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本文用高温固相反庆法合成了(Sr1- x Mx )2P2O7 ∶Sn (3.3×10- 2)和(Sr0.9Mg0.1)2P2O7∶xSn 两个体系系列样品,在紫外线激发下,详细测定了它们的激发和发射光谱,讲座了Mg 含量对(Sr1- xMgx)2P2O7∶Sn 和Sn 含量对(Sr0.9Mg0.1)2P2O7∶xSn 体系发光性能的影响。 相似文献
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以碳酸钙、氧氯化锆、氧化铟为原料,用pH=8.5~9.5的草酸-氨水溶液作沉淀剂,并加入适量的表面活性剂,制得了成分准确、颗粒均匀、分散性好的CaZr_(1-x)In_xO_(3-α)的前驱物。该沉淀物经1000℃,3h煅烧即可生成CaZr_(1-x)In_xO_(3-α)相;此产物经1600℃,8h时烧结,得到相对密度大于95%的致密烧结体。测量了烧结体在湿空气中的阻抗谱并提出了合理的等效电路,得到CaZr_(1-x)In_xO_(3-α)的本体电导率与温度和组成的关系。 相似文献
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化学沉淀法除去废水中的氨及其机理的研究 总被引:5,自引:0,他引:5
了用化学沉淀除去废水中的氨,探讨了不同沉淀剂如Mg(OH)2+H3PO4或MgHPO4,不同初始Mg(OH)2:h3PO4摩尔比,不同PH值及初始氨浓度对氨除去效率的影响。 相似文献
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带有一个反凸约束的线性规划,其可行域一般是非凸不连通集,因而这是一类困难的全局解问题。在回顾了已有的理论和方法之后,给出了这个问题的一个切割-转轴算法。算法收敛到或有限步内终止于问题的全局解。并且给出了执行算法的例子。 相似文献
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本文报道用于甲基丙烯醛(MAL)选择氧化制甲基丙烯酸(MAA)的PMoV杂多酸盐催化剂的研究结果。IR和XRD考察结果表明,本文所研究的催化剂均具有稳定的Keggin结构,催化剂物相组成为H(4-2y-2)PO4(MoO3)(12-x)(VO3)xCUyCsz。在300℃,原料气组成MAL:H2O:O2:N2=1:10:3:32.体积空速1200h(-1)的条件下,最佳催化剂的MAL转化率为94.1%,MAA选择性达88.7%。 相似文献
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在PH5.3~7.1的六次甲基四胺缓冲溶液中,Al(Ⅲ)—CAS—CPB—TritonX—100络合物的最大吸收波长为630nm,ε=1.10x10 ̄5L.mol ̄(-1).cm ̄(-1),摩尔组成比Al(Ⅲ):CAS:CPB=1:3:3,铝量在0.2~8μg/25mol范围内符合比尔定律,回收率99~104%。本法以盐酸羟胺和邻菲啉作联合掩蔽剂,常见金属离子干扰少,用本法测定自来水、废水中微量铝,结果令人满意。 相似文献
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固定化细胞生产L-苹果酸新工艺及动力学研究 总被引:2,自引:0,他引:2
对产氨短杆菌MA-2固定化细胞在富马酸铵体系中转化生成L-苹果酸的优化工艺条件做了探讨,结果表明,富马酸铵浓度为1.8mol/L,pH7.0~8.0,反应温度为37℃时,L-苹果酸得率达200g/L左右。同时,对固定化细胞的动力学进行了研究,结果为:r(max)=58mmol/(L·h·g固定化湿细胞)),Km=6.25×1O ̄(-2)mol/L,P_m=1.56mol/L 相似文献
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证明了1个定理:若预先给定的正整数对(x,y)满足:x≥384088,y是偶数,且73788x≤y≤9258010429x-192877,则可以构造1个一般型的极小代数曲面Ⅹ,使Ⅹ具有预先给定的陈不变量C21(X)=y,χ(X)=x,且Χ具有纤维化。 相似文献
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A SIMULATION OF A MOTIONLESS MIXER 总被引:2,自引:0,他引:2
Continuous laminar mixing in segmented twisted-tape motionless mixers is considered. A solution to the steady isothermal creeping flow of a Newtonian fluid in a twisted-tape mixer has been obtained via two-dimensional numerical procedures. The developed flow within a section of the mixer has been solved in a helical coordinate system by an iterative scheme. The resulting solution is rigorously correct in the absence of entrance and exit flows at the junction between sections. An algorithm is presented for the modelling of these junction flows via two-dimensional procedures. Simulated cross-sectional mixing patterns have been generated for comparison with experimental results
The performance of twisted-tape mixers is simulated for various designs, beginning with the particular geometry of the Kcnics Static Mixer, and for different operating conditions Results suggest that the rate of mixing as a function of the total twist per section is optimized with respect to pressure drop when sections contain 80 degrees of twist. The capability for rational improvement in other design and operating parameters is illustrated. The mechanisms of laminar mixing are discussed and quantified; of primary importance is the tendency for interfacial area to assume an orientation within each section which is favorable to mixing in subsequent sections. 相似文献
The performance of twisted-tape mixers is simulated for various designs, beginning with the particular geometry of the Kcnics Static Mixer, and for different operating conditions Results suggest that the rate of mixing as a function of the total twist per section is optimized with respect to pressure drop when sections contain 80 degrees of twist. The capability for rational improvement in other design and operating parameters is illustrated. The mechanisms of laminar mixing are discussed and quantified; of primary importance is the tendency for interfacial area to assume an orientation within each section which is favorable to mixing in subsequent sections. 相似文献
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The activated sludge process is widely used to treat domestic and industrial wastewater. A significant drawback of this process is the production of “sludge”, the disposal of which can comprise a significant proportion of the total operating costs of a wastewater treatment plant. We analyze the steady-state operation of a membrane bioreactor system (MBR) incorporating a sludge disintegration unit (SDU) to reduce sludge production. We provide a qualitative understanding of the model by finding analytically the steady-state solutions of the model and determining its stability as a function of the residence time. In practice a target value of the mixed liquor suspended solids (MLSS) content within the membrane reactor is specified. Applying the mathematical technique of singularity theory we show that if the sludge disintegration factor is sufficiently high then the MLSS content is guaranteed to be below the target value. This model prediction, of key interest from a practical perspective, was not identified in the original investigation of this model, which relied upon numerical integration of the governing equations. 相似文献
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在浮法玻璃生产过程中,氮气流量保持恒定,是保持锡槽工况稳定的重要条件,是生产优质浮法玻璃的重要前提条件之一.只有制氮设备的稳定运行,才能保证氮气供应.本文就制氮空压机运行中出现的故障现象、原因进行了分析,并提出了改进措施. 相似文献
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Mauri Soininen 《Drying Technology》1985,3(2):153-170
Drying of thin paper sheet on a Yankee cylinder equipped with a steam heated high velocity hood is examined. When possible infiltration of air from the surroundings is considered, then the process is fully determined by twelve variables. One of these can be chosen as an independent variable. An equation group of eleven equations is derived. The method of solution is iterative. Finally, a numerical demonstration example is presented. 相似文献