Fractographic observations on delamination growth and the subsequent migration through the laminate

This paper describes fractographic observations from the detailed examination of delamination fracture surfaces and offers an interpretation of the key growth mechanisms. Firstly, the relationship between toughness, delamination failure criteria and fracture morphology is presented and the influence of cusp formation and deformation on toughness is discussed. Observations regarding delaminations migrating through the lamina at multidirectional ply interfaces are then discussed. It is demonstrated how this migration process can be avoided in fracture toughness coupons and consequently the toughness of multidirectional ply interfaces can be characterised. The influence of migration on delamination growth from embedded defects in laminates under compression is presented, and these results are extended to demonstrate how migration influences damage growth in structures. The paper concludes by making recommendations for realistic modelling of migration, and suggests how it can be exploited in damage tolerant structural design.     

Effect of stitch density and stitch thread thickness on compression after impact strength and response of stitched composites

In this paper, the damage failure and behaviour of stitched composites under compression after impact (CAI) loading are experimentally investigated. This study focuses on the effect of stitch density and stitch thread thickness on the CAI strength and response of laminated composites reinforced by through-thickness stitching. Experimental findings show that stitched composites have higher CAI failure load and displacement, which corresponds to higher energy absorption during CAI damage, mainly attributed to greater energy consumption by stitch fibre rupture. The coupling relationships between CAI strength, impact energy, stitch density and stitch thread thickness are also revealed. It is understood that the effectiveness of stitching has high dependency on the applied impact energy. At low impact energy range, CAI strength is found to be solely dependent on stitch density, showing no influence of stitch thread thickness. It is however observed that stitch fibre bridging is rendered ineffective in moderately stitched laminates during compressive failure, as local buckling occurs between stitch threads, resulting in unstitched and moderately stitched laminates have similar CAI strength. The CAI strength of densely stitched laminates is much higher due to effective stitch fibre bridging and numerous stitch thread breakages. At high impact energy level, CAI strength is discovered to be intimately related to both stitch density and stitch thread thickness. Since CAI failure initiates from impact-induced delamination area, stitch fibre bridging is considerable for all specimens due to the relatively large delamination area present. Stitch threads effectively bridge the delaminated area, inhibit local buckling and suppress delamination propagation, thus leading to increased CAI strength for laminates stitched with higher stitch density and larger stitch thread thickness. Fracture mechanisms and crack bridging phenomenon, elucidated by X-ray radiography are also presented and discussed. This study reveals novel understanding on the effectiveness of stitch parameters for improving impact tolerance of stitched composites.     

Quantification of flexural fatigue life and 3D damage in carbon fibre reinforced polymer laminates

Carbon fibre reinforced polymer (CFRP) laminated composites have become attractive in the application of wind turbine blade structures. The cyclic load in the blades necessitates the investigation on the flexural fatigue behaviour of CFRP laminates. In this study, the flexural fatigue life of the [+45/−45/0]_2s CFRP laminates was determined and then analysed statistically. X-ray microtomography was conducted to quantitatively characterise the 3D fatigue damage. It was found that the fatigue life data can be well represented by the two-parameter Weibull distribution; the life can be reliably predicted as a function of applied deflections by the combined Weibull and Sigmodal models. The delamination at the interfaces in the 1st ply group is the major failure mode for the flexural fatigue damage in the CFRP laminate. The calculated delamination area is larger at the interfaces adjacent to the 0 ply. The delamination propagation mechanism is primarily matrix/fibre debonding and secondarily matrix cracking.     

Acoustic structural health monitoring of composite materials : Damage identification and evaluation in cross ply laminates using acoustic emission and ultrasonics

The characterisation of the damage state of composite structures is often performed using the acoustic behaviour of the composite system. This behaviour is expected to change significantly as the damage is accumulating in the composite. It is indisputable that different damage mechanisms are activated within the composite laminate during loading scenario. These “damage entities” are acting in different space and time scales within the service life of the structure and may be interdependent. It has been argued that different damage mechanisms attribute distinct acoustic behaviour to the composite system. Loading of cross-ply laminates in particular leads to the accumulation of distinct damage mechanisms, such as matrix cracking, delamination between successive plies and fibre rupture at the final stage of loading. As highlighted in this work, the acoustic emission activity is directly linked to the structural health state of the laminate. At the same time, significant changes on the wave propagation characteristics are reported and correlated to damage accumulation in the composite laminate. In the case of cross ply laminates, experimental tests and numerical simulations indicate that, typical to the presence of transverse cracking and/or delamination, is the increase of the pulse velocity and the transmission efficiency of a propagated ultrasonic wave, an indication that the intact longitudinal plies act as wave guides, as the transverse ply deteriorates. Further to transverse cracking and delamination, the accumulation of longitudinal fibre breaks becomes dominant causing the catastrophic failure of the composite and is expected to be directly linked to the acoustic behaviour of the composite, as the stiffness loss results to the velocity decrease of the propagated wave. In view of the above, the scope of the current work is to assess the efficiency of acoustic emission and ultrasonic transmission as a combined methodology for the assessment of the introduced damage and furthermore as a structural health monitoring tool.     

