Effects of post-weld heat treatment on microstructure and mechanical properties of friction stir welded joints of 2219-O aluminium alloy

Abstract

Post-weld heat treatment (PWHT) of 2219-O aluminium alloy friction stir welding joints was carried out at solution temperatures of 480, 500 and 540°C for 32 min followed by aging at 130°C for 9 h. The effects of PWHT on the microstructure and mechanical properties of the joints were investigated. Experimental results show that PWHT causes coarsening of the grains in the weld, and the coarsening degree increases with increasing solution temperature. The tensile strength of the heat treated joints increases with increasing solution temperature. The maximum tensile strength can reach 260% that of the base material at the solution temperature of 540°C. PWHT has a significant effect on the fracture locations of the joints. When the solution temperature is lower than 500°C, the joints fracture in the base material; when the temperature is higher than 500°C, the joints fracture in the weld. The change of the fracture locations of joints is attributed to the presence of precipitate free zones beside the grain boundaries and coarsening equiaxed grain structures in the weld.     

2A12铝合金筋板件T型搅拌摩擦焊工艺及焊后热处理

为评价2A12铝合金筋板件搅拌摩擦焊工艺并探寻提高接头强度的途径,进行了2A12铝合金筋板件的T型搅拌摩擦焊焊接工艺试验,并对不同人工时效热处理下焊接接头的微观组织及性能进行了研究.研究表明:采用T型搅拌摩擦焊即可实现2A12铝合金筋板件的成形,当搅拌头旋转速度为750 r/min、焊接速度60mm/min时,接头的抗...     

5083铝合金搅拌摩擦焊接头拉伸行为研究

目的 研究5083铝合金搅拌摩擦焊接（FSW）的组织、力学性能和拉伸应变,分析接头的拉伸行为。方法 采用数码相机、光学显微镜、电子扫描显微镜等表征分析方法,对焊缝的表面宏观成形、微观组织、断口形貌进行分析;利用拉伸机、三维数字动态散斑应变测量分析系统和显微维氏硬度计对接头的力学性能和拉伸应变进行测试。结果 不同焊接工艺参数下FSW接头的最低抗拉强度为305 MPa,断后延伸率达到了14%以上;焊核区拉伸应变沿板厚方向呈现上高下低和上宽下窄的不均匀梯度分布,发生了较大程度的变形强化,直到拉伸应力达到抗拉强度。断裂失效前300/120接头的最大拉伸应变在晶粒粗大的母材区,500/120和500/200接头的最大拉伸应变则位于晶粒尺寸差异较大的后退侧焊核区与热力影响区交界处。接头拉伸断口宏观上均为45°剪切韧性断裂,微观上均以韧窝韧性断裂为主,而高热输入500/120接头出现脆性断裂特征,其延伸率明显降低。结论 高热力耦合输入使铝合金FSW接头薄弱区发生转变,强韧性降低。     

Improvement of weld temperature distribution and mechanical properties of 7050 aluminum alloy butt joints by submerged friction stir welding

Submerged friction stir welding (FSW) in cold and hot water, as well as in air, was carried out for 7050 aluminum alloys. The weld thermal cycles and transverse distributions of the microhardness of the weld joints were measured, and their tensile properties were tested. The fracture surfaces of the tensile specimens were observed, and the microstructures at the fracture region were investigated. The results show that the peak temperature during welding in air was up to 380 °C, while the peak temperatures during welding in cold and hot water were about 220 and 300 °C, respectively. The temperature at the retreated side of the joint was higher than that at the advanced side for all weld joints. The distributions of microhardness exhibited a typical “W” shape. The width of the low hardness zone varied with the weld ambient conditions. The minimum hardness zone was located at the heat affected zone (HAZ) of the weld joints. Better tensile properties were achieved for joint welded in hot water, and the strength ratio of the weld joint to the base metal was up to 92%. The tensile fracture position was located at the low hardness zone of the weld joints. The fracture surfaces exhibited a mixture of dimples and quasi-cleavage planes for the joints welded in cold and hot water, and only dimples for the joint welded in air.     

