DUST STRANDS IN CYCLONE SEPARATORS AT LOW DUST CONCENTRATION

State of the art in calculating a cyclone separator is the application of the equilibrium theory and taking the formation of dust strands into account as well. The latter process does not depend on particle size mainly. An ideal flow pattern for the formation of dust strands is the so called Dean-vortex: it is being realized favorably in the axial flow cyclone. A dust strand can be produced down to a raw gas concentration C₀ ≈ 10^-5. Then, it is being exhausted through one or few holes in the mantle of the axial cyclone applying bleeding of about 10 % of the volume flow Separating its dust in a bin cyclone and recirculating the binflow gas to the main, axial cyclone completes this high performance cyclone separator. Dimensional analysis shows that the clean gas concentration c₁ mainly depends on the swirl W_tan/w_ax, the raw gas concentration c₀and on Reynolds number. For usual dust conditions a clean gas concentration c₁ ≤ 50 mg/m³ is feasible.     

Numerical Study of Air Compressibility During Horizontal Pneumatic Transport

Using numerical simulations, the effect of the compressibility of air on the flow pattern of particles and pressure drop in the presence of particles during horizontal pneumatic transport operating under negative pressure was examined. The length and inside diameter of the pipeline were 30 m and 40 mm, respectively, and the chosen particles (4 mm in diameter) had densities of ρ_p = 1000 and 2000 kg/m³. The mean air velocities at pipe the inlet were U_inlet = 19, 22, and 28 m/s, and the range of the mass flow rate ratios of particle to air, μ, was varied up to 2.0. For a given inlet air velocity, the difference in the flow pattern between compressible and incompressible flow calculation is generally small. For ρ_p = 1000 kg/m³ particles the additional pressure drop in compressible flow increases when μ is above 0.5 and U_inlet is 28 m/s, μ is above 1.3 and U_inlet is 22 m/s, and μ is above 1.5 and U_inlet is 19 m/s. In these cases, the particle flow pattern is homogeneous. For ρ_p = 2000 kg/m³ particles, the pressure drop increases only when μ is above 1.5 and U_inlet is 28 m/s. The difference is not noticeable when the particle flow pattern is heterogeneous. Also, the difference in the additional pressure drop is much larger during homogeneous flow than heterogeneous flow.     

DISTRIBUTIONS OF THE TANGENTIAL VELOCITIES ON THE DUST LADEN GAS FLOW IN THE CYLINDRICAL CYCLONE DUST COLLECTOR

The authors measured the distributions of the tangential velocities of the feed dust concentration C_o = 0. 6 ~15. 0 g/ m³ by the hot wire anemometers. The test dust was fly-ash which had the mean diameter Xpn = 2.03 μm. The used cylindrical cyclone had the diameter D1 = 140 mm, the diameter of the exit pipe D2 = 50 mn and the total length HT = 382 mm. In order to measure the fluctuating velocities and the time mean velocity on the dust Iaden gas flow and on the pure air flow, we had applied two kinds of the hot-wires. The flow Reynolds number Rec was Rec = Qo/HiV = 797~5582. The expert mental results sho-ed that there were no distinct differences of the time mean and fl uctuating velocities between the pure air flow and the dust laden gas flow. Then the authors have tried to explain those expert mental results by the response time of the fine solid particles and that of the scale of the nixing length in the turbulent rotational air flow.     

FREE SETTLING OF A NON-SPHERICAL PARTICLE IN A STAGNANT LIQUID

The free settling behavior of the cylindrical particles made of four kinds of materials with horizontal motion in the stagnant water observed with an aid of the image sensor anemometer in the Reynolds number ranged from about 150 to 1000 was investigated in this paper. The four kinds of materials were finished into cylindrical specimens having the diameters “d” of 1.5 to 3.0 mm and the ratios of “d” to the length of specimen “1_s” of d/1_s = 1/2 to 1/3.5.

From the experimental results, the settling behavior of the particles was found to be simply expressed by the equation of a simple harmonic motion. By correcting the drag coefficient of the cylindrical particles with a correction factor which is obtained from the simple harmonic motion, the relationship between the drag coefficient and Reynolds number for the cylindrical particles was found to be parallel to that for the spherical particles.     