Damage tolerance of fully orthotropic laminates in compression

The compression after impact (CAI) strength of fully orthotropic composite laminates with up to 21 plies is presented, as analysed by an existing strip model. Candidate layups, which can be symmetric, anti-symmetric or non-symmetric, are preselected to exhibit no elastic coupling response, with manufacturing rules applied. These criteria, along with the use of a simple surrogate sublaminate buckling model, were chosen to allow analysis of all feasible laminates in the design space without excessive computation time. Results indicate that although the inclusion of non-symmetric layups in the design space does not give benefits with respect to maximum achievable damage tolerance, these laminates can exhibit damage tolerance close to that of an anti-symmetric design for some ply counts, and better than symmetric solutions in most cases. It is also noted that in some instances increasing the number of plies in a laminate can actually reduce the highest achievable threshold load for damage tolerance, as a result of the large influence Poisson’s ratio has on sublaminate buckling. Average errors in the surrogate model were low in all cases, with maximum non-conservative errors less than 1%. The surrogate buckling model reduced computational time by over 99% when compared to the fully exhaustive search.     

Structural design of single lap joints with delaminated FRP composite adherends

This paper deals with the structural design of single lap joints (SLJs) with delaminated adherends using fracture mechanics principles. The interlaminar stresses and Strain Energy Release Rate (SERR) are considered as damage characterizing parameters used for designing the SLJ when delamination damages are pre-embedded in both the adherends at similar positions. Three dimensional geometrically non-linear finite element analyses (FEAs) of SLJ with delaminated adherends have been performed to determine the interlaminar and SERR values along the delamination fronts by simulating the simultaneous interaction delamination damages when pre-embedded at similar positions in both the adherends. SERR values are evaluated using Modified Crack Closure Technique (MCCI) which is based on energy principle. The delaminations are assumed to be of linear front, and have been considered to be embedded in both the laminated FRP composite adherends beneath the surface ply of the adhesively bonded SLJ. The delamination damages are presumed either to pre-exist or get evolved at the interlaminar locations. Such delaminations have been modelled using the sublaminate technique. The critical issues of modelling pre-embedded delamination damages are discussed in detail. The numerical results presented in this paper are based on the validated FE model compared with the available literature. Based on the present analyses, the structural design recommendations have been made for the SLJ when pre-embedded delamination damages are present in both the adherends. It is observed from the stress based design that the delamination damage when present in the bottom adherend is more detrimental for failure of SLJ compared to that for the case when it is present in the top adherend. Also, SERR based design reveals that the opening mode predominantly governs the propagation of delamination damage for all positions of the pre-embedded delaminations in both the adherends of the SLJ.     

含界面脱粘及表板基体开裂损伤的复合材料夹层板非线性稳定性的研究

本文作者基于"zig-zag"模型和Mindlin一阶剪切变形板理论,推导了复合材料夹层板屈曲分析的有限元列式,在该列式中考虑了面板的横向剪切变形和芯体的面内刚度对夹层板力学性能的影响。针对具有面板和芯体间界面脱粘和纤维增强树脂基体微裂纹损伤的夹层板损伤特征,分别提出了分层模型和多标量损伤模型,并推导了多标量形式的损伤本构关系。采用修正的 Newton-Raphson迭代格式求解含损复合材料夹层板的非线性稳定性性状。通过算例研究了脱粘面积、基体的损伤演化、表板的铺设方式及载荷形式对复合材料夹层板屈曲性态的影响。本文作者给出的有限元模型和结论,对复合材料夹层板结构设计的损伤容限的制定具有一定的参考价值。     