Effect of welding speed on microstructures and mechanical properties of underwater friction stir welded 2219 aluminum alloy

Underwater friction stir welding (underwater FSW) has been demonstrated to be available for the strength improvement of normal FSW joints. In the present study, a 2219 aluminum alloy was underwater friction stir welded at a fixed rotation speed of 800 rpm and various welding speeds ranging from 50 to 200 mm/min in order to clarify the effect of welding speed on the performance of underwater friction stir welded joint. The results revealed that the precipitate deterioration in the thermal mechanically affected zone and the heat affected zone is weakened with the increase of welding speed, leading to a narrowing of softening region and an increase in lowest hardness value. Tensile strength firstly increases with the welding speed but dramatically decreases at the welding speed of 200 mm/min owing to the occurrence of groove defect. During tensile test, the joint welded at a lower welding speed is fractured in the heat affected zone on the retreating side. While at higher welding speed, the defect-free joint is fractured in the thermal mechanically affected zone on the advancing side.     

Effect of temperature on the fracture behaviour of heat‐treated Al–Cu–Li alloy laser welds under low‐cycle fatigue loading

The paper presents the results of the studies of the effect of temperature on the fracture behaviour of Al–Cu–Li alloy laser welds under low‐cycle fatigue loading. The mechanical properties and the microstructure of the welded joints without and after postweld heat treatment (PWHT) were investigated. The tensile strength and the low‐cycle fatigue resistance of the welded joints were studied at various test temperatures (20°C, 85°C and ? 60°C). It was been found that heating up to 85°C and cooling down to ?60°C reduced the maximum number of loading cycles of the welded joints after PWHT by 1.5–2.0 times compared with that at a test temperature of 20°C.     

Effect of post-weld heat treatment on microstructure and properties of electron beam welded joint of Ti2AlNb/TC11

Abstract

The present paper reports the influence of post-weld heat treatment (PWHT) on microstructure and properties of electron beam welded dissimilar joint. Ti₂AlNb and TC11 alloys were used to fabricate the joints. Three PWHTs were applied to the welded joints. The structures were analysed using optical microscopy, X-ray diffraction, scanning electron microscopy and transmission electron microscopy techniques. The results show that weld metal of the fusion zone is mainly composed of α₂ and β phases. As the energy input increases under different PWHTs, the decomposition degree of metastable phases (α′/β) rises, but the tensile strength and impact toughness of the joint reduce. Under each condition, the tensile strength of the joint is higher than that of the TC11 base metal.     

Identification of the pin offset effect on the friction stir welding (FSW) via Taguchi – Grey relational analysis: A Case study for AA 7075 – AA 6013 alloys

The aim of this work is to present a case study relating to the dissimilar friction stir welding (FSW) ability of AA 7075‐T651 and AA 6013‐T6 by applying pin offset technique. An orthogonal array L18 was conducted to perform the overlapped weld seams using three different values of pin offset, welding speed and tool rotational speed along with two different pin profiles determine the impact of welding parameters on the tensile properties of friction stir welded joints. The nugget zone for each of overlapped weld seams exhibited a complex structure and also, the pin offset and profile also were found to have a great impact on the microstructural evolution of the nugget zone. The ultimate tensile strength, elongation at the rapture and bending strength of welded joints were measured in the ranges of 194–215 MPa, 1.79–3.34 % and 203–352 MPa. From the Taguchi based Grey relational analysis, the optimum welding condition was determined for the welded joint performed using a single fluted pin profile with the zero pin offset, tool rotational speed of 630 min^?1 and welding speed of 63 mm/min. Microstructural and macro‐structural observations revealed that welded joints exhibiting lower tensile strength are consistent of various types of defects (e. g. cracks, tunnels and cavities). The fracture location of welded joints was found to be on the heat affected zone and between the heat affected zone and AA 6013‐base metal. The tool and pin wear was not observed during the welding applications     

Combined effects of post-weld heat treatment and aging on alloy 800/2·25Cr–1Mo steel joint

Abstract

The combined effects of post-weld heat treatment (PWHT) and aging on the interfacial microstructure and tensile properties of alloy 800/2·25Cr–1Mo steel transverse weld specimens, welded using Inconel 182, were studied to determine the optimum PWHT temperature for the joint. In the present study, the joints were subjected to PWHT for 1 h at 948, 973, 998, and 1023 K, followed by aging at 873 K for 100–5000 h. The aging treatment at 873 K is intended to provide an accelerated simulation of service exposure at 773 K. The results of the present work show that the optimum PWHT temperature for the joint investigated is 973 K.

