Stability of the spectral responsivity of cryogenically cooled InSb infrared detectors

The spectral responsivity of two cryogenically cooled InSb detectors was observed to drift slowly with time. The origin of these drifts was investigated and was shown to occur due to a water-ice thin film that was deposited onto the active areas of the cold detectors. The presence of the ice film (which is itself a dielectric film) modifies the transmission characteristics of the antireflection coatings deposited on the active areas of the detectors, thus giving rise to the observed drifts. The magnitude of the drifts was drastically reduced by evacuating the detector dewars while baking them at 50 degrees C for approximately 48 h. All InSb detectors have antireflection coatings to reduce the Fresnel reflections and therefore enhance their spectral responsivity. This work demonstrates that InSb infrared detectors should be evacuated and baked at least annually and in some cases (depending on the quality of the dewar and the measurement uncertainty required) more frequently. These observations are particularly relevant to InSb detectors mounted in dewars that use rubber O rings since the ingress of moisture was found to be particularly serious in this type of dewar.     

Practical limit of the accuracy of radiometric measurements using HgCdTe detectors

The spectral responsivity of HgCdTe detectors operating in the thermal infrared region was observed to drift slowly with time. The characteristics of the drift were investigated and were shown to have a different origin from the drifts previously reported by one of the authors. Those drifts were caused by a thin film of water ice depositing on the active area of the cold detector. The source of the new drift is far more serious because it is fundamental, making the acquisition of accurate radiometric measurements with these detectors very difficult. It is demonstrated that the source of the new drift is the nonlinearity in the response of the HgCdTe detectors, coupled with the fluctuations of the irradiance reaching them. These fluctuations are due to variations in the thermal background caused by changes in the temperature of objects in the field of view of the detectors. This phenomenon is expected to provide a practical limit to the accuracy of radiometric measurements using not only HgCdTe detectors but also other detectors whose linearity is a function of the thermal background.     

Development of low-noise high value chromium silicide resistors for cryogenic detector applications

Extremely high sensitivity detectors, such as silicon bolometers are required in many NASA missions for detection of photons from the X-ray to the far infrared regions. Typically, these detectors are cooled to well below the liquid helium (LHe) temperature of 4.2 K to achieve the maximum detection performance. As photodetectors, they are generally operated with a load resistor and a pre-set bias voltage, which is coupled to the input gate of a source-follower field effect transistor (FET) circuit. It is imperative that the detector system signal-to-noise performance be limited by the noise of the detector and not by the noise of the external components. The load resistor value is selected to optimize the detector performance. These two criteria tend to be contradictory in that these detectors require load resistors in the hundreds of megaohms, which leads to a higher Johnson noise. Additionally, the physical size of the resistor must be small for device integration as required by such missions as the NASA High Resolution Airborne Wide-Band Camera instrument and the Submillimeter High-Angular Resolution Camera for the Caltech Submillimeter Observatory, both of which employ 384 detectors and resistors. We have designed, fabricated and characterized thin film resistors using a CrSi/TiW/Al metal system on optical quality quartz substrates. The resistor values range from 75 MΩ to over 650 MΩ and are Johnson noise limited to below LHe temperatures. The resistor film is sputtered with a sheet resistance ranging from 300 to 1600 Ω/□ and the processing sequence developed for these devices allows for chemically fine-tuning the sheet resistance in situ. The wafer fabrication process was of sufficiently high yield (>80%) providing clusters of good resistors for integrated multiple detector channels, a very important feature in the assembly of these two instruments.     

