surface superheat of transition boiling and when the surface temperature at macrolayer formation is equal to a time-averaged value. © 1998 Scripta Technical, Heat Trans Jpn Res, 27(2): 155–168, 1998     

Study of the critical heat flux condition with water and R-123 during flow boiling in microtubes. Part I: Experimental results and discussion of parametric effects

Extensive experimentation was performed to obtain flow boiling critical heat flux data in single stainless steel microtubes with diameters from 0.286 to 0.700 mm over a wide range of mass fluxes, inlet subcoolings, and exit pressures for two different working fluids (water and R-123). The effect of different operating parameters – mass flux, inlet subcooling, exit quality, heated length and diameter – were assessed in detail (Part I of the paper). The conventional DNB-type behavior is observed in the high subcooled region, and the typical dryout type behavior is seen in the high-quality saturated region when the flow is completely annular. The flow in transitional flow patterns (churn–annular or slug–annular) causes a peculiar increase of CHF with exit quality. Also, the increased void fraction near the saturated region in subcooled boiling results in increased subcooled CHF values. Part II of the paper deals with comparison of data with existing correlations and development of a new correlation to predict the CHF condition in the subcooled liquid region.     

Enhanced boiling of HFE-7100 dielectric liquid on porous graphite

Enhanced boiling of HFE-7100 dielectric liquid on porous graphite measuring 10 mm × 10 mm is investigated, and results are compared with those for smooth copper (Cu) of the same dimensions. Although liquid is out-gassed for hours before performing the pool boiling experiments, air entrapped in re-entrant type cavities, ranging in size from tens to hundreds of microns, not only enhanced the nucleate boiling heat transfer and the critical heat flux (CHF), but also, the mixing by the released tiny air bubbles from the porous graphite prior to boiling incipience enhanced the natural convection heat transfer by ∼19%. No temperature excursion is associated with the nucleate boiling on porous graphite, which ensues at very low surface superheat of 0.5–0.8 K. Conversely, the temperature overshoot at incipient boiling on Cu is as much as 39.2, 36.6, 34.1 and 32.8 K in 0 (saturation), 10, 20 and 30 K subcooled boiling, respectively. Nucleate boiling ensues on Cu at a surface superheat of 11.9, 10.9, 9.5 and 7.5 K in 0 (saturation), 10, 20 and 30 K subcooled boiling, respectively. The saturation nucleate boiling heat flux on porous graphite is 1700% higher than that on Cu at a surface superheat of ∼10 K and decreases exponentially with increased superheat to ∼60% higher near CHF. The CHF values of HFE-7100 on porous graphite of 31.8, 45.1, 55.9 and 66.4 W/cm² in 0 (saturation), 10, 20 and 30 K subcooled boiling, are 60% higher and the corresponding superheats are 25% lower than those on Cu. In addition, the rate of increase in CHF with increased liquid subcooling is 50% higher than that on Cu.     

Correlation of critical heat flux and two-phase friction factor for subcooled convective boiling in structured surface microchannels

Critical heat flux (CHF) and pressure drop of subcooled flow boiling are measured for a microchannel heat sink containing 75 parallel 100 μm × 200 μm structured surface channels. The heated surface is made of a Cu metal sheet with/without 2 μm thickness diamond film. Tests and measurements are conducted with de-ionized water, de-ionized water +1 vol.% MCNT additive solution, and FC-72 fluids over a mass velocity range of 820–1600 kg/m² s, with inlet temperatures of 15(8.6)°C, 25(13.6)°C, 44(24.6)°C, and 64(36.6)°C for DI water (FC-72), and heat fluxes up to 600 W/cm². The CHF of subcooled flow boiling of the test fluids in the microchannels is measured parametrically. The two-phase pressure drop is also measured. Both CHF and the two-phase friction factor correlation for one-side heating with two other side-structured surface microchannels are proposed and developed in terms of the relevant parameters.     

