Fretting wear of composite ceramic coating produced on D16 aluminum-based alloy using microarc oxidation

The mechanism of the wear of a composite ceramic coating, which has been produced on the D16 aluminum-based alloy using microarc oxidation, under low-amplitude reciprocal friction (fretting) is studied. The ball-on-plane arrangement in which a diamond ball slides reciprocally against a flat specimen covered with the microarc-oxidation coating is considered. The three following regions of the fracture of the coating have been identified: the moderate wear range, which is characterized by a constant wear rate and in which a smoothed wear spot is formed; the severe wear range, which is characterized by the partial delamination of the top layer of the coating; and the extreme wear range, which is characterized by the cracking of the coating through its entire thickness up to the metal. Based on the experimental results, the boundary of the transition to the inoperative region of the extreme wear of the coating has been determined over the entire ranges of the load and displacement under study.     

Abrasive wear behaviour of B4C particle reinforced Al2024 MMCs

In this study, the effects of volume fraction and particle size of boron carbide on the abrasive wear properties of B₄C particle reinforced aluminium alloy composites have been studied. For this purpose, a block-on-disc abrasion test apparatus was utilized where the samples slid against the abrasive suspension mixture at room conditions. The volume loss, specific wear rate and roughness of the samples have been evaluated. The effects of sliding time, particle content and particle size of B₄C particles on the abrasive wear properties of the composites have been investigated. The dominant wear mechanisms were identified using scanning electron microscopy. The results showed that the specific wear rate of composites decreased with increasing particle volume fraction. Furthermore, the specific wear rate decreased with increasing the size of particle for the composites containing the same amount of B₄C. Hence, it is deduced that aluminium alloy composites reinforced with larger B₄C particles are more effective against the abrasive suspension mixture than those reinforced with smaller B₄C particles.     

合金成分对激光熔覆TiC-TiB_2复合涂层组织性能影响

为增强材料表面硬度和耐磨性,以Ti O2-Al-B4C-C作为粉末体系,利用激光熔覆技术在45#钢基材表面上制备了Ti C-Ti B2增强复合涂层,采用金相显微镜、扫描电镜(SEM)、X射线衍射仪(XRD)、显微硬度计和摩擦磨损试验机研究了不同含量的Ti O2-Al-B4C-C系合金粉末对涂层组织性能的影响。结果表明:复合涂层与基材冶金结合,无裂纹和气孔等缺陷,Ti C、Ti B2弥散分布于涂层中;随着Ti O2-Al-B4C-C系合金粉末含量的增加,涂层组织中Ti C、Ti B2及等轴晶的量逐渐增多;熔覆层的硬度也逐渐增加,当合金粉末含量为70Wt%时,熔覆层硬度最高,为基材的4倍。Ti O2-Al-B4C-C系合金粉末含量为50Wt%时,熔覆层磨损量最小,耐磨性最好     

Microstructural and sliding wear behaviour of a heat-treated zinc-based alloy

The effect of heat treatment on microstructure, hardness, tensile properties, fracture mode and wear behaviour during lubricated and dry sliding of the zinc-based alloy with 25 wt.%Al was studied. Microstructural investigation and chemical analysis of as-cast and heat-treated specimens, the fracture and worn surfaces, as well as wear debris were performed by scanning electron microscopy and energy dispersive spectroscopy. Wear tests were carried out using a disc-on block-type wear machine. By a relatively simple heat treating consisting of a short-term annealing in the single-phase region followed by water-quenching, the elongation has been markedly improved, while the strength was maintained high. The results indicate that the wear rate strongly depends on the microstructure, applied load and sliding conditions. The wear rate increases with load, and under dry sliding conditions the wear rate is approximately two orders of a magnitude higher than under lubricated conditions. During dry sliding the best wear behaviour was displayed by the water-quenched specimens, whereas slowly cooled specimens showed the higher wear rate. Lubrication strongly affects the wear behaviour. Contrary to dry sliding, slowly cooled specimens exhibit the best wear properties under lubricated conditions. The wear mechanisms were proposed for dry and lubricated sliding. An erratum to this article can be found at     

Microstructural and wear properties of sputtered carbides and silicides

Sputtered Cr₃C₂, Cr₃Si₂ and MoSi₂ wear-resistant films (0.05–3.5 μm thick) were deposited on metal and glass surfaces. Electron transmission, electron diffraction and scanning electron microscopy were used to determine the microstructural appearance. Strong adherence was obtained with these sputtered films. Internal stresses and defect crystallographic growth structures of various configurations within the film have progressively more undesirable effects for film thicknesses greater than 1.5 μm. Sliding contact and rolling element bearing tests were performed with these sputtered films. Bearings sputtered with a duplex coating (a 0.1 μm thick undercoating of Cr₃Si₂ and subsequently a 0.6 μm coating of MoS₂) produced marked improvement (more than 10.5 × 10⁷ cycles) over straight MoS₂ films.     