AC-Mode Short-Wavelength IR Radiation Thermometers for Measurement of Ambient Temperatures

Recent improvements in the fabrication of short-wave infrared (SW-IR) quantum detectors have opened a new era in radiation thermometry. Ambient and higher temperatures can be measured with low uncertainties using thermoelectrically (TE) cooled extended-InGaAs (E-IGA) and short-wave photovoltaic-HgCdTe (SW-MCT) detectors. Since these detectors have low cut-off wavelengths (2.5 μm and 2.8 μm, respectively), they do not respond past cut-off and are less sensitive to the background infrared radiation, resulting in orders of magnitude lower background noise than traditional broad-band infrared detectors such as cryogenically cooled quantum detectors or thermal detectors. At the same time, the cut-off is far enough in the infrared to obtain a large enough signal from the source of interest. Because of the low detector cut-off wavelength, traditional glass-based optics can be used in the radiation thermometers. A chopper-produced alternating-current (AC) signal was used to measure low temperatures by separating the AC signal from the background-radiation-produced direct-current (DC) signal and its fluctuations. Design considerations and characteristics of a newly developed SW-IR radiation thermometer are discussed. A noise-equivalent temperature difference (NETD) of < 3mK for a 50°C blackbody was measured. At the human body temperature of 36°C, the obtained NETD of ~10mK indicates that these detectors can be used in non-contact temperature measurements to replace thermopile- or pyroelectric-based radiation thermometers.     

Design,fabrication and test of Load Bearing multilayer insulation to support a broad area cooled shield

Improvements in cryogenic propellant storage are needed to achieve reduced or Zero Boil Off of cryopropellants, critical for long duration missions. Techniques for reducing heat leak into cryotanks include using passive multi-layer insulation (MLI) and vapor cooled or actively cooled thermal shields. Large scale shields cannot be supported by tank structural supports without heat leak through the supports. Traditional MLI also cannot support shield structural loads, and separate shield support mechanisms add significant heat leak. Quest Thermal Group and Ball Aerospace, with NASA SBIR support, have developed a novel Load Bearing multi-layer insulation (LBMLI) capable of self-supporting thermal shields and providing high thermal performance.We report on the development of LBMLI, including design, modeling and analysis, structural testing via vibe and acoustic loading, calorimeter thermal testing, and Reduced Boil-Off (RBO) testing on NASA large scale cryotanks.LBMLI uses the strength of discrete polymer spacers to control interlayer spacing and support the external load of an actively cooled shield and external MLI. Structural testing at NASA Marshall was performed to beyond maximum launch profiles without failure. LBMLI coupons were thermally tested on calorimeters, with superior performance to traditional MLI on a per layer basis. Thermal and structural tests were performed with LBMLI supporting an actively cooled shield, and comparisons are made to the performance of traditional MLI and thermal shield supports. LBMLI provided a 51% reduction in heat leak per layer over a previously tested traditional MLI with tank standoffs, a 38% reduction in mass, and was advanced to TRL5. Active thermal control using LBMLI and a broad area cooled shield offers significant advantages in total system heat flux, mass and structural robustness for future Reduced Boil-Off and Zero Boil-Off cryogenic missions with durations over a few weeks.     

Properties of Indium Antimonide Detectors for use as Transfer Standards for Detector Calibrations

The properties of 4-mm-diameter and 7-mm-diameter liquid-nitrogen-cooled indium antimonide detectors were investigated to determine their suitability as transfer standards (i.e., reference detectors) for the detector calibration facility at the National Research Council of Canada. The spectral responsivity of the InSb detectors in the spectral range 1000-3000 nm was determined by atwo-step procedure involving the use of germanium transfer standardsand suitably characterized thermopiles. It is shown that thelong-term reproducibility of the InSb detector calibrations is approximately ?1%. The uniformity and linearity as a function of wavelength, as well as the background current noise and drift of thetwo detectors, are compared. It is shown that the 7-mm-diameter detector is clearly superior to the 4-mm one for use as a transfer standard. It is estimated that the overall accuracy of the calibrations of the two InSb detectors is ?2% in the range 1200-2800 nm.     