Subcooled and saturated boiling of ammonia–lithium nitrate solution in a plate-type generator for absorption machines

This paper presents the experimental heat transfer evaluation during subcooled and saturated boiling of ammonia–lithium nitrate solution in a fusion plate heat exchanger, acting as a vapor generator under operating conditions representative of single-effect absorption machines. The solution flow rate and outlet temperature were modified in the ranges of 0.041–0.083 kg/s and 78–97 °C, respectively. The region where vapor bubbles begin to arise is estimated using a correlation for the wall superheat required for the onset of nucleate boiling. Results show that subcooled boiling is present in the generator. The initial boiling temperature is about 3.1 °C lower than the saturation temperature. The influence of the heat and mass fluxes on the boiling heat transfer coefficient is analyzed. The paper offers a correlation for the Nusselt number, including the subcooled and saturated boiling regions.     

Non-heating simulation of pool-boiling critical heat flux

This paper presents a non-heating experimental method that simulates the critical heat flux (CHF) phenomenon in pool boiling. In the experiments, with providing controlled air flow through the holes on a plate submerged in a pool of water, the liquid sublayer (macrolayer) thickness and bubble departure frequency have been successfully measured by a conductance probe. The CHF is reasonably predicted by applying the measured parameters to a liquid macrolayer dryout model. The measured trends of the macrolayer thickness and bubble departure frequency with air mass flux are also consistent with the present understanding. As a result of this experimental study, it is expected that the non-heating method would be useful to investigate the various parametric effects on pool and flow boiling CHF, with avoiding the difficulty in heating and large electric power requirement even for complex geometries.     

Effects of heater size and working fluids on nucleate boiling heat transfer

The present study is an experimental investigation of nucleate boiling heat transfer mechanism in pool boiling from wire heaters immersed in saturated FC-72 coolant and water. The vapor volume flow rate departing from a wire during nucleate boiling was determined by measuring the volume of bubbles from the wire utilizing the consecutive-photo method. The effects of the wire size on heat transfer mechanism during a nucleate boiling were investigated, varying 25 μm, 75 μm, and 390 μm, by measuring vapor volume flow rate and the frequency of bubbles departing from a wire immersed in saturated FC-72. One wire diameter of 390 μm was selected and tested in saturated water to investigate the fluid effect on the nucleate boiling heat transfer mechanism. Results of the study showed that an increase in nucleate boiling heat transfer coefficients with reductions in wire diameter was related to the decreased latent heat contribution. The latent heat contribution of boiling heat transfer for the water test was found to be higher than that of FC-72. The frequency of departing bubbles was correlated as a function of bubble diameters.     

Boiling enhancement by TiO2 nanoparticle deposition

TiO₂ nanoparticle-coated nickel wires were produced by electrical heating in various nanofluid concentrations ranging from 0.01 to 1 wt.% with various processing heat fluxes from 0 to 1000 kW/m². The experimental results demonstrated up to 82.7% enhancement on critical heat flux (CHF) in condition of coated nickel wire (processed in 1 wt.% with 1000 kW/m²) boiling in pure water. The contact angle measurement revealed that the hydrophilic porous coating formed by vigorous vaporization of TiO₂ nanofluid in nucleate boiling regime enormously modified the wettability of heating surface consequently improving the CHF. Besides, it is evident that the coverage of nanoparticle deposition tended to become more complete as concentration and processing heat flux increased based on SEM and EDS analysis. The nanoparticles dispersed in base fluid exhibited little effect on CHF enhancement and could even hinder the percentage of CHF augmentation from boosting, which demonstrated that one could enhance CHF by using only small amount of nanoparticles just adequate to form surface coatings instead of preparing working fluid with great bulk. However, according to the boiling curves in all cases of coated nickel wires, it is supposed that the nucleate boiling heat transfer coefficient deteriorates as a result of thermal resistance resulted from the occurrence of nanoparticle deposition. In summary, the coated porous structure of nanoparticles leads to enhance CHF and to decrease boiling heat transfer coefficient.     