MST/1474     

Joint properties of dissimilar Al6061-T6 aluminum alloy/Ti–6%Al–4%V titanium alloy by gas tungsten arc welding assisted hybrid friction stir welding

Hybrid friction stir butt welding of Al6061-T6 aluminum alloy plate to Ti–6%Al–4%V titanium alloy plate with satisfactory acceptable joint strength was successfully achieved using preceding gas tungsten arc welding (GTAW) preheating heat source of the Ti alloy plate surface. Hybrid friction stir welding (HFSW) joints were welded completely without any unwelded zone resulting from smooth material flow by equally distributed temperature both in Al alloy side and Ti alloy side using GTAW assistance for preheating the Ti alloy plate unlike friction stir welding (FSW) joints. The ultimate tensile strength was approximately 91% in HFSW welds by that of the Al alloy base metal, which was 24% higher than that of FSW welds without GTAW under same welding condition. Notably, it was found that elongation in HFSW welds increased significantly compared with that of FSW welds, which resulted in improved joint strength. The ductile fracture was the main fracture mode in tensile test of HFSW welds.     

Effect of welding parameters on microstructure and mechanical properties of friction stir welded joints of AA7039 aluminum alloy

A high strength Al–Zn–Mg alloy AA7039 was friction stir welded by varying welding and rotary speed of the tool in order to investigate the effect of varying welding parameters on microstructure and mechanical properties. The friction stir welding (FSW) process parameters have great influence on heat input per unit length of weld, hence on temperature profile which in turn governs the microstructure and mechanical properties of welded joints. There exits an optimum combination of welding and rotary speed to produce a sound and defect free joint with microstructure that yields maximum mechanical properties. The mechanical properties increase with decreasing welding speed/ increasing rotary speed i.e. with increasing heat input per unit length of welded joint. The high heat input joints fractured from heat affected zone (HAZ) adjacent to thermo-mechanically affected zone (TMAZ) on advancing side while low heat input joints fractured from weld nugget along zigzag line on advancing side.     

Effect of post-weld heat treatment and electrolytic plasma processing on tungsten inert gas welded AISI 4140 alloy steel

Post-weld heat treatment (PWHT) is commonly adopted on welded joints and structures to relieve post-weld residual stresses; and restore the mechanical properties and structural integrity. An electrolytic plasma process (EPP) has been developed to improve corrosion behavior and wear resistance of structural materials; and can be employed in other applications and surface modifications aspects. In this study the effects of PWHT and EPP on the residual stresses, micro-hardness, microstructures, and uniaxial tensile properties are explored on tungsten inert gas (TIG) welded AISI-4140 alloys steel with SAE-4130 chromium–molybdenum alloy welding filler rod. For rational comparison all of the welded samples are checked with nondestructive Phased Array Ultrasonic Testing (PAUT) and to ensure defect-free samples before testing. Residual stresses are assessed with ultrasonic testing at different distances from weld center line. PWHT resulted in relief of tensile residual stress due to grain refinement. As a consequence higher ductility but lower strength existed in PWHT samples. In comparison, EPP-treated samples revealed lower residual stresses, but no significant variation on the grain refinement. Consequently, EPP-treated specimens exhibited higher tensile strength but lower ductility and toughness for the martensitic formation due to the rapid heating and quenching effects. EPP was also applied on PWHT samples, but which did not reveal any substantial effect on the tensile properties after PWHT at 650 °C. Finally the microstructures and fracture morphology are analyzed using scanning electron microscopy (SEM) and optical microscope to study the evolution of microstructures.     