Stirling Cryocooler for High-Temperature Super Conductor RF Filters

The High Temperature Super Conducting (HTSC) radio frequency (RF) filters (as used, for example, in ground base stations for cellular phone systems) are passive devices. To operate properly, they must be cooled well below their transition temperature to super conducting stage (usually to 65–80 K). These HTSC RF filters are connected through a coaxial cable to an array of Low Noise Amplifiers (LNA), which are active devices and, therefore, induce a few hundreds mWatts of heat. On the other hand, the LNA array is connected by coaxial cable to a feedthrough of the vacuum chamber. This coaxial cable also contributes a few hundreds mWatts of heat load. The third source of heat load is the thermal radiation from the vacuum jacket wall to the cryogenically cooled surfaces. This portion of heat load is assessed as hundreds of mWatts as well. The signal-to-noise ratio of LNA devices is improved significantly when they are cooled down to a temperature of 90–110 K and their effectiveness reaches 99% at a temperature of 77 K. Traditionally, cooling of the system is achieved by placing both the HTSC RF filters and the LNA array device on the cold tip of a single-stage cryogenic cooler. Hence, both devices are cooled down to a temperature of 60–80 K, which is required by the manufacturers of HTSC RF filters. Because of the high level of heat loads induced by the LNA array, this method requires an extra cooling capacity from a cryogenic cooler. This increases power consumption, weight, and size and decreases its reliability. This paper describes a method of reducing the overall heat load. This method relies on the idea of maintaining the HTSC RF filters and the LNA arrays in different operational temperatures. The objective of this method is to provide a reduction in thermal losses, input power, weight, and size and to increase the reliability of the entire cryogenic cooler. The method allow for better ruggedising of the mechanical support for cooled electronic package of the LNA array plate.     

Cooled infrared filters and dichroics for the James Webb Space Telescope Mid-Infrared Instrument

The cooled infrared filters and dichroic beam splitters manufactured for the Mid-Infrared Instrument are key optical components for the selection and isolation of wavelengths in the study of astrophysical properties of stars, galaxies, and other planetary objects. We describe the spectral design and manufacture of the precision cooled filter coatings for the spectrometer (7 K) and imager (9 K). Details of the design methods used to achieve the spectral requirements, selection of thin film materials, deposition technique, and testing are presented together with the optical layout of the instrument.     

Filter-protected photodiodes for high-throughput enzymatic analysis

This paper relates to the use of a thin film of re-crystallized (polycrystalline) silicon as a low-pass rejection filter in the ultraviolet light range and, more particularly, to the use of this layer as a protective layer for semiconductor diodes. The polycrystalline silicon filters were fabricated by laser annealing a thin film of amorphous silicon deposited by an LPCVD process. A standard component of the polysilicon-gate CMOS process is the boron phosphor silicate glass (BPSG) planarization layer. Since this layer is always applied, the possibility of using it as the isolator between the diode and the filter (and, thereby, omit one SiO/sub 2/ layer) is considered. Using scanning electron microscopy, we compared the crystallization process of the LPCVD silicon film deposited on a glass substrate and on a BPSG layer. The fabrication and the characterization of the filter-protected photodiodes are described in the paper.     

Effect of Cryogenic Cooling of Tool Electrode on Machining Titanium Alloy (Ti–6Al–4V) during EDM

The discharge characteristics and discharge gap of machining Ti–6Al–4V titanium alloy by cryogenically cooled tool electrode electrical discharge machining (EDM) in distilled water were investigated in this study using the monopulse discharge method. The influence of the cryogenically cooled tool electrode on the discharge gap and the initial maintaining voltage between the electrode and workpiece were analyzed under various temperatures. Test results showed the initial maintaining voltage of the cryogenically cooled tool electrode EDM was lower than that of conventional EDM. The discharge gap of the cryogenically cooled tool electrode EDM was also smaller than that of conventional EDM, which improved the copying accuracy of die-sinking EDM. A comparative experiment of machining Ti–6Al–4V titanium alloy was carried out by using cryogenically cooled tool electrode EDM and conventional EDM, lower electrode wear, higher material removal ratio, and higher corner size machining accuracy was obtained by using cryogenically cooled tool electrode EDM.     