GLARE层板挤压渐进损伤分析

对GLARE36/5层板进行挤压性能试验研究,采用超声C扫描、断口微距拍摄和扫描电子显微镜等方法观测GLARE层板挤压渐进损伤过程和最终破坏模式。结果表明:GLARE层板挤压起始损伤为铝合金塑性变形;损伤扩展阶段,0°纤维主要承受挤压正应力,铝合金塑性变形增大,铺层间分层起始并扩展;0°纤维屈曲折断后层内纤维基体损伤和分层损伤急剧扩展,层板最终发生挤压破坏。将GLARE层板挤压失效分为层内失效和层间失效,采用应变描述的Hashin准则和界面单元方法并引入金属塑性建立GLARE层板挤压渐进损伤数值模型,数值模型对层板损伤起始位置、分层产生位置、损伤演化过程、最终破坏模式及破坏载荷进行了预测,计算结果与试验结果吻合较好,说明该计算方法能够有效模拟GLARE层板挤压渐进损伤性能。      

含分层损伤缝合复合材料层板的剩余压缩强度

基于渐进损伤方法,研究了含单脱层缝合复合材料层板在压缩载荷下的剩余强度。通过商用软件ABAQUS建立了含单脱层缝合复合材料层板剩余压缩强度计算模型,考虑了子层屈曲和分层扩展对剩余强度的影响。通过UMAT子程序实现了层板失效、层间失效和缝线失效的模拟。通过嵌入式杆单元结构模拟了缝线桥联作用及失效。采用Hashin准则及刚度折减法对纤维拉压、基体拉压失效进行了模拟。通过渐进损伤分析,揭示了缝合情况下含单脱层复合材料层板的失效机理,讨论了缝合参数对剩余压缩强度的影响。所预测的破坏模式和剩余强度结果与实验能较好地吻合。分析表明缝合可以明显提高含分层损伤复合材料层板的子层屈曲载荷,抑制分层扩展,并提高层板的剩余压缩强度。     

Integrated XFEM-CE analysis of delamination migration in multi-directional composite laminates

Progressive damage and failure in composites are generally complex and involve multiple interacting failure modes. Depending on factors such as lay-up sequence, loading and specimen configurations, failure may be dominated by extensive matrix crack-delamination interactions, which are very difficult to model accurately. The present study further develops an integrated extended finite element method (XFEM) and cohesive element (CE) method for three-dimensional (3D) delamination migration in multi-directional composite laminates, and validates the results with experiment performed on a double-cantilever beam (DCB). The plies are modeled by using XFEM brick elements, while the interfaces are modeled using CEs. The interaction between matrix crack and delamination is achieved by enriching the nodes of cohesive element. The mechanisms of matrix fracture and delamination migration are explained and discussed. Matrix crack initiation and propagation can be predicted and delamination migration is also observed in the results. The algorithm provides for the prediction of matrix crack angles through the ply thickness. The proposed method provides a platform for the realistic simulation of progressive failure of composite laminates.     

A micrographic study of bending failure in five thermoplastic-carbon fibre composite laminates

The local deformation and failure sequences of five thermoplastic matrix composites were microscopically observed while bending the samples in a small fixture attached to a microscope stage. The thermoplastics are polycarbonate, polysulphone, polyphenylenesulphide, polyethersulphone and polyetheretherketone. The composites made from these plastics contain a variety of carbon fibres, though all with similar properties, and have fibre volume fractions ranging from 32 to 66%. Comparison is made to an epoxy matrix composite, 5208-T-300. Laminates tested are (0/90)_2S, with outer ply fibres parallel to the beam axis. Four-point bending is used at a typical span-to-thickness ratio of 39:1. A shallow notch is put in the samples at mid-span to avoid failure under the loading pins. It was found that all the thermoplastic composites failed by abrupt longitudinal compression buckling of the outer ply. Very little precursory damage was observed. Micrographs reveal typical fibre kinking associated with longitudinal compression failure. Curved fracture surfaces on the fibres suggest they failed in bending rather than direct compression. Delamination was suppressed in the thermoplastic composites, and the delamination that did occur was found to be the result of compression buckling, rather than vice versa. Microbuckling also caused other subsequent damage such as ply splitting, transverse ply shear failure, fibre tensile failure, and transverse ply cracking.     

Finite element model for compression after impact behaviour of stitched composites

A finite element (FE) model using coupling continuum shell elements and cohesive elements is proposed to simulate the compression after impact (CAI) behaviour and predict the CAI strength of stitched composites. Continuum shell elements with Hashin failure criterion exhibit the composite laminate damage behaviour; whilst cohesive elements using traction-separation law characterise the laminate interfaces. Impact-induced delamination is explicitly modelled by reducing material properties of damaged cohesive elements. Computational results have demonstrated the trend of increasing CAI strength with decreasing impact-induced delamination area. Spring elements are introduced into the model to represent through-thickness stitch thread in the composite laminates. Results in this study validate experimental finding that CAI strength is improved when stitching is incorporated into the composite structure. The proposed FE model reveals good CAI strength predictions and indicates good agreement with experimental results, making it a valuable tool for CAI strength prediction of stitched composites.     

