Mn-Cr齿轮钢动态再结晶行为及组织演变

采用Gleeble 1500热模拟试验机研究了一Mn-Cr齿轮钢在变形速率为0.1～1 s-1、变形温度为900～1150℃、原始奥氏体晶粒尺寸为70～150 μm条件下的动态再结晶行为及再结晶奥氏体晶粒尺寸的变化规律.实验结果表明,Mn-Cr齿轮钢在温度较高,应变速率较低及原始奥氏体晶粒较细的情况下变形时,表现出典型的动态再结晶行为.再结晶发生的条件为Zener-Hollomon参数小于某一临界值(Zc).再结晶晶粒按晶界突出机制形核.通过回归分析,确定该齿轮钢的再结晶激活能为378.6 kJ/mol,应力指数为5.8.Z参数控制形变储存能,因而唯一地决定动态再结晶晶粒尺寸Ds,二者符合关系式Ds=1.3×105Z-0.25.     

基于复合变形的镁合金动态再结晶及晶粒尺寸研究

目的 研究复合变形工艺参数对镁合金动态结晶体积分数及镁合金晶粒度的影响规律.方法 采用镁合金板材压痕-压平复合变形技术、扫描电子显微镜和EBSD等材料性能先进检测技术,获得经过复合变形后的镁合金材料的微观组织及动态结晶体积分数、镁合金的晶粒度等相关数据.结果 当变形温度为350℃、复合变形系数为0.375时,动态再结晶...     

23CrNi3Mo钢动态再结晶行为和组织演变研究

利用Gleeble-1500热模拟试验机进行单道次热压缩变形,通过控制变形温度(900,950,1 000,1 050℃)和应变速率(0.01,0.1和1 s-1)研究了23CrNi3Mo钢的动态再结晶行为,分析了变形温度、应变速率对动态再结晶行为和组织演变的影响.结果表明:23CrNi3Mo钢动态再结晶的再结晶激活能为293.23 kJ/mol;采用θ-σ模型较精确地获得了发生动态再结晶的临界应变与峰值应变,并确定了其平均比值εc/εp=0.63;确定了材料常数和热变形本构方程.通过对热模拟实验数据的分析和显微组织观察,建立了不同变形条件下动态再结晶模型和晶粒尺寸模型.     

30CrMnSi钢的热变形行为与晶粒演化特征

对于初始粗晶的高强钢30CrMnSi进行了圆柱体热压缩实验研究,获得了该种材料在不同温度不同应变速率条件下的真应力一应变曲线以及动态再结晶和晶粒细化的规律。应用峰值应力的实验结果计算出了该材料热变形过程的激活能以及每个实验条件的Z参数,得到了高强钢30CrMnSi的热变形过程以及动态再结晶过程的主要特征变量作为Z参数的函数表达式。发现在z参数=1．0E＋12／s～1．OE＋13／s、工程应变一60％的条件下动态再结晶会产生较好的晶粒细化效果。     

16Mn钢奥氏体动态再结晶及晶粒细化的研究

本文研究了16Mn 钢奥氏体动态再结晶、晶粒大小、晶粒细化率及γ→α相变后铁素体晶粒大小与工艺参数:变形量ε,变形温度之间的关系。通过大量数据的回归处理,得到奥氏体晶粒细化率在一定温度条件下,与变形量ε之间满足指数函数关系:动态再结晶完成后,奥氏体晶粒平均直径与形变速率温度修正系数 z 之间符合线性关系:γ→α相变后铁素体晶粒大小在一定温度条件下与变形量之间也存在指数函数关系:     

超高强度钢奥氏体相变再结晶的形核机制

运用高温金相和ＴＥＭ方法，对超高强度钢３００Ｍ的奥氏体相变再结晶过程和新晶界进行了定位观察。实验结果表明：在高温金相下，奥氏体相变再结晶晶界横穿过板条组织，而在ＴＥＭ下为高密度位错缠结条带。据试验结果，提出了奥氏体相变再结晶位错形核机制。     