Wall heat flux partitioning during subcooled forced flow film boiling of water on a vertical surface

Subcooled flow film boiling experiments were conducted on a vertical flat plate, 30.5 cm in height, and 3.175 cm wide with forced convective upflow of subcooled water at atmospheric pressure. Data have been obtained for mass fluxes ranging from 0 to 700 kg/m²s, inlet subcoolings ranging from 0 to 25 °C and wall superheats ranging from 200 to 400 °C. Correlations for wall heat transfer coefficient and wall heat flux partitioning were developed as part of this work. These correlations derive their support from simultaneous measurements of the wall heat flux, fluid temperature profiles, liquid side heat flux and interfacial wave behavior during steady state flow film boiling. A new correlation for the film collapse temperature was also deduced by considering the limiting case of heat flux to the subcooled liquid being equal to the wall heat flux. The premise of this deduction is that film collapse under subcooled conditions occurs when there is no net vapor generation. These correlations have also been compared with the data and correlations available in the literature.     

Measurements of critical heat flux and liquid–vapor structure near the heating surface in pool boiling of 2-propanol/water mixtures

Saturated pool boiling of 2-propanol/water mixtures on a 12 mm diameter horizontal disk under atmospheric pressure was investigated. The CHF of the mixtures increased up to 1.7 times the CHF of water at 3.0–4.7 mol% concentrations of 2-propanol. To examine the mechanism of the CHF enhancement in the mixtures, liquid–vapor structures close to the heating surface were measured using a conductance probe. It was found that in the boiling of the mixtures, liquid–vapor structures show strong non-uniformity in the radial direction of the heating surface. The void fractions at 0.1–1 mm above the heating surface are small at the central region and large near the periphery of the heating surface. The liquid layer between the vapor mass and the heating surface is considerably thicker than that of water at the central region and becomes thinner near the periphery of the heating surface. This thicker liquid layer is likely to be the cause of the CHF enhancement in the 2-propanol/water mixtures.     

Theoretical research of critical heat flux in subcooled impingement boiling on the stagnation zone

A new mechanism model for determination of the critical heat flux (CHF) in subcooled impingement boiling on the stagnation zone is proposed in this paper. It is based on the combination of the Helmholtz instability theory of macrolayer and the model of bubble induced turbulent heat transfer in subcooled impingement boiling. A semi-theoretical and semi-empirical correlation and its nondimensional form of the CHF for subcooled jet impingement boiling on the stagnation zone are also derived. Under the circumstances of CHF, the bubble induced turbulent heat transfer coefficient gets doubled as compared to the single-phase laminar heat transfer coefficient according to the theoretical model and the experimental data. And this kind of bubble induced turbulent heat transfer enhancing effect can be considered as a fixed ratio. The theoretical analysis result for the present case is successfully verified by the experimental result obtained on the smooth heating surface. Through the discussions, it is obtained that the CHF ratio of the subcooled jet impingement boiling against the saturated jet impingement boiling is theoretically related to the surface condition of the heater and the properties and impact velocity of the working fluid.     

An Experimental Investigation of Nucleate Pool Boiling Heat Transfer of Nanofluids From a Hemispherical Surface

An experimental investigation of nucleate pool boiling heat transfer is carried out using SiO₂ nanofluid in atmospheric pressure and saturated conditions. The results show that the nucleate boiling heat transfer coefficient (HTC) of the nanofluids is lower than that of deionized water, especially in high heat fluxes. In addition, the experimental results indicate that the critical heat flux (CHF) improves up to 45% with the increase of the nanoparticle volume concentration. Atomic force microscopy images from the boiling surface reveal that the nanoparticles are deposited on the heating surface during the nanofluid pool boiling experiments. It is found that the boiling HTC deteriorates as a result of the reduction in active nucleation sites and the formation of extra thermal resistance due to blocked vapor in the porous structures near the heating surface. Furthermore, the improvement of the surface wettability causes an increase in CHF. Based on the experimental investigations, it can be concluded that the changes in the properties of the boiling surface are mainly responsible for the variations in nanofluids boiling performance.     