焊后热处理对AA7204-T4铝合金搅拌摩擦焊接头组织与力学性能的影响

采用搅拌摩擦焊对AA7204-T4铝合金板材进行焊接,研究焊后热处理对FSW接头组织与力学性能的影响。结果表明:焊后(AW)态焊核区平均晶粒尺寸和再结晶分数分别为4.7μm和81.9%,焊后直接人工时效(AA)后二者分别为4.8μm和82.4%,焊后固溶+人工时效(SAA)后分别为5.9μm和86.5%,AA态并未对焊核区的晶粒结构产生明显的影响,而SAA态则使其分别提高了25.5%和5.6%。AW态,AA态和SAA态接头抗拉强度分别为296.6,318.2 MPa和357.4 MPa,AA态对接头力学性能提升有限,而SAA态则有效提升接头力学性能,焊接系数达92.0%。焊后固溶淬火导致接头连接界面"S"线处产生微裂纹,接头断裂于此,且伸长率严重降低。     

AA7075 bit for repairing AA2219 keyhole by filling friction stir welding

In the present study, 7.8 mm thick AA2219 rolled plates were successfully filling friction stir welded (FFSW) without keyhole using a semi-consumable tool. The influences of the bit’s geometric parameters and the plunge speed on the joint’s mechanical properties were investigated. Microstructure of the joint, especially at the interface, was observed. The results revealed that the AA7075 bit’s employment was able to decrease the shedding bit material effectively. During tensile tests, the maximum ultimate tensile strength (UTS) and elongation of the joint were 179.6 MPa and 13.7%, equivalent to 96.6% and 99% of the original defect-free friction stir welding (FSW) joint, respectively. The defect-free FFSW joints were produced at lower plunge speeds, and the fracture locations were at the softened region within the heat affected zone (HAZ) adjacent to the thermo-mechanically affected zone (TMAZ) on the retreating side. With increasing the plunge speed, the fracture location was more mainly dependent on the interface strength instead of the hardness distribution.     

The microstructure and mechanical properties of friction stir welded Al–Zn–Mg alloy in as welded and heat treated conditions

High strength aluminium alloys generally present low weldability because of the poor solidification microstructure, porosity in the fusion zone and loss in mechanical properties when welded by fusion welding processes which otherwise can be welded successfully by comparatively newly developed process called friction stir welding (FSW). This paper presents the effect of post weld heat treatment (T₆) on the microstructure and mechanical properties of friction stir welded 7039 aluminium alloy. It was observed that the thermo-mechanically affected zone (TMAZ) showed coarser grains than that of nugget zone but lower than that of heat affected zone (HAZ). The decrease in yield strength of welds is more serious than decrease in ultimate tensile strength. As welded joint has highest joint efficiency (92.1%). Post weld heat treatment lowers yield strength, ultimate tensile strength but improves percentage elongation.     

Effects of initial oxide on microstructural and mechanical properties of friction stir welded AA2219 alloy

Effects of various initial surface oxide films on microstructural and mechanical properties of friction stir welded (FSW) joints have been studied in the present paper. Anodizing was adopted to produce oxidation on AA2219-T62 surface. A series of friction stir welded joints were produced with various initial surface oxidations to study the effects on microstructural and mechanical properties of the joints. X-ray radiography inspection was conducted to determine the existence of welding defects. Optical microscopy (OM), scanning electron microscope (SEM) and transmission electron microscope (TEM) were used to characterize stir zone features and microstructure. Tensile test was employed to obtain FSW joint mechanical properties. Results show that initial surface oxide film has pronounced effect on the joint line remnant (JLR) distribution, microcosmic appearance and mechanical properties. Further analysis of the JLR particles suggests that the dispersed particles are Al₂O₃ oxide with the characteristics of polycrystalline structure because of the effect of the thermo-mechanical cycles. In addition, tensile strength of FSW joints with JLR inside the stir zone only reached about 60% of a sound FSW joint. Fractography analysis of broken tensile specimens exposed a series of severe “scalloping” correlated with JLR flaw, while sound weld exhibits fine dimples on the fracture surface.     

