《中国钼业》来稿须知

1刊登范围和要求 本刊主要刊登钼及其共（伴）生金属（钨、铼、金、银、铂、镍、钯、铱、铜、铁、、锌、钙、铅、铀、锡等）的地质、采矿、选矿、冶炼、合金、加工、化工、有价金属回收与利用、设备、分析检测等领域内的”四新”（新产品、新工艺、新技术、新材料）科技与成果,还报道钼市场动态、行业信息、专利技术等。     

《中国钼业》来稿须知

1刊登范围和要求 本刊主要刊登钼及其共（伴）生金属（钨、铼、金、银、铂、镍、钯、铱、铜、铁、、锌、钙、铅、铀、锡等）的地质、采矿、选矿、冶炼、合金、加工、化工、有价金属回收与利用、设备、分析检测等领域内的”四新”（新产品、新工艺、新技术、新材料）科技与成果,还报道钼市场动态、行业信息、专利技术等。     

电感耦合等离子体原子发射光谱法测定高碳除尘灰中11种元素

实验重点探讨了高含量碳对除尘灰样品中镁、铝、钾、钙、铬、锰、铜、钡、铅、镉、锌等元素测定的影响,并解决了除碳的问题。样品使用马弗炉高温除碳,采用盐酸-硝酸-氢氟酸-高氯酸消解样品灰分,选择了镁、铝、钾、钙、铬、锰、铜、钡、铅、镉、锌等元素的分析谱线和扣背景模式,建立了使用电感耦合等离子体原子发射光谱法(ICP-AES)测定高碳除尘灰中镁、铝、钾、钙、铬、锰、铜、钡、铅、镉、锌等元素的方法。在仪器最佳工作条件下,各元素校准曲线线性相关系数r均大于0.999 5,方法检出限在1.08～26.01 mg/kg之间。方法应用于除尘灰实际样品中镁、铝、钾、钙、铬、锰、铜、钡、铅、镉、锌的测定,结果的相对标准偏差(RSD,n=11)为0.90%～7.1%,目标元素的加标回收率为90%～117%;按照实验方法测定除尘灰中镁、铝、钾、钙、锌,结果与火焰原子吸收光谱法(FAAS)的测定结果相吻合。     

《鞍钢技术》投稿须知

正(1)来稿应为针对鞍钢及国内外矿山、焦化、烧结、炼铁、炼钢、轧钢、金属材料、节能环保、耐火材料、能源动力、自动化及仪表、理化检验、综合利用、机电技术等钢铁领域上下游产业链相关的新技术、新装备和新工艺等方面撰写的论文,应做到选题新颖、工艺技术先进、试验研究成果借鉴性强。     

沁阳市沁龙化学防腐有限公司

河南省沁阳市沁龙化学防腐有限公司是从事研制生产多功能新型螺旋溜槽、摇床、旋流分级机、磁选机、浮选机、搅拌槽、打砂机、玻璃钢冷却塔、风机、管道、防腐贮罐等多种产品的专业公司,已有近三十年的生产历史,通过了lS09001:2000质量体系认证,主导产品为多功能新型螺旋溜槽、摇床,是选别有色金属、黑色金属、非金属、贵重金属的理想选矿设备,如金矿、银矿、沙金矿、锅矿、钛铁矿、硫铁矿、赤铁矿、褐铁矿、铬铁矿、钨矿、钽泥矿、煤矿、独居石、蓝宝石、重晶石、金红石、锆英石、硅砂等。现有8000多台设备在全国各地矿山使     

辉光放电光谱法测定因瓦合金中14种元素

采用11种与因瓦合金成分含量相接近的镍基合金标准样品绘制校准曲线,建立了基本不需要样品处理即可对因瓦合金中14种元素(C、Si、Mn、P、S、Ni、Cr、Mo、Cu、Al、Nb、Ti、Co、Fe)同时测定的辉光放电光谱法。确定辉光光谱仪检测因瓦合金的最佳条件:模块电压和相电压分别为8.22 V和3.82 V;功率为70 W;冲洗时间为80 s;积分时间为60 s。以各元素质量分数为横坐标,其对应的光谱强度为纵坐标绘制校准曲线,各元素校准曲线的相关系数均在0.99以上。采用实验方法对因瓦合金实际样品进行分析,结果显示:Cr、Ni、Mo、Ti、Fe的质量分数均大于0.3%,各元素测定值的相对标准偏差(RSD,n=11)均不大于1%;C、Si、Mn、P、S、Cu、Al、Nb、Co的质量分数均小于0.3%,各元素测定值的RSD(n=11)均小于5%。将实验方法应用于对因瓦合金样品中14种元素的测定,测得结果与滴定法测定Ni和Fe、高频燃烧红外吸收法测定C和S、电感耦合等离子体原子发射光谱法测定Si、Mn、P、Cr、Mo、Cu、Al、Nb、Ti和Co元素的结果基本一致。     