42CrMoA钢热变形过程动态再结晶行为

目的 通过Deform-3D软件模拟42CrMoA钢的热压缩过程,研究在压缩量为60%、变形温度为950~ 1 100 ℃和应变速率为0.01~10 s⁻¹条件下42CrMoA钢再结晶模型的可靠性。方法 将热压缩试样沿轴线对半分开,以试样中心和边部位置作为金相观察区,分析42CrMoA钢的热变形行为,将计算得到的动态再结晶临界模型输入Deform-3D软件的前处理模块中,模拟过程的变形参数与实验过程的相同,通过在模拟试样的心部和边部位置进行点追踪,实现模拟结果和实验结果中组织的对比分析。结果 在压缩过程中42CrMoA钢真应力的变化受加工硬化和动态软化协同作用影响。随着温度的升高,试样心部和边部的再结晶体积分数均有所上升,且试样心部动态再结晶体积分数大于边部的。模拟结果显示,当温度由1 000 ℃升高至1 100 ℃时,试样心部动态再结晶体积分数由75.6%升高至89.5%,在相同条件下,通过金相观察到试样心部的动态再结晶体积分数由73.2%升高至85.3%。结论 基于Johnson-Mehl-Avrami模型改进的Yada再结晶模型可以较好地描述42CrMoA钢的动态再结晶过程,实验结果与模拟结果间的相对误差小于8.35%,验证了动态再结晶模型的准确性。     

300M超高强度钢的奥氏体相变再结晶温度和低倍粗晶的消除

利用高温金相、热处理等手段测定了飞机起落架用超高强度钢３００Ｍ的奥氏体相变结晶温度。试验结果表明，３００Ｍ钢的奥氏体相变再结晶发在一温度区间，此温度区间的高低受加热方式，原始组织的影响，根据试验结果，确定了消除３００Ｍ钢低倍粗晶的热处理工艺。     

一种压力容器用钢动态再结晶行为的研究

本文利用Gleeble 3500热／力模拟试验机,在不同变形温度和变形速率下,对一种压力容器用钢进行单道次热压缩试验。试验结果表明：该种钢在热变形时,同时发生加工硬化和动态再结晶（动态软化）过程。根据试验数据,可以计算出热变形时的动态再结晶激活能。     

23Co13Ni11Cr3Mo超高强钢的高温变形行为

在Glreeble 1500热模拟机上进行大变形等温压缩实验,研究了23Co13Ni11Cr3Mo钢的高温变形行为.结果表明:流变应力随着变形温度的降低和应变速率的升高而增大,在高温、低应变速率下动态再结晶软化效应显著,在温度为1000℃、应变速率为0.001 s-1时流变应力下降29.6％.23Co13Ni11Cr3...     

Dynamic Recrystallization Behavior of a Heat-resistant Martensitic Stainless Steel 403Nb during Hot Deformation

Dynamic recrystallization(DRX) behaviors of a heat-resistant martensitic stainless steel 403Nb during hot deformation have been investigated by single-pass thermo-mechanical simulative experiment at temperatures of 900-1150 C and strain rates of 0.01-1 s 1.The results show that the true stress-true strain curves of this alloy can be classified into two types,one is of dynamic recovery and the other is of dynamic recrystallization.The DRX in 403Nb alloy is easy to occur at strain rates lower than 0.5 s 1 and deformation temperatures higher than 1000 C.Using regression analysis,the stress multiplier(α) and apparent stress exponent(n) were calculated to be 0.0153 and 3.22,respectively,while the activation energy(Q d) for DRX of 403Nb was calculated to be 367.293 kJ/mol.The constitutive equation of peak stress for DRX was also obtained.Based on P-J method,the critical strain for DRX was accurately determined.The mathematical models of peak strain and kinetic equation for DRX of 403Nb steel were finally established.     

Dynamic Recrystallization and Precipitation Behavior of Mn-Cu-V Weathering Steel

The hot deformation behavior of a Mn-Cu-V weathering steel was investigated at temperatures ranging from 850 to 1050℃ and strain rates ranging from 0.01 to 5 s-1 using MMS-300 thermal-mechanical simulator. The activation energy for dynamic recrystallization and stress exponent were calculated to be 551 kJ/mol and 7.73, respectively. The accurate values of critical strain were determined by the relationship between work hardening rate and flow stress (θ-σ) curves. The hyperbolic sine constitutive equation was employed to describe the relationship between the peak stress and Zener-Hollomon parameter during hot deformation. The interaction between dynamic recrystallization and dynamic precipitation of V(C,N) at a low strain rate was analyzed. The results showed that precipitation particles size of weathering steel increased with increasing strain at deformation temperature 950℃ and strain rate 0.1 s-1. The calculation results of the recrystallization driving force and pinning force showed that dynamic precipitation could retard the progress of dynamic recrystallization but not prevent it while the pinning forces is less than driving force. On the contrary, dynamic precipitation can effectively prevent the progress of dynamic recrystallization.     