Sorption and agglutination phenomenon of nanofluids on a plain heating surface during pool boiling

The pool nucleate boiling heat transfer experiments of water (H₂O) based and alcohol (C₂H₅OH) based nanofluids and nanoparticles-suspensions on the plain heated copper surface were carried out. The study was focused on the sorption and agglutination phenomenon of nanofluids on a heated surface. The nanofluids consisted of the base liquid, the nanoparticles and the surfactant. The nanoparticles-suspensions consisted of the base liquid and nanoparticles. The both liquids of water and alcohol and both nanoparticles of CuO and SiO₂ were used. The surfactant was sodium dodecyl benzene sulphate (SDBS). The experimental results show that for nanofluids, the agglutination phenomenon occurred on the heated surface when the wall temperature was over 112 °C and steady nucleated boiling experiment could not be carried out. The reason was that an unsteady porous agglutination layer was formed on the heated surface. However, for nanoparticles-suspensions, no agglutination phenomenon occurred on the heating surface and the steady boiling could be carried out in the whole nucleate boiling region. For the both of alcohol based nanofluids and nano-suspensions, no agglutination phenomenon occurred on the heating surface and steady nucleate boiling experiment could be carried out in the whole nucleate boiling region whose wall temperature did not exceed 112 °C. The boiling heat transfer characteristics of the nanofluids and nanoparticles-suspensions are somewhat poor compared with that of the base fluids, since the decrease of the active nucleate cavities on the heating surface with a very thin nanoparticles sorption layer. The very thin nanoparticles sorption layer also caused a decrease in the solid–liquid contact angle on the heating surface which leaded to an increase of the critical heat flux (CHF).     

Pool boiling characteristics of nanofluid on flat plate based on heater surface analysis

Nucleate pool boiling of Al₂O₃ based aqueous nanofluid on flat plate heater has been studied experimentally. For boiling of nanofluid (< 0.1 vol.%) on heating surface with ratio of average surface roughness to average diameter of particles much less than unity when boiling continue to CHF, the heat transfer coefficient of nanofluid boiling reduces while critical heat flux (CHF) increases. CHF enhancement increased with volume fraction of nanoparticles. Atomic force microscope (AFM) images from boiling surface showed that after boiling of nanofluid the surface roughness increases or decreases depending on initial condition of heater surface. Changes in boiling surface topology during different regions of boiling, wettability and thermal resistance of heater surface owing to nanoparticles deposition cause to variations in nanofluids boiling performance.     

Comparison study of liquid replenishing impacts on critical heat flux and heat transfer coefficient of nucleate pool boiling on multiscale modulated porous structures

The critical heat flux (CHF) and heat transfer coefficient of de-ionized (DI) water pool boiling have been experimentally studied on a plain surface, one uniform thick porous structure, two modulated porous structures and two hybrid modulated porous structures. The modulated porous structure design has a porous base of 0.55 mm thick with four 3 mm diameter porous pillars of 3.6 mm high on the top of the base. The microparticle size combinations of porous base and porous pillars are uniform 250 μm, uniform 400 μm, 250 μm for base and 400 μm for pillars, and 400 μm for base and 250 μm for pillars. Both the CHF and heat transfer coefficient are significantly improved by the modulated porous. The boiling curves for different kinds of porous structures and a plain surface are compared and analyzed. Hydrodynamic instability for the two-phase change heat transfer has been delayed by the porous pillars which dramatically enhances the CHF. The highest pool boiling heat flux occurring on the modulated porous structures has a value of 450 W/cm², over three times of the CHF on a plain surface. Additionally, the highest heat transfer coefficient also reaches a value of 20 W/cm² K, three times of that on a plain copper surface. The study also demonstrates that the horizontal liquid replenishing is equally important as the vertical liquid replenishing for the enhancement of heat transfer coefficient and CHF improvement in nucleate pool boiling.