Self-Cleaning Transparent Dust Shields for Protecting Solar Panels and Other Devices

The development of transparent flexible dust shields using both single- and three-phase electrodynamic shields is reported here for possible application on Mars and Earth to minimize obscuration of solar panels from the deposition of dust. The electrodynamic screens (EDS) are made of transparent plastic sheets, such as polyethylene terephthalate (PET) for its UV radiation resistance, and a set of parallel conducting electrodes made of transparent indium tin oxide (ITO) embedded under a thin transparent film. The basic principle of EDS operation, a simplified mathematical model of particle trajectories, the experimental setup used for testing the screens, and their dust removal efficiencies (DRE) are described. Results of our measurements on dust removal efficiency of EDS as a function of the particle size and electrostatic charge distributions of Mars simulant dust are reported. The results show that the EDS technology has a strong potential for protecting solar panels against dust hazards with DRE higher than 80% for dust. The power requirements will be approximately 10 watts per square meter of the panels when cleaning is needed.     

High-performance infrared narrow-bandpass filters for the Indian National Satellite System meteorological instrument (INSAT-3D)

This paper describes the design and manufacture of a set of precision cooled (210 K) narrow-bandpass filters for the infrared imager and sounder on the Indian Space Research Organisation (ISRO) INSAT-3D meteorological satellite. We discuss the basis for the choice of multilayer coating designs and materials for 21 differing filter channels, together with their temperature-dependence, thin film deposition technologies, substrate metrology, and environmental durability performance.     

Self-Cleaning Transparent Dust Shields for Protecting Solar Panels and Other Devices

The development of transparent flexible dust shields using both single- and three-phase electrodynamic shields is reported here for possible application on Mars and Earth to minimize obscuration of solar panels from the deposition of dust. The electrodynamic screens (EDS) are made of transparent plastic sheets, such as polyethylene terephthalate (PET) for its UV radiation resistance, and a set of parallel conducting electrodes made of transparent indium tin oxide (ITO) embedded under a thin transparent film. The basic principle of EDS operation, a simplified mathematical model of particle trajectories, the experimental setup used for testing the screens, and their dust removal efficiencies (DRE) are described. Results of our measurements on dust removal efficiency of EDS as a function of the particle size and electrostatic charge distributions of Mars simulant dust are reported. The results show that the EDS technology has a strong potential for protecting solar panels against dust hazards with DRE higher than 80% for dust. The power requirements will be approximately 10 watts per square meter of the panels when cleaning is needed.     

SeaWiFS on-orbit gain and detector calibrations: effect on ocean products

The NASA Ocean Biology Processing Group's Calibration and Validation Team has analyzed the mission-long Sea-Viewing Wide Field-of-View Sensor (SeaWiFS) on-orbit gain and detector calibration time series to verify that lunar calibrations, obtained at nonstandard gains and radiance ranges, are valid for Earth data collected at standard gains and typical ocean, cloud, and land radiances. For gain calibrations, a constant voltage injected into the postdetector electronics allows gain ratios to be computed for all four detectors in each band. The on-orbit lunar gain ratio time series show small drifts for the near infrared bands. These drifts are propagated into the ocean color data through the atmospheric correction parameter epsilon, which uses the 765/865 nm band ratio. An anomaly analysis of global mean normalized water-leaving radiances at 510 nm shows a small decrease over the mission, while an analysis of epsilon shows a corresponding increase. The drifts in the lunar time series for the 765 and 865 nm bands were corrected. An analysis of the revised water-leaving radiances at 510 nm shows the drift has been eliminated, while an analysis of epsilon shows a reduced drift. For detector calibrations, solar diffuser observations made by the individual detectors in each band allows the response of the detectors to be monitored separately. The mission-long time series of detector calibration data show that the variations in the response of the individual detectors are less than 0.5% over the mission for all bands except the 865 nm band, where the variations are less than 1%.     