B4C颗粒对AZ61蠕变及磨损性能影响的研究

采用机械搅拌法制备B4C/AZ61镁基复合材料,并通过对比AZ61镁合金和B4C/AZ61镁基复合材料的蠕变和磨损试验,分析B4C颗粒对AZ61镁合金蠕变及磨损性能的影响.结果表明:在蠕变性能上,与AZ61镁合金相比,B4C/AZ61镁基复合材料具有较小的初始蠕变量和较小的总蠕变量,进入稳态蠕变阶段的时间和进入稳态蠕变状态时的蠕变速率与AZ61镁合金基本相同;在磨损性能上,B4C颗粒的添加使得AZ61镁合金的抗磨损性能得到明显提升.     

Microstructure and wear properties of in situ TiC/FeCrBSi composite coating prepared by gas tungsten arc welding

Using a gas tungsten arc welding (GTAW) process, in situ synthesis TiC particles reinforced Fe-based alloy composite coating has been produced by preplaced FeCrBSi alloy, graphite and ferrotitanium powders. The microstructure and wear properties of the composite coatings were studied by means of scanning electron microscopy (SEM), X-ray diffractometer (XRD) and wear test. The effects of thickness of the pre-placed powder layer on the microstructure, hardness and wear resistance of the composite coatings were also investigated. The results indicated that TiC particles were produced by direct metallurgical reaction between ferrotitanium and graphite during the GTAW process. TiC particles with sizes in the range of 3–5 μm were dispersed in the matrix. The volume fraction of TiC particles and microhardness gradually increased from the bottom to the top of the composite coatings. The TiC-reinforced composite coatings enhance the hardness and wear resistance. The highest wear resistance of the composite coating with a 1.2 mm layer was obtained.     

Microstructure and wear properties of in situ TiC/FeCrBSi composite coating prepared by gas tungsten arc welding

Using a gas tungsten arc welding (GTAW) process, in situ synthesis TiC particles reinforced Fe-based alloy composite coating has been produced by pre-coated FeCrBSi alloy, graphite and ferrotitanium powders on the substrate. The microstructure and wear properties of the composite coatings were studied by means of scanning electron microscopy (SEM), X-ray diffractometer (XRD) and wear test. The effects of thickness of the pre-coated powder layer on the microstructure, hardness and wear resistance of the composite coatings were also investigated. The results indicated that TiC particles were produced by direct metallurgical reaction between ferrotitanium and graphite during the GTAW process. TiC particles with sizes in the range of 3–5 μm were dispersed in the matrix. The volume fraction of TiC particles and microhardness gradually increased from the bottom to the top of the composite coatings. The TiC-reinforced composite coatings enhance the hardness and wear resistance. The highest wear resistance of the composite coating with a 1.2 mm layer was obtained.     

固体自润滑涂层摩擦磨损特性研究

随着机械加工技术和空间技术的发展,固体润滑涂层在比较恶劣的润滑环境下能起到独特的润滑效果,得到高速发展和广泛应用.在综合国内外研究和报道的基础上,对一般固体润滑涂层和纳米固体润滑涂层的摩擦磨损特性的研究现状进行归纳,指出固体润滑涂层摩擦磨损研究的发展方向.     

Studies on friction and wear properties of surface produced by ultrasonic vibration-assisted milling

The grinding of elliptical gears on a computer numerical control (CNC) gear grinder with conical wheel is studied according to the mesh theory of elliptical gears. Two machining methods form the machine structure and movement, namely a mobile grinding wheel type and a fixed grinding wheel type. Mathematical models of the movement relation for the elliptical gear grinding process are built up. Since the teeth of the elliptical gears are different from each other, their generating length is also different. Based on the analysis of generating and indexing movement, a universal generating length formula of each tooth is proposed. Basic machining parameters of each tooth, for these two types of machines, are computed using a practical example. The dynamic simulation of generating track is given. The research results show that the grinding of elliptical gears with a CNC conical wheel gear grinder is feasible.     

