共查询到20条相似文献,搜索用时 15 毫秒
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Daniele Passeri Ugo Sassi Andrea Bettucci Emanuela Tamburri Francesco Toschi Silvia Orlanducci Maria Letizia Terranova Marco Rossi 《Advanced functional materials》2012,22(14):2956-2963
The thermoacoustic effect of isolated single‐wall carbon nanotubes aligned between electrodes is experimentally observed for the first time by imaging the emitted acoustic wave using an atomic force microscopy‐based technique specifically developed for the task. The capability of such a technique for single‐point thermoacoustic measurements is first verified on carbon nanotubes layers with two electrodes for injecting alternate electric current. The technique is then demonstrated to allow the acquisition, simultaneously with the topography, of images reflecting the pressure of the acoustic wave at fixed distance from the sample. Such a capability is used to collect images reflecting the amplitude of acoustic waves generated by isolated nanotubes and nanotube bundles by the thermoacoustic effect. 相似文献
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The origin of artifacts in atomic force microscopy is discussed. They are classified by basic distinct features. Various solutions to this problem are suggested using the literature data. Metrological issues of the problem are touched upon. 相似文献
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Astankova K. N. Kozhukhov A. S. Gorokhov E. B. Azarov I. A. Latyshev A. V. 《Semiconductors》2018,52(16):2081-2084
Semiconductors - Metastable germanium monoxide (GeO) thin-insulating films have been investigated as a new promising material for atomic force microscope (AFM) oxidation lithography. The kinetics... 相似文献
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原子力显微镜针尖同接触面的纳米压痕粘着力 总被引:3,自引:0,他引:3
建立了原子力显微镜(AFM)针尖同接触面的纳米压痕物理模型;根据Hamaker三个假设和Lennard-Jones 势理论,利用连续方法推导出针尖同接触面的纳米压痕粘着力表达式.针对Hamaker常数实验值受环境影响较大,给Hamaker常数的具体应用产生困难的问题,从Lifshitz理论,得出Hamaker常数的近似表达式,并计算了Au、Cu、Al、Ag、Hg的Hamaker常数.计算结果同有关文献的实验结果符合,从而为微机械中广泛存在的纳米接触、"微碰"现象研究提供理论基础. 相似文献
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建立了原子力显微镜(AFM)针尖同接触面的纳米压痕物理模型;根据Hamaker三个假设和Lennard-Jones 势理论,利用连续方法推导出针尖同接触面的纳米压痕粘着力表达式.针对Hamaker常数实验值受环境影响较大,给Hamaker常数的具体应用产生困难的问题,从Lifshitz理论,得出Hamaker常数的近似表达式,并计算了Au、Cu、Al、Ag、Hg的Hamaker常数.计算结果同有关文献的实验结果符合,从而为微机械中广泛存在的纳米接触、"微碰"现象研究提供理论基础. 相似文献
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Lianqing Liu Yilun Luo Ning Xi Yuechao Wang Jiangbo Zhang Guangyong Li 《Mechatronics, IEEE/ASME Transactions on》2008,13(1):76-85
The main problem of atomic force microscopy (AFM)-based nanomanipulation is the lack of real-time visual feedback. Although this problem has been partially solved by virtual reality technology, the faulty display caused by random drift and modeling errors in the virtual reality interface are still limiting the efficiency of the AFM-based nanomanipulation. Random drift aroused from an uncontrolled manipulation environment generates a position error between the manipulation coordinate and the true environment. Modeling errors due to the uncertainties of the nanoenvironment often result in displaying a wrong position of the object. Since there is no feedback to check the validity of the display, the faulty display cannot be detected in real time and leads to a failed manipulation. In this paper, a real-time fault detection and correction (RFDC) method is proposed to solve these problems by using the AFM tip as an end effector as well as a force sensor during manipulation. Based on the interaction force measured from the AFM tip, the validity of the visual feedback is monitored in real time by the developed Kalman filter. Once the faulty display is detected, it can be corrected online through a quick local scan without interrupting manipulation. In this way, the visual feedback keeps consistent with the true environment changes during manipulation, which makes it possible for several operations to finish without an image scan in between. The theoretical study and the implementation of the RFDC method are elaborated. Experiments of manipulating nanomaterials including nanoparticles and nanorods have been carried out to demonstrate its effectiveness and efficiency. 相似文献