GAS HOLDUP IN BAFFLED BUBBLE COLUMNS OF DILUTE SLURRIES OF FINE POWDERS AND VISCOUS LIQUIDS

Experimental gas phase holdup data reported by the authors as taken on two baffled bubble columns and involving slurries of fine powders (average particle diameter ≤90 μm) and dilute suspensions (mass fraction ≤ 20 percent) in viscous fluids are re-examined after correction for a small calculation error in superficial gas velocity. The two bubble columns are: a Plexiglas bubble column, 0.108 m in diameter and 2.25 m tall, equipped with seven 19 mm tubes arranged in equilateral triangular configuration with a pitch of 36.5 mm and a Pyrex glass column, 0.305 m in diameter and 3.24 m tall, equipped with thirty-seven 19 mm tubes arranged in the same configuration. Air and nitrogen are used as gas phase, water and Therminol as liquid phase, and iron oxide powders, glass beads and sand as solid phase. The small column data are at ambient temperature while those belonging to the large column extend from ambient to 473K. These data are examined to assess the influence of column diameter (scale-up), temperature, slurry concentration and viscosity, and superficial gas velocity on gas holdup for baffled columns.

It is found that in the 0.108 m diameter column the holdup is about the same for axial probes of different diameters, 19 mm, 31.8 mm and 50.8 mm, for two-phase systems involving liquids of small (water) and large (Therminol) viscosities. However, when a seven-tube bundle is installed, the holdup increases. This is consistent with the bubble dynamics and observed bubble sizes. This qualitative trend is also upheld by three-phase systems involving dilute slurries of fine powders. In the larger column when fully packed with a thirty-seven tube bundle, the holdup is found to be the same as for the small column. A loosely packed bundle gives smaller holdup at temperatures greater than the ambient due to the larger size of bubbles. The gas holdup is greater for a less viscous system and this is again due to the larger size of bubbles in a more viscous system. The influence of temperature is pronounced and is very characteristic of the nature of liquid involved. For example for water and Therminol the variations are in opposite directions with change in temperature. Bubble splitting and foaming control the nature of these dependencies. With the addition of solids the holdup is almost insignificantly altered at all temperatures.     

CFD Studies of Indoor Airflow and Contaminant Particle Transportation

This article presents a numerical study of indoor airflows and contaminant particle transportation in three ventilated rooms. The realizable k - ε model is employed to model the air-phase turbulence, while the Lagrangian particle tracking model is utilized for the particle-phase simulation. The predicted air-phase velocities and contaminant particle concentrations are validated against the experimental data obtained from the literature. In the first case, the realizable k - ε model successfully captures the flow trend and reasonably predicts the airflow velocity. The realizable k - ε model under-predicts the vertical air velocities along the vertical inlet jet axis by 11% at x = 0.219 m, which is slightly better than the standard k - ε model error of 17%. In a two-zone room case, the realizable k - ε model, combined with a Lagrangian particle tracking model, predicts the particle concentration decay with the highest normalized difference being 24%. In the third case, the influence of particle size, location of particle resource, and particle-wall collision on the particle concentrations is investigated by the realizable k - ε model and the Lagrangian model. It is found that for relatively small particles (diameter ≤ 10 μm), the particle concentration may be insensitive to the particle diameter. In addition it has been observed that the particle-collision model may have considerable effect on the particle concentration prediction.     

Surface Topography Analysis When High-Speed Rough Milling Hardened Steel

This study is part of a bigger picture on investigating three main cutter path strategies—raster, single-direction raster, and offset—in order to evaluate the feasibility of employing high axial depths of cut (10 mm ≤ A_d ≤ 20 mm) when high-speed rough milling hardened AISI H13 hot work tool steel with the aim of achieving high volume of metal removed with short machining time. Here, comparative studies were made of the surface topography maps induced at various axial depths of cut in order to gain an in-depth understanding of their effects on the surface texture obtained via the parametric study of alternative cutter path strategies. Previous work has shown that the use of an offset cutter path strategy when high-speed rough milling hardened steel using an axial depth of 15 mm resulted in the lowest tool life, as compared with the use of raster and single-direction raster strategies.[1]This article also describes a novel approach on improving the offset cutter path strategy by selecting the proper entrance and exit conditions to improve surface texture. The effects of an offset strategy and a modified offset strategy are investigated in terms of surface roughness and surface texture.     

MASS TRANSFER OF SULFUR DIOXIDE TO CONDENSING AQUEOUS AEROSOLS

Sodium chloride aerosols were generated from a 1.0 percent solution and passed through a tubular furnace, then recondensed at 29°C in a cooling section in the presence of SO₂. The dry particles ranged from 0.711 to 0.843 µm and the condensed droplets were in the 1.66 to 2.88 µm range. Final droplet size was varied by controlling the temperature of the nebulizer solution between 17 and 50°C. The SO₂ concentration in the gas phase of the condensing cloud was varied between 0.5x10 - ³ and 2.5 xl0 - ³ atm.