Advancement and characterization of Al-Mg-Si alloy using reinforcing materials of Fe2O3 and B4C composite produced by stir casting method

The modifications of Al6061-T6 metal matrix composites is an extraordinary enthusiasm of recent pertinence for lesser weight materials with high value of tensile strength, hardness and wear protection, which can be widely used in automotive and aircraft design. In this paper, we investigate the impacts of the reinforced Al6061 composite with 5 wt% of Fe₂O₃ in addition to 2 %, 4 %, 6 % weight of B₄C being made-up by stir casting technique. In this research, Al6061 composites have analyzed by its physical and mechanical properties like as density, hardness, impact strength, ultimate tensile and compressive strength, and an optical microscope is utilized to assess the metallurgical properties such as microstructure with different wt% of reinforcement of Al6061 composite. The microstructure of newly prepared composites was shown a regular spreading of reinforcements in the matrix by an optical microscope and also the muscular bonding between the matrix and reinforcements were demonstrated by SEM analysis. It is further identifying that, microstructure uniformity and therefore the tensile strength of the metal composites was enhanced with increasing the fraction of Fe₂O₃ and B₄C particles without any decrement in elongation.

     

Effects of different metals on adhesive wear behaviour of alloy surface produced by TIG process

Abstract

Low carbon steel surfaces were alloyed with composite powders using the tungsten inert gas welding method. After the alloying process, the effects of cladding surface on the microstructural characteristics and adhesive wear of the alloyed samples were examined. The sliding wear behavior of samples was investigated in a block on ring apparatus under the loads of 20, 40, 60 and 80 N respectively. In the experimental investigation, a low carbon steel surface was alloyed with austenitic stainless steel powder and austenitic stainless steel powder mixed with 4·5% Co, Mo and Ti particles respectively. Following surface alloying, conventional characterisation techniques, such as optical microscopy, scanning electron microscopy, energy dispersive spectrograph and X-ray diffraction, were used to study the microstructure of the alloyed zone. Examination of the microstructure revealed the presence of M₂₃C₆ carbides, solid melt phases and intermetallic phases, such as Ni₃Ti, depending on the alloying element in the composite. As the amount of the reinforcing material increased, the saturation rates for the samples decreased, while their hardness increased. The adhesive abrasion tests conducted revealed that temperature input plays a significant role on the microstructure characteristics, which positively affected the adhesive abrasion values of the samples. Consequently, the tungsten inert gas welding method was successfully used for the surface alloying of low carbon steels.     

Research on manufacturing Cu matrix Fe-Cu-Ni-C alloy composite parts by indirect selective laser sintering

The property of alloy parts can be adjusted conveniently if alloy element powders are used for manufacturing alloy parts by indirect selective laser sintering (SLS), but there have been no reports in this field. Fe, Cu, Ni, C composite powders of two compositions were obtained through a 3D blending way in this paper. Green parts of above composite powder were manufactured by indirect SLS. Then, Cu matrix Fe-Cu-Ni-C alloy composites were produced after green parts had been depolymerized, high temperature sintered and infiltrated by molten Cu. The post-processing of green parts, microstructure and mechanical properties of alloy composites were investigated. The results show: Ni, Cu and C diffuse into γ-Fe when green parts are being sintered at high temperature and the distributing non-uniformity of alloy elements is eliminated basically; at room temperature, alloy composite microstructures are composed of lower bainite, α-Cu precipitated out of γ-Fe and Fe-Ni after they have been solution treated at 930°C and held at 350°C for 1 h later; the yield strength of alloy composites is near to 400 MPa and the elongation is under 3%. It can be used for manufacturing injection mold or other functional parts by indirect SLS.     

Enhancement of wear resistance of ductile cast iron by Ni–SiC composite coating

Wear resistance of unalloyed ductile iron (Dl) can be enhanced either by heat treatment or by deposition of hard coating. The electrodeposition of Ni–SiC composite on unalloyed Dl (GGG 40) has been applied. The effect of operating conditions including current density and SiC content in the plating solution on the SiC incorporation in the deposited layer were studied. It was found that the volume percent of SiC particles in the composite layer increases with increasing current density and SiC content in the bath. The maximum SiC incorporation could be attained at optimum conditions; 60 g/1 of SiC particles in suspension, 5 A/dm², pH 5 and 50 °C. Also the results reveal that the particle inclusion in the coating layer depends mainly on the treatment process (activation with PdCI₂). The mechanical properties of the composite such as hardness and wear resistance were examined comparing with the uncoated substrate. The reinforced particles incorporated with Ni-matrix improve the hardness and wear resistance of coated Dl comparing with uncoated substrate.     