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S. Piperno I. Kaplan‐Ashiri S. R. Cohen R. Popovitz‐Biro H. D. Wagner R. Tenne E. Foresti I. G. Lesci N. Roveri 《Advanced functional materials》2007,17(16):3332-3338
Geoinspired synthetic chrysotile nanotubes both stoichiometric and 0.67 wt % Fe doped were characterized by transmission electron microscopy and electron diffraction. Bending tests of the synthetic chrysotile nanotubes were performed using the atomic force microscope. The nanotubes were found to exhibit elastic behaviour at small deformations (below ca. 20 nm). Young's modulus values of (159 ± 125) GPa and (279 ± 260) GPa were obtained from the force‐deflection curves using the bending equation for a clamped beam under a concentrated load, for the stoichiometric and the Fe doped chrysotile nanotubes, respectively. The structural modifications induced by Fe doping altered the mechanical properties, with an apparent dependence of the latter on the number of constituting walls of the nanotubes. 相似文献
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Photopicking: In Situ Approach for Site‐Specific Attachment of Single Multiprotein Nanoparticles to Atomic Force Microscopy Tips
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Ivan Liashkovich Gonzalo Rosso Martina Rangl Andreas Ebner Wali Hafezi Joachim Kühn Peter Schön Peter Hinterdorfer Victor Shahin 《Advanced functional materials》2017,27(8)
Ligand–receptor interactions are fundamental in life sciences and include hormone–receptor, protein–protein, pathogen–host, and cell–cell interactions, among others. Atomic force microscopy (AFM) proved to be invaluable for scrutinizing ligand–receptor interactions at the single molecular level. Basically, a ligand is attached to the AFM tip while its cognate receptor is immobilized on a surface or vice versa, and interactions are studied following triggered ligand–receptor binding. However, with rising biological complexity it becomes increasingly challenging to attach a single intact biomolecule to the tip and ensure interaction‐specific orientation. This study presents a novel strategy of inducible in situ tip functionalization with complex multiprotein nanoparticles exemplified by viral capsids, termed photopicking. It ensures a firm attachment of single 125 nm large capsids to the tip. Specific orientation is attained by weak immunosorption of capsids to the substrate and strong photoinducible covalent cross‐linking to the tip. Validation of the tip functionalization success is immediate in situ. The versatility of the strategy is further demonstrated on 20–60 nm large amino‐modified nanoparticles. In conclusion, considering the size range of the tested biomolecules, the presented strategy is applicable to viruses, viral particles, cellular organelles, multiprotein ligands/receptors, and therapeutic nanoparticles, among others. It therefore opens up exciting new avenues in broad biomedical research fields. 相似文献
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用原子力显微镜和扫描电镜相结合的方法表征了KOH腐蚀后的Si掺杂GaN外延层中的位错腐蚀坑.根据腐蚀坑的不同形状和在表面的特定位置可将其分成三种类型,它们的起源可由一个关于腐蚀机制的模型加以解释.纯螺位错易于沿着由它结束的表面阶梯被腐蚀,形成一个小的Ga极性面以阻止进一步的纵向腐蚀,因而其腐蚀坑是位于两个表面阶梯交结处的截底倒六棱椎.纯刃位错易于沿位错线被腐蚀,因而其腐蚀坑是沿着表面阶梯分布的尖底倒六棱椎.极性在GaN的腐蚀过程中起了重要作用. 相似文献
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用原子力显微镜和扫描电镜相结合的方法表征了KOH腐蚀后的Si掺杂GaN外延层中的位错腐蚀坑.根据腐蚀坑的不同形状和在表面的特定位置可将其分成三种类型,它们的起源可由一个关于腐蚀机制的模型加以解释.纯螺位错易于沿着由它结束的表面阶梯被腐蚀,形成一个小的Ga极性面以阻止进一步的纵向腐蚀,因而其腐蚀坑是位于两个表面阶梯交结处的截底倒六棱椎.纯刃位错易于沿位错线被腐蚀,因而其腐蚀坑是沿着表面阶梯分布的尖底倒六棱椎.极性在GaN的腐蚀过程中起了重要作用. 相似文献
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A tabular analytic method for calculating space surface parameters of different materials is suggested. It uses Fourier transforms obtained with an atomic force microscope. Examples of calculation are given for periodic space structures and surfaces with different degrees of anisotropy and periodicity. It is shown that space parameters, namely, texture direction and texture direction index and also radial wavelength and radial wavelength index, allow anisotropy characterization and periodicity determination at a nanometer scale. 相似文献
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超光滑光学基底表面原子力显微镜测试方法 总被引:1,自引:0,他引:1
原子力显微镜(AFM)是评价亚纳米级表面粗糙度σRMS最主要的测试仪器,但其测试结果会因采样条件(采样间距、采样点数)及测量点位置变化而改变。以AFM测试超光滑光学基底随机表面为例,应用累积功率谱理论建立了确定合理采样条件的方法,避免了采样条件选取不当带来的数据丢失或冗余;通过全局优化选取测量点和局部优化选取测量点相结合,降低了样品表面区域性差异给测试结果带来的不确定性,并大大减少了获得可靠测试结果所需的测试量。上述工作为超光滑光学基底AFM测试提供了有效方案。 相似文献