Cloud droplets were separated from the gas stream in a point-to-plane electrostatic precipitator and the droplets analyzed colorimetrically for total sulfur content.

Concentrations of SO₂ in the aqueous phase were about one order of magnitude greater than values obtained from equilibrium constants. The collection rate of SO₂ at 29°C appeared to be first order in SO₂ gas phase concentrations.

A model for this process was constructed, based on the hydrate formation in the gas-water interface[SO₂]_g + n[H₂O]ℓ ⇋ [SO₂ · n(H₂O)]ℓ

The order of the hydrate n was estimated to be 4.0.     

Influence of a Weak Magnetic Field on Photoconductivity Spectrum of C60 Single Crystal

Comparative research of the excitation photoconductivity spectra (quantum light energy 2-5 eV) of C₆₀ single crystal in and out of magnetic field at the temperature T = 250-350 K has been carried. The spectral evolution at this temperature range is described. It is shown that the spectra changes abrupt at temperature T₁ ∼ 260 K and T₂ ∼ 315 K. An increase in the photoconductivity up to 15% was observed in the magnetic field (B = 0.4 T) within the photon energy range 2.5-4.5 eV. Local photoconductivity peak's appearances in the magnetic field have been proven that the charge transfer excitons take part in a photoconductivity.     

Investigation of CdTex and Cd1-xZnxTe Schottky Barrier Diode Structure Based γ-Ray Detectors

Cadmium Telluride (CdTe) and Cadmium Zinc Telluride (CdZnTe) based detectors have been developed for hard X-ray and γ -ray detection. These semiconducting materials have high resistivity because of the wide bandgap and also have high photon absorption efficiency because of the large atomic number (Z_Cd = 48, Z_Te = 52). CdTe and CdZnTe substrates (7 mm × 9 mm × 0.5 mm) with different stoichiometry were taken for the fabrication of γ-ray detectors. The substrate was prepared by polishing the bulk crystals grown by the rotational Bridgman method. Crystals with maximum electrical resistivity were grown in this way. For fabrication of Schottky barrier diode structures, the Schottky contacts were made by electroless deposition for gold (Au) and thermal evaporation for Indium (In). The Au/CdTe/In and Au/CdZnTe/In Schottky barrier diodes were linked to the charge sensitive preamplifier by gold wires. Then, I-V measurement and detector efficiency like charge collection performance with energy resolutions were analyzed at room temperature by using ⁵⁷Co and ¹³⁷Cs gamma sources. The good energy resolutions of ⁵⁷Co (122 KeV) and ¹³⁷Cs (662 KeV) sources are obtained for both CdTe and CdZnTe diode detectors.     

Some problems involving distributions of screw dislocations in a finite slab

This paper considers two problems involving distributions of screw dislocations in a finite slab. The first problem is concerned with the spread of plasticity from a crack ¦x₁¦c, x₂ = 0 in the finite slab ¦x₂¦ h/2 subject to an externally applied shear stress p₂₃ = σ, and is treated in terms of the theory of continuous distributions of dislocations. The extent to which the dislocations describing the plastic relaxation spread from a crack tip is determined, together with the relative displacement of the crack surfaces at its tips. Thus the criterion for crack extension is calculated, particular attention being given to the case when fracture occurs at low applied stresses. The second problem studied is the special case of the first problem that arises when no plastic relaxation is allowed; the criterion for crack extension is then determined from energetic considerations; the similarity between the two sets of results for low stress fractures is emphasized.     

EFFECT OF PARTICLE SIZE DISTRIBUTION ON TRANSFER EFFICIENCY AND APPEARANCE IN POWDER COATINGS

Three powder samples of identical chemistry were taken from the same lot under different conditions: (1) relatively wide size distribution (Sample A) d₅₀ = 18.1μm, (2) narrow size distribution, d₅₀ = 22.4μm (Sample B), and (3) wide size distribution with more fines than Sample A, d₅₀ = 15.1μm (Sample C). Within this relatively minor variation of Particle Size Distribution (PSD) with respect to d₅₀, the appearance of the powder with minimum d₅₀ (15.1μm) was best. The results show two trends: (1) PSD with d₅₀ about 15μm can result in excellent appearance (GM Tension in the range of 18 to 19 on a scale of 0 to 20), and (2) the width of the distribution need not be narrow when d₉₀ is less than 40μm.