6005A铝合金挤压型材搅拌摩擦焊接头的疲劳性能

对6005A-T6铝合金挤压型材进行焊速为1000 mm/min的搅拌摩擦高焊速焊接,研究了对接面机械打磨对接头组织和力学性能的影响.结果 表明,与生产中常用的焊前打磨处理相比,尽管对接面未机械打磨的接头焊核区的"S"线更明显,但是两种接头的硬度分布和拉伸性能相当,拉伸时都在最低硬度区即热影响区断裂.高周疲劳实验结果表...     

焊接速度对 7A52 铝合金 FSW 组织及力学性能的影响

目的在保证搅拌速度一定时,针对8 mm厚的7A52铝合金,在不同焊接速度下采用搅拌摩擦焊(FSW)进行焊接试验,研究其焊接接头的显微组织及力学性能。方法利用搅拌摩擦焊机进行对接焊接,焊后制取金相试样观察焊接接头宏观形貌和显微组织,并测定其力学性能。结果7A52铝合金FSW焊接接头焊核区的面积随着焊接速度的增大而增大,当焊接速度为250mm/min时,焊接接头的焊核区面积最大,焊核区的显微组织都为细小的等轴晶,焊接接头横截面的焊核区呈明显"洋葱环"的形貌,而热力影响区的结构特征则呈现出了较高的塑性变形流线层。焊接接头显微硬度分布都呈现出"W"形变化,在焊接速度为150 mm/min时,焊接接头的平均抗拉强度能达到452 MPa,达到了母材抗拉强度的89%。结论通过对不同焊接速度下7A52铝合金FSW焊接接头的组织和性能进行研究,得到了不同焊接速度下焊接接头组织和力学性能。     

Effect of a post-weld heat treatment on the mechanical and microstructure properties of AA6061 joints welded by the gas metal arc welding cold metal transfer method

This work studies the effect of a post-weld heat treatment (PWHT) on the mechanical and microstructure properties of an AA6061 sample welded using the gas metal arc welding (GMAW) cold metal transfer (CMT) method. The CMT method was used because the method provides spatter-free welding, outstanding gap bridging properties, low heat input and a high degree of process flexibility. The welded samples were divided into as-welded and PWHT samples. The PWHTs used on the samples were solution heat treatment, water quenching and artificial aging. Both welded samples were cut according to the ASTM E8M-04 standard to obtain the tensile strength and the elongation of the joints. The failure pattern of the tensile tested specimens was analysed using scanning electron microscopy (SEM). A Vickers microhardness testing machine was used to measure the hardness across the joints. From the results, the PWHTs were able to enhance the mechanical properties and microstructure characteristics of the AA6061 joints welded by the GMAW CMT method.     

Improving tensile strength and bend ductility of titanium/AlSI 304L stainless steel friction welds

Abstract

The metallurgical and mechanical properties of friction welds between titanium and AISI 304L stainless steel were examined. Joint tensile strength increased when high friction pressure (>196 MN m^?2) and high upsetting pressure (294 MN m^?2) were used during welding. Although the surface roughness of the titanium substrate had no effect on joint strength, decreasing the surface roughness of the AISI 304L material did increase the tensile strength of completed joints. As welded dissimilar joints had poor bend test ductility and failed in the interface region. Detailed microscopy and X-ray diffraction analysis confirmed that the poor bend ductility was caused by a combination of high hardness of the titanium material immediately adjacent to the joint interface, the presence of unrelieved residual strain at the joint interface, and intermetallic phases formed during the welding operation. Detailed transmission electron microscopy and X-ray analysis confirmed that a thin layer rich in intermetallics was present in the as welded joints. (FeNiCr)Ti phases were formed during seizure formation and disruption; this provided the necessary conditions for anomalously high rates of diffusion of titanium in stainless steel, and of iron, chromium, and nickel in titanium. Low temperature post-weld heat treatment (PWHT), involving heating to 500–600°C followed by immediate air cooling, reduced intermetallic precipitation, promoted stress relaxation, and facilitated complete bonding across the whole joint interface. This treatment markedly improved bend ductility and had a negligible effect on joint tensile strength. High PWHT temperatures (≥900°C) and long holding times at temperature markedly reduced joint tensile strength and bend ductility, owing to excessive formation of intermetallic phases at the joint interface.

MST/1521