《中国钼业》来稿须知

1刊登范围和要求本刊主要刊登钼及其共(伴)生金属(钨、铼、金、银、铂、镍、钯、铱、铜、铁、锌、钙、铅、铀、锡等)的地质、采矿、选矿、冶炼、合金、加工、化工、有价金属回收与利用、设备、分析检测等领域内的"四新"(新产品、新工艺、新技术、新材料)科技与成果,还报道钼市场动态、行业信息、专利技术等。     

《中国钼业》来稿须知

1刊登范围和要求本刊为中国科技核心期刊。主要刊登钼及其共(伴)生金属(钨、铼、金、银、铂、镍、钯、铱、铜、铁、锌、钙、铅、铀、锡等)的地质、采矿、选矿、冶炼、合金、加工、化工、有价金属回收与利用、设备、分析检测等领域内的     

国家拟出台严厉措施淘汰落后产能

国家拟出台进一步加强淘汰落后产能工作的通知,协调发改委、工信部、环保部、国土部、商务部、海关总署、财政部、央行、银监会、质检总局、安监总局、工商总局、电监会、能源局等,以严厉措施,重点完成电力、煤炭、钢铁、水泥、有色、焦炭、造纸、皮革、     

《太钢科技》投稿指南

《太钢科技》是太原钢铁（集团）有限公司根据党和国家的政策、法令创办的,经山西省新闻出版局批准备案的科学技术刊物。主要刊登太钢矿山、耐火、焦化、炼铁、炼钢、连铸、轧钢、锻造、理化检验、能源、机械、土建、计控、自动化、环保、安全等专业以及科研、工艺质量攻关、产品开发、技术开发和技术管理等方面的试验研究、科技成果、技术总结、综合评述和经验介绍等。     

全泥氰化工艺尾水综合回收新工艺

针对全泥氰化工艺尾水开展100t/d工业试验研究,开发纳滤、反渗透二段浓缩铜银络合离子工艺,通过置换、中性萃取、酸性反萃、电积全新工艺技术,在不改变尾水理化性能的条件下,实现了活化游离氰根,提高金、银浸出率,综合回收电积铜的目的。     

Preparation and performance of electrodeposited Ni-TiB₂-Sm₂O₃ composite coatings

Sm2O3 and TiB2 were used as codeposited particles in electrodeposition Ni-TiB2-Sm2O3 composite coatings to improve its performance. Ni-TiB2-Sm2O3 composite coatings were electrodeposited in the nickel sulfate,hexadecylpyridinium bromide and cetyltrimethylammonium bromide solution containing TiB2 and Sm2O3 particles. The content of codeposited Sm2O3 in the composite coating was controlled by changing the concentrations of Sm2O3 particles in the solution. The composite coatings were characterized with X-ray diffraction(XRD) and inductively coupled plasma-atomic emission spectrometer(ICP-AES) . The effects of Sm2O3 content on microhardness,wear weight loss and friction coefficient of composite coatings were investigated,respectively. The microhardness of the Ni-TiB2-Sm2O3 composite coatings was 19.35%,16.58%,2.03% higher than that of the Ni coating,Ni-Sm2O3 and Ni-TiB2 composite coatings,respectively. The wear weight loss of the Ni-TiB2-Sm2O3 composite coatings was 7,2.33,1.22 times lower than that of the Ni coating,Ni-Sm2O3 and Ni-TiB2 composite coatings,respectively. The friction coefficient of the Ni coating,Ni-Sm2O3,Ni-TiB2 and Ni-TiB2-Sm2O3 composite coatings were 0.712,0.649,0.850 and 0.788,respectively. The loading-bearing capacity and the wear-reducing effect of the Sm2O3 particles were closely related to the content of Sm2O3 particles in the composite coatings.     

[(Fe<Subscript>0.5</Subscript>Co<Subscript>0.5</Subscript>)<Subscript>0.75</Subscript>B<Subscript>0.20</Subscript>Si<Subscript>0.05</Subscript>]<Subscript>96</Subscript>Nb<Subscript>4</Subscript> Metallic Glasses with Small Cu Additions

Recently, (Fe-Co)-B-Si-Nb bulk metallic glasses (BMGs) were produced. Such BMGs exhibit high glass-forming ability (GFA) as well as good mechanical and magnetic properties. These alloys combine the advantages of functional and structural materials. The soft magnetic properties can be enhanced by nanocrystallization. To force the nanocrystallization, small content of Cu was added to the starting composition. In this article, {[(Fe_0.5Co_0.5)_0.75Si_0.05B_0.20]_0.96Nb_0.04}_100–x Cu _x glassy alloys (x = 1, 2, and 3) were chosen for investigation. The GFA and the thermal stability of these alloys were evaluated. The effects of crystallization during heat-treatment processes on the phase evolution and the magnetic properties, including M _s , H _c , and T _c , in these alloys were investigated. The phase analyses were done with the help of the X-ray diffraction patterns recorded in situ by using the synchrotron radiation in transmission configuration.     