Polymer powders in this size range do not fluidize well without agitation, but when vibration was applied, all three samples had R values (fluidity) 200 or above, which is adequate for fluidization and transport. The maximum R value was obtained for Sample A, which had the widest size distribution. Thus, the fluidity tests agreed with the expected results.     

Factorial Modeling for Transient Solid Particle Velocity in a Fluidized Bed Combustor Cold Model

Transient hydrodynamics phenomena in the fluidized bed combustor (FBC) freeboard have been critical in the past two decades. Within a 152 mm ID FBC cold model, solid particle transient velocities were measured and analyzed with the assistance of advanced laser-based particle image velocimetry (PIV) instrumentation. Two layers of swirling secondary air were injected into the cold model. The PIV system was applied to the FBC cold model to visualize transient solid particle velocity. A series of transient solid particle velocity profiles were generated for the factorial analysis. In each profile, the solid particle velocity vectors (Vx and Vy) for 10 × 10 grids were generated. Analysis of variance (ANOVA) was used to determine the significant factors that affect transient solid particle velocities, time, and position coordinates. Then, the 10¹⁰ factorial design method was used to develop a specific empirical model of transient solid particle velocity in the FBC freeboard, which was in the shape of V_x = f₁(t, x, y) and V_y = f₂(t, x, y).

This unique factorial analysis method proved to be a very effective and practical method to evaluate experimental conditions and analyze experimental results in the FBC systems.     

RE-ENTRAINMENT OF DUSTS FROM THE DUST LAYER ON THE THE DEPOSITED DUSTS IN THE CYCLONE DUST COLLECTORS

There were many papers concerning the experimental results of the collection efficiency, but up to this time there are a few papers concerning the experimental results of the re-entrainment or dispersion of the dust particles from the dust layer by the turbulent rotational air flow in the dust bunker for the cyclone dust collector. Then in this paper, the author described the experimental results of the re-entrainment of the test dust ( talc X_R50 = 8.O µm ) for the four kinds of the throat diameter D₃ = 50, 80, 100 and 150 mm. Especially it is very importance to take into consideration of flow rate Qb into the dust bunker which is a function of D₃ and cyclone diameter D₁ and the maximum tangential velocity Vet in the dust bunker which depends on D₁,D₃ and Qb.     

LED Lighting Configurations for Visual Inspection of IC Packages

This article discusses configurations of light-emitting diode (LED) light sources for visual inspection of integrated circuit (IC) packages. A package visual inspection (PVI) system with multiple LED light sources used for inspection of IC packages was designed. The image contrast changes of the sample IC packages are explained using the Torrance-Sparrow (TS) model. A few conclusions on appropriate lighting configurations for inspection of various IC packages are achieved. The TS model can be used to represent the specular lobe component. The contrast between two surfaces with different surface roughness values increases with increasing θ_i (incident light angle). Lighting C (θ_i = 75°) is recommended for packages with high surface roughness heights and resin materials. Lighting B (θ_i = 60°) is recommended for packages with moderate surface roughness heights and metal materials. If the background is white, the use of light sources A (θ_i = 15°) and B simultaneously is recommended. Light sources A and C are recommended to be chosen for packages with low surface roughness values and transparent materials. The experimental results with the actual gray-level values of the images are compared to support the conclusions. The PVI system is part of an inspection machine. All images of the sample IC packages reported in this article were obtained from an actual production line. Therefore, the results are close to those of the actual inspection situation in the manufacturing industry.     

Synthesizing and Physical Properties of GdPr-123 High-Tc Superconductor

Ceramic Gd_1-xPr_xBa₂Cu₃O_7-y (GdPr-123) high-T_c superconductors have been synthesized by the standard solid state reaction method and characterized by XRD, SEM, TGA, and DT techniques in the range of x, 0.0 ≤ x ≤ 1.0 Samples have orthorhombic structure with Pmmm symmetry and there is a small percentage (less than 1%) of the Ba sites occupied by Pr ions in some Pr-rich samples. In these samples a small trace of BaCuO₂ and Pr BaO₃ secondary phases persist with the main peaks at 2θ = 29.3° and 28.9° respectively. Microstructure analysis indicates a uniform grain size distribution with a mean size of 5 μm. No significant change of grain size is shown throughout the range of x studied. The valence of Pr and Cu were determined by magnetization measurements in the temperature range 100 to 250°K. These data reveal a valence of 3.86+ for Pr in all samples independant of x. The similarity of the superconducting and insulating properties in this system to those of the oxygen deficient RBa₂Cu₃O₇ (R-123) (R: Y or rare earth) system implies that the mechanism of superconductivity in high-T_c. superconductors cannot be two-dimensional, even though the superconductive current occurs in two dimensions.     