Failure mechanisms on composite specimens subjected to compression after impact

Composite panels are widely used in aeronautic and aerospace structures due to their high strength/weight ratio. The stiffness and the strength in the thickness direction of laminated composite panels is poor since no fibres are present in that direction and out-of-plane impact loading is considered potentially dangerous, mainly because the damage may be left undetected. Impact loading in composite panels leads to damage with matrix cracking, inter-laminar failure and eventually fibre breakage for higher impact energies. Even when no visible impact damage is observed at the surface on the point of impact, matrix cracking and inter-laminar failure can occur, and the carrying load of the composite laminates is considerably reduced. The greatest reduction in loading is observed in compression due to laminae buckling in the delaminated areas. The objective of this study is to determine the mechanisms of the damage growth of impacted composite laminates when subjected to compression after impact loading. For this purpose a series of impact and compression after impact tests were carried out on composite laminates made of carbon fibre reinforced epoxy resin matrix. An instrumented drop-weight-testing machine and modified compression after impact testing equipment were used together with a C-scan ultrasonic device for the damage identification. Four stacking sequences of two different epoxy resins in carbon fibres representative of four different elastic behaviours and with a different number of interfaces were used. Results showed that the delaminated area due to impact loading depends on the number of interfaces between plies. Two buckling failure mechanisms were identified during compression after impact, which are influenced more by the delamination area than by the stacking sequence.     

Micromechanical modeling to determine the compressive strength and failure mode interaction of multidirectional laminates

Computational models to predict the compressive strength of carbon fiber reinforced polymer matrix composites are proposed here, motivated by the failure mechanisms observed in compression tests. Delamination, fiber kink-banding and their interaction are seen to dominate the failure response. An upscaled semi-homogenized laminate model is developed to predict the observed compressive response of multidirectional laminates. A generalized 2-D formulation is presented to determine the interfaces most susceptible to delamination. Subsequently, cohesive elements are added along these interfaces to introduce delamination capability in the model. Predictions of the model are compared against experimental data, and are found to be in agreement with respect to compressive strength and failure modes. Further, the effect of stacking sequence on the compressive strength and failure mode is investigated.     

Near-surface delamination induced local bending failure of laminated composites monitored by acoustic emission and micro-CT

Aiming to investigate the effects of the near-surface delamination on buckling response behavior of carbon fiber reinforced laminated composites under different bending modes, acoustic emission (AE) data analysis and X-ray micro-computed tomography (micro-CT) imaging method were promoted to characterize the mechanical properties, acoustic responses and damage visualization. Due to the existence of the artificial embedded delamination, when subjected to local compression induced by bending loads, the laminated composites showed a strong tendency to buckling behavior. The mechanical properties indicated that under different bending modes, the size of delamination had little influence on the relative change ratio of ultimate bearing capacity, but the thickness of specimen had a significant influence on the relative change ratio of ultimate load. AE monitoring results showing the characteristics of energy release for composites were related to the mutation rate of load curve. Moreover, cluster results indicate that matrix failure, interfacial failure and fiber failure are the main damage mechanisms. Micro-CT results illustrated that as the thickness of composites increases, there is a reduction in crack density. AE monitoring can reflect the initiation and evolution process of damage, and damage mechanism identification can be realized by clustering analysis. Besides, the internal damage morphologies acquired by micro-CT can directly verify the damage mechanisms. The cross-validation of AE and micro-CT can provide a basis for structural health monitoring of composites.

     

3D damage characterisation and the role of voids in the fatigue of wind turbine blade materials

The fatigue mechanisms of Glass Fibre Reinforced Polymer (GFRP) used in wind turbine blades were examined using computed tomography (CT). Prior to mechanical testing, as-manufactured [+45/−45/0]_3,s glass/epoxy specimens were CT scanned to provide 3-dimensional images of their internal microstructure, including voids. Voids were segmented and extracted, and individual characteristics and volumetric distributions were quantified. The coupons were then fatigue tested in uniaxial loading at R = −1% to 40% of the nominal tensile failure stress. Some tests were conducted to failure for correlation with the initial void analysis and to establish failure modes. Other tests were stopped at various life fractions and examined using CT to identify key damage mechanisms. These scans revealed transverse matrix cracking in the surface layer, occurring predominantly at free edges. These free-edge cracks then appeared to facilitate edge delamination at the 45/−45° interface. Propagation from sub-critical, surface ply damage to critical, inner ply damage was identified with either a −45/0° delamination, or a 0° fibre tow failure allowing a crack to propagate into the specimen bulk. Final failure occurred in compression and was characterised by total delamination between all the 45/−45° plies. A quantitative void analysis, taken from the pre-test CT scans, was also performed and compared against the specimens’ fatigue lives. This analysis, to the authors’ knowledge the first of its kind, measured and plotted approximately 10,000 voids within the gauge length of each specimen. The global void measurement parameters and distributions showed no correlation with fatigue life. A local ply-level investigation revealed a significant correlation between the largest void and fatigue life in the region of the laminate associated with the crack propagation from sub-critical to critical damage.     