Study on analysis of crystal structure in CeO₂ doped with Er₂O₃ or Gd₂O₃

To simulate the effects of burnable poison doping in nuclear fuel UO2,Er2O3(or Gd2O3)-doped CeO2 pellets were prepared. Changes in lattice constant and atomic disordering for CeO2 due to the Er2O3 and Gd2O3 doping were measured by means of XRD and XAFS. By the Er2O3 doping,the lattice constant decreased,and a disordering of lattice structure was induced in the samples. The doping with Er2O3 also induced the disordering of atomic arrangement around Er atoms,which was observed through the change in XAFS spectra. In contrast,the effect of Gd2O3 doping was smaller than that of Er2O3 doping. The result was discussed in terms of ionic size of dopants in CeO2 crystal.     

Research on microstructure and magnetostriction of Fe₈₃Ga₁₇Dy_x alloys

The crystal structure,microstructure and the magnetostriction of Fe83Ga17Dyx(x=0,0.2,0.4,0.6) series alloys were studied.The results showed that the influence of the Dy on the crystal structure of the alloy was very small but the effect on the microstructure was significant when different contents of Dy were added into the Fe83Ga17 alloy,respectively.Meanwhile,the magnetostriction of Fe83Ga17Dy0.2 alloy was greatly enhanced,the magnetostriction λ value reached 300×10-6 at 400(kA/m) magnetic field.     

Reduction-Carburization of NiO-WO<Subscript>3</Subscript> Under Isothermal Conditions Using H<Subscript>2</Subscript>-CH<Subscript>4</Subscript> Gas Mixture

Ni-W-C ternary carbides were synthesized by simultaneous reduction–carburization of NiO-WO₃ oxide precursors using H₂-CH₄ gas mixtures in the temperature range of 973 to 1273 K. The kinetics of the gas–solid reaction were followed closely by monitoring the mass changes using the thermogravimetric method (TGA). As a thin bed of the precursors were used, each particle was in direct contact with the gas mixture. The results showed that the hydrogen reduction of the oxide mixture was complete before the carburization took place. The nascent particles of the metals formed by reduction could react with the gas mixture with well-defined carbon potential to form a uniform product of Ni-W-C. Consequently, the reaction rate could be conceived as being controlled by the chemical reaction. From the reaction rate, Arrhenius activation energies for reduction and carburization were evaluated. Characterization of the carbides produced was carried out using X-ray diffraction and a scanning electron microscope (SEM) combined with electron dispersion spectroscopy (SEM-EDS) analyses. The grain sizes also were determined. The process parameters, such as the temperature of the reduction–carburization reaction and the composition of the gas mixture, had a strong impact on the carbide composition as well as on the grain size. The results are discussed in light of the reduction kinetics of the oxides and the thermodynamic constraints.     

Nonverbal behaviors of "good" and "poor" counselors.

Determined whether skills involved in decoding of nonverbal behaviors are related to the clinical skills of the beginning counselor. Two groups of master's level counselor-trainees (N?=?24) served as Ss. One group was judged by the practicum supervisor as "good" (top 20%) and the other was judged as "poor" (bottom 20%) in interviewing skills. Each counselor conducted a 21-min videotaped interview with a client. The counselor's nonverbal behaviors were rated by the client (using the Behavior Rating Form) and were analyzed by 2 training judges on 4 dimensions of nonverbal behaviors. Decoding skills, as measured by a film test (the Profile of Nonverbal Sensitivity), were compared between good and poor groups. Also, client- and judge-rated counselor nonverbal behaviors were compared with decoding skills. Results show no significant difference between good and poor counselors in nonverbal decoding abilities. Counselor nonverbal behaviors, as rated by judges, showed no significant correlations with decoding skills; however, client ratings were inversely related to nonverbal decoding skills. (7 ref) (PsycINFO Database Record (c) 2010 APA, all rights reserved)     

多层级NaHoF4纳米核壳颗粒的制备及其抗癌诊疗

为能够在无Ce掺杂时增强NaHoF4的荧光发射能力,设计制备了Yb3+浓度梯度多层级纳米核壳颗粒,并对其微观形貌、荧光发射能力、相结构及抗癌诊疗效果进行了测试。结果表明,合成的六边形NaHoF4颗粒结晶度良好,尺寸约为20 nm;多层级包覆壳层薄且均匀,该结构的荧光发射强度高于无/单一壳层包覆。980 nm激光照射下,表面修饰Ce6的多层级NaHoF4纳米核壳颗粒在HeLa癌细胞中具有良好的抗癌诊疗作用。     

The effect of CaF<Subscript>2</Subscript> on thermodynamics of CaO-CaF<Subscript>2</Subscript>-SiO<Subscript>2</Subscript>(-MgO) slags

To address the role of CaF₂ in the CaO-CaF₂-SiO₂(-MgO) slag system employed for the production of low-pressure rotor steels, the thermodynamic aspects of the slag were investigated by equilibrating it with liquid iron at 1873 K in CaO or MgO crucibles. Presaturation of slag with an oxide block piece of CaO or MgO in a Pt crucible and application of a carbon paste to the outside of an oxide crucible were designed to prevent crucible failure during the slag-metal experiments. The liquidus isotherm and phase boundary of the preceding slag system were investigated using the slag-metal equilibria. Also, the effect of CaF₂ on the sulfide capacity and the activity coefficient of Fe _t O were of particular interest in controlling the sulfur level and cleanliness of low-pressure rotor steels.