Sliding friction and wear of magnesium alloy AZ91D produced by two different methods

Alloy AZ91D is a leading magnesium alloy used for structural applications. It contains aluminum and zinc as principal alloying elements. This alloy is normally die-cast, but recent developments in semi-solid injection molding (Thixomolding^®), which offers certain processing advantages, produces a slightly different microstructure than die-casting, and it was of interest to determine whether the two processing routes would measurably affect the friction and wear of AZ91D. The present work involved ambient air, room temperature testing of die-cast (DC) and Thixomolded^® (ThM) AZ91D, in both unidirectional and reciprocating sliding motion, using stainless steel type 440C as the counterface. After running-in, the average sliding friction coefficients in both types of test fell into the range of 0.29–0.35, irrespective of processing method. The formation of a built-up edge raised the friction slightly in unidirectional tests compared with reciprocating tests. The average wear rate of the ThM alloys in reciprocating sliding was approximately 25% lower than that for DC alloys. However, the wear rates of the magnesium specimens in unidirectional sliding were comparable for DC and ThM materials. Owing to the transfer of magnesium, there was no measurable wear on the stainless steel 440C balls. The wear mechanism during sliding involves the formation of thin, narrow shards along the edges of wear grooves which break off to produce loose particles.     

Dry sliding friction and wear properties of metallic glass coating and martensite stainless coating

The wire arc spraying process was used to prepare FeB-based metallic glass coating and 3Cr13 coating. The effects of wear parameters, such as sliding distance, linear speed and normal loads, on the wear performances of the coatings were analyzed in detail. The results showed that, with increase in sliding distance, linear speed and normal loads, the volume losses of the metallic glass coatings increased. The relationships between wear behavior and microstructure of the coatings were discussed. The metallic glass coating had excellent wear resistance. The relatively wear resistance of the metallic glass coating was about 2.6 times that of the 3Cr13 coating under the same testing conditions. The main failure mechanism of the metallic glass coating was brittle failure and fracture.     

激光强化40Cr合金钢表面磨损特性研究

采用CO2激光器及不同的激光强化参数对40Cr钢进行表面强化,并将其与热轧Q235钢组成摩擦副,在干摩擦条件下进行摩擦磨损试验,旨在确定合理的激光强化参数,为提高矫直辊耐磨性提供试验依据。通过对试验结果的定量分析得出,激光强化可以提高40Cr钢的耐磨性。采用扫描电镜对激光强化后的40Cr钢表面和磨损表面进行分析,发现激光强化后40Cr钢的金相组织主要是致密的马氏体,而且磨损表面比正常淬火的40Cr钢的表面光滑,仅产生一些微裂纹。     

Fabrication of two-layered Al-B4C composites by conventional hot pressing uuder nitrogen atmosphere and their characterization

In this study, we describe the conventional hot pressing (CHP) of layered Al-B₄C composites and their characterization. The matrix alloy A1-5 wt.%Cu was prepared from elemental powder mixtures. The metal and B₄C powders were mixed to produce either Al-Cu-10vol.%B₄C or Al-Cu-30vol.%B₄C combinations. Then, these powder mixtures were stacked as layers in the hot pressing die to form a two-layered composite. Hot pressing was carried out under nitrogen atmosphere to produce 30×40×5 mm specimens. Microstructural features and age hardening characteristics of composites were determined by specimens cut longitudinally. The flexural strength of both layered composites and their monolithic counterparts were investigated via three point bending tests. In the case of layered specimens of both 10vol.%B₄C and 30vol.%B₄C containing layers were loaded for three-point test. The results show that a homogeneous distribution of B₄C particles in the matrix alloy which is free of pores, can be obtained by CHP method. The ageing behavior of the composites was found to be influenced by the reinforced materials, i.e. higher hardness values were reached in 8 hrs for the composites than that for the matrix alloy. Flexural strength test showed that two-layered composites exhibited improved damage tolerance depending on layer arrangement. Microstructural investigation of the fracture surfaces of the bending specimens was performed by means of scanning electron microscope (SEM). While layer with lower reinforcement content exhibited large plastic deformation under loading, the other with higher reinforcement content exhibited less plastic deformation.     

Microstructure and wear characteristics on Al alloy matrix composite reinforced with Ni perform

Al based composite reinforced with Nickel is used for diesel engine piston, because the thermal properties, strength and corrosion resistant are for better than Al alloy alone. For processing, the intermetallic compounds of Ni and Al improves wear resistance due to its high hardness. Existing process methods for MMC (metal matrix composite) using preform were manufactured under high-pressure. However, this causes deformation of the preform or weaknesses in the completed MMC. Low-pressure infiltration can prevent these problems, and there is an advantage of cost reduction in of production with small-scale of production equipment. In this study, the microstructure and wear characteristics of Al-based composite with Ni preform as reinforcement with low-pressure infiltration was analyzed.