Characterization of high-velocity impact damage in CFRP laminates: Part I – Experiment

This study investigated mechanisms of the extension of high-velocity impact damage in CFRP laminates. To this end, damage states due to near-perforation impact were studied in detail. This study consists of two parts. Part I presents the experiment results of high-velocity impact tests for CFRPs with specified stacking sequences. A crater and splits were observed on the impacted surface, while multiple splits with fiber breaks extended on the back surface. The cross-section beneath the impact point included catastrophic ply failure with extensive fiber breaks. Impacted specimens also exhibited a particular delamination pattern consisting of pairs of symmetric fan-shaped delaminations emanating from to the impact point and elongated delamination along the cracks in the bottom ply. These damage patterns were common to all of the stacking sequences. Part II of this study presents a numerical analysis of high-velocity impact based on smoothed-particle hydrodynamics and discusses damage extension mechanisms.     

Post Buckling Progressive Failure Analysis of Composite Laminated Stiffened Panels

The present work deals with the numerical prediction of the post buckling progressive and final failure response of stiffened composite panels based on structural nonlinear finite element methods. For this purpose, a progressive failure model (PFM) is developed and applied to predict the behaviour of an experimentally tested blade-stiffened panel found in the literature. Failure initiation and propagation is calculated, owing to the accumulation of the intralaminar failure modes induced in fibre reinforced composite materials. Hashin failure criteria have been employed in order to address the fiber and matrix failure modes in compression and tension. On the other hand, the Tsai-Wu failure criterion has been utilized for addressing shear failure. Failure detection is followed with the introduction of corresponding material degradation rules depending on the individual failure mechanisms. Failure initiation and failure propagation as well as the post buckling ultimate attained load have been numerically evaluated. Final failure behaviour of the simulated stiffened panel is due to sudden global failure, as concluded from comparisons between numerical and experimental results being in good agreement.     

含面芯界面缺陷的蜂窝夹芯板侧向压缩破坏模式

为了对含面芯层间脱胶缺陷的蜂窝夹芯板在侧向压缩载荷作用下的典型破坏模式进行数值预报, 建立了基于蔡-希尔破坏准则和粘结模型的计算模型。该计算模型是建立在对蜂窝夹芯板的双悬臂梁(DCB)和单臂梁(SLB) 试验中所发现的一种新的破坏模式的分析基础之上的。对蜂窝夹芯板的侧向压缩破坏行为的数值预报中, 发现一种新的破坏模式: 位于脱胶区域的面板首先发生局部屈曲失稳, 随后面板内部靠近芯子的45°/0°层间出现分层, 与此同时最靠近芯子的45°铺层发生断裂, 伴随着45°/0°层间分层的扩展, 面板发展成为对称性整体屈曲失稳。与侧向压缩试验测试结果对比发现, 计算模型模拟中所预报的破坏模式在实验测试中也得到了很好的验证。      

Low velocity impact modeling in composite laminates capturing permanent indentation

This paper deals with impact damage and permanent indentation modeling. A numerical model has been elaborated in order to simulate the different impact damage types developing during low velocity/low energy impact. The three current damage types: matrix cracking, fiber failure and delamination, are simulated. Inter-laminar damage, i.e. interface delamination, is conventionally simulated using interface elements based on fracture mechanics. Intra-laminar damage, i.e. matrix cracks, is simulated using interface elements based on failure criterion. Fiber failure is simulated using degradation in the volume elements. The originality of this model is to simulate permanent indentation after impact with a “plastic-like” model introduced in the matrix cracking elements. This model type is based on experimental observations showing matrix cracking debris which block crack closure. Lastly, experimental validation is performed, which demonstrates the model’s satisfactory relevance in simulating impact damage. This acceptable match between experiment and modeling confirms the interest of the novel approach proposed in this paper to describe the physics behind permanent indentation.