Ag-assisted CBE growth of ordered InSb nanowire arrays

We present growth studies of InSb nanowires grown directly on [Formula: see text] and [Formula: see text] substrates. The nanowires were synthesized in a chemical beam epitaxy (CBE) system and are of cubic zinc blende structure. To initiate nanowire nucleation we used lithographically positioned silver (Ag) seed particles. Up to 87% of the nanowires nucleate at the lithographically pre-defined positions. Transmission electron microscopy (TEM) investigations furthermore showed that, typically, a parasitic InSb thin film forms on the substrates. This thin film is more pronounced for InSb((111)B) substrates than for InAs((111)B) substrates, where it is completely absent at low growth temperatures. Thus, using InAs((111)B) substrates and growth temperatures below 360?°C free-standing InSb nanowires can be synthesized.     

彩色冷反光镜的斜入射效应与补偿设计

讨论了斜入射对薄膜的光学特性的影响，提出了呈椭球旋转面的彩色冷反光镜膜层的均匀分布不同行于平行平面薄膜的均匀分布，在同一圆周方向上的膜层分布应均匀等厚，而从镜底到到镜口的轴向方向膜层应逐渐加厚。     

Monitoring the arbitrary thickness of optical thin films and their error simulation: a method

This paper was the method of monitoring the absolute value for film layer transmittance to monitor the thickness of optical thin film. For this purpose, a 2S3G double-color three-path monitoring apparatus was built. Simulation analyses of monitoring errors have been conducted and a flow diagram is given. Using this method and apparatus, 9-, 15-, and 23-layer broadband neutral dichroic filters, cold light coatings, edge filters, and polarizers have been plated; good reproducibility and satisfactory results have been obtained, thereby achieving the preparation of the non-lambda/4 multilayer system     

High-performance silicon photonics technology for telecommunications applications

By way of a brief review of Si photonics technology, we show that significant improvements in device performance are necessary for practical telecommunications applications. In order to improve device performance in Si photonics, we have developed a Si-Ge-silica monolithic integration platform, on which compact Si-Ge–based modulators/detectors and silica-based high-performance wavelength filters are monolithically integrated. The platform features low-temperature silica film deposition, which cannot damage Si-Ge–based active devices. Using this platform, we have developed various integrated photonic devices for broadband telecommunications applications.     

Variable narrow-band transmission filters for spectrometry from space. 2. Fabrication process

The optical components described here are variable narrow-band transmission filters, where the transmittance peak varies with the position along the surface of the filter itself. They allow the construction of ultracompact and low-weight spectrometers for space applications. The theoretical behavior of graded filters has been already investigated by the authors, for imaging spectrometry of the Earth surface. The application of graded filters to miniaturized instruments for planetary missions (Mercury) is considered. Experimental results on the fabrication of small-dimension variable transmission filters operating over a wide spectrum, from visible to near infrared, are reported.     

Surface enhanced absorption and transmission from dye coated gold nanoparticles in thin films

Absorption spectra of gold nanoisland thin film and the composite film of gold having thin coating of Methylene Blue and Rh6G dyes have been studied. Thin gold nanoisland film shows surface plasmon resonance (SPR) peak in the visible wavelength range, which shifts to near infrared with an increase in the thickness of the film. It was found that thin film of gold consists of nanoparticles of different size and shape, particularly nanorods of noncylindrical shapes. A linear relation was found between SPR peak wavelength and the aspect ratio of the nanoparticles in gold thin film. Effective medium refractive index of the gold film is estimated to be ~2.5, which decreases with an increase in film thickness. The coating of dyes on gold films splits the SPR peak with an enhanced absorption. Enhancement in absorption of composite film is maximal when the dye absorption peak coincides with the SPR peak; otherwise enhancement in transmission is observed for all the wavelength range. Absorption amplitude of composite film peaks increase with an increase in the gold film thickness, which tend toward saturation for film thickness of ≥6 nm. A correlation shows that absorption spectra can be described by the Maxwell Garnett theory, when the gold nanoparticles have a nearly spherical shape for very thin film (≤6 nm).