Investigation of Transformation for Ultrahigh Strength Steel Aermet 100

1. IntroductionUP to now, the investigation of tempering forAF1410 and Aermet 100 steels is generally concentrated on the traditional procedure, i.e., after settinga series of tempering temperatures and tempering fora certain period of time respectively, the microstructure and relationship between the former and mechanical properties are inspectedll~4]. Obviouslys this kindof experimental method does not really reflect thetransformational law in the dynamic course of tempering. Therefore, in…     

Dynamic Recrystallization Behavior of a Fe-Cr-Ni Super-Austenitic Stainless Steel

The super-austenitic stainless steels are extensively utilized in the seamless tubes production for oil extraction industries.Due to the importance of thermo-mechanical processing in the production of these tubes, the dynamic recrystallization(DRX)characteristics of a Cr-Ni super austenitic stainless steel(1.4563)were investigated in the present study.This was performed using the hot compression testing method in the temperature range of 950-1150-C and the strain rate of 10-3-10-1 s-1.The initiation and evo...     

高温退火时间对含铌低温取向电工钢二次再结晶行为的影响

利用OM、SEM、EDS、EBSD等技术观察和分析二次再结晶中断抽出试样的组织和取向.结果表明:高温退火保温时间达到5 h时,部分晶粒发生了二次再结晶,随着二次再结晶持续时间的延长,发生二次再结晶晶粒的数量显著增多,达到25 h时基本形成了完全的二次再结晶组织.Goss织构随保温时间的延长逐渐增多,而{111}〈112〉织构和{411}〈148〉织构含量显著降低,Goss织构含量在退火保温25 h时达到91.1％,其强度达到284.771;抑制剂随高温退火时间的延长逐渐粗化,其对晶界的钉扎逐渐减弱直到完全失去抑制作用.     

Improvement of Toughness of Ultrahigh Strength Steel Aermet 100

1.IntroductionUp to now,the experimental investigation on the ul-trahigh strength steel has been basically limited to the ex-ploration of increasing strength and there have been fewreports on the breakthrough of combination optimiza-tion between strength and toughness[1~6].Moreover,afundamental understanding on some critical microstruc-tural features and the problem of the stability of AR inthe steel are still not clear[1].Generally speaking,the larger fraction of AR formedat higher temperat…     

Cr8钢的动态再结晶行为及组织转变

利用Gleeble-3500热/力模拟试验机对Cr8支承辊用钢在应变速率0.01～1s-1、变形温度950～1 200℃条件下进行了热压缩变形试验,研究了其热变形力学行为和再结晶规律,并对该钢热变形后的显微组织及物相变化进行了分析。结果表明:在应变速率较低为0.01s-1,当变形温度低于1 050℃时,Cr8钢热变形后的组织主要为动态回复型,当变形温度高于1 100℃时,热变形后的组织为动态再结晶型,且随着变形温度的升高,动态再结晶晶粒逐渐长大;当应变速率增加到0.1s-1时,热变形后的组织在温度低于1 050℃时为动态回复型,在温度高于1 100℃时为动态再结晶型;当应变速率增加到1s-1时,变形温度高于1 050℃时,热变形后的组织即发生了明显的再结晶,奥氏体晶粒大部分已长成为等轴的再结晶晶粒;Cr8钢热变形后的物相主要为α-Fe和γ-Fe,显微组织主要为马氏体和残余奥氏体。     

A Model of Dynamic Recrystallization in Alloys during High Strain Plastic Deformation

1.IntroductionVerysmallrecrystallizedgrainswereobservedintheadiabaticshearbandsinmetalswhentheywereheavilydeformedathighstrainrates,whichwerezonesofhighlylocalizedplasticdeformation[1~5].Pak[1]foundthatshearbandsinacommerciallypuretitaniumwereconsistedofsmallgrainsof5o~3Oonmindiameterwithwell-definedboundaries.Chokshi[2],And.ade[3jandHinesI4Jalsoobservedtherecrystal-lizedgrainswith1oO~2Oonmdiameterswithintheshearbandsofcopper.Cho151showedthattherewereequiaxedcellswiththesizesof2oo~5oonminth…