Impact and penetration by L/D ≤ 1 projectiles

Calculations of steel target penetration by L/D ≤ 1 tungsten and tungsten alloy projectiles have been extended to L/D = 1/32 over the velocity range 1.5 to 5 km/s. The ratio of crater to projectile diameter tends to 1 as L/D decreases over this entire velocity range. For impact velocities of 1.5 and 3 km/s, penetration depth normalized by projectile length, P/L, increases with decreasing projectile L/D up to a maximum value and then decreases for still lower L/D. Experiments at impact velocities of 2 and 3 km/s confirm these results. For 5 km/s impact velocity, the calculations show P/L increasing with decreasing projectile L/D over the entire range 1/32 ≤ L/D ≤ 1. The projectile L/D for which the maximum P/L occurs appears to depend on the impact velocity. P/L generally scales with impact velocity as P/L v^f(L/D) where f(L/D) ranges from 0 for a long rod to, we believe, 2 in the limit as projectile L/D approaches zero. The calculations show for 1/8 ≤ L/D ≤ 1/2, P/L v^0.9; for L/D = 1/16, P/L v^1.5; and for L/D = 1/32, the new results give P/L v^1.9.     

The Indiana silicon sphere 4π charged-particle detector array

A low threshold charged particle detector array for the study of fragmentation processes in light-ion-induced reactions has been constructed and successfully implemented at the IUCF and Saturne II accelerators. The array consists of 162-triple-element detector telescopes mounted in a spherical geometry and covering 74% of 4π in solid angle. Telescope elements are composed of (1) an axial-field gas ionization chamber operated with C₃F₈ gas; (2) a 0.5 mm thick passivated silicon detector, and (3) a 2.8 cm thick CsI(Tl) scintillation crystal with photodiode readout. Discrete element identification is obtained for ejectiles up to Z 16 over the dynamic range 0.7 ≤ E/A ≤ 95 MeV/nucleon. Isotopes are also distinguished for H, He, Li and Be ejectiles with 8 E/A 95 MeV. Custom-designed electronics are employed for bias supplies and linear signal processing. Data are acquired via a CAMAC/VME/Ethernet system.     

Comparison between measurements on Rayleigh scattering and form-factor theories for 1 Å ≤ x ≤ 50 Å

From our measured differential cross section of Rayleigh scattering, the form factor for momentum transfers in the range 1 Å⁻¹ ≤ x ≤ 50 Å⁻¹ was deduced. Data for U, Pb, Pt, W, Sn, Cd, Ag, Mo and Cu at energies from 60 to 662 keV and scattering angles ranging from 5° to 140° were used. In addition, for the region 1 Å⁻¹ ≤ x ≤ 50 Å⁻¹ of momenta, experimental data from other authors at higher energies were analyzed. The experimental values obtained were compared with various form-factor theories and limits of validity are established. For the relativistic modified form factor G a good agreement always exists for θ ≤ 65°, independently of energy and atomic number.     

Enhancement of gene transfer to cervical cancer cells using transferrin-conjugated liposome

Transferrin-conjugated cationic liposome (T_f -DDAB liposome) was developed as a targeted gene delivery system by using heterobifunctional cross-linking agent, N-succimidyl-3-(2-pyridyldithio)propionate (SPDP), and gradient metrizamide ultracentrifugation method. Physico-chemical properties of T_f -liposome were determined by scanning/transmission electron microscopy (SEM/TEM) and dynamic laser-light scattering method (DLS) with a mean diameter of 584±15 nm. Gel retardation assay was performed using various DDAB:DNA ratios, and proved that the 6:1 weight ratio formulation gave the most neutralized complex. In vitro transfection was done in human cervical cancer cells, HeLa, and the transfection efficiency of T_f -liposome was found to be fivefold higher than that of unconjugated (plain) DDAB liposome and twofold higher than that of Lipofectin™. In conclusion, a target-oriented T_f -DDAB liposome was made successfully and proved to be very efficient in DNA delivery into the cervical cancer cells in culture.