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对钼的极谱性能已有较多的研究,提出了好些微量钼的极谱测定体系[1~6],但未见钼-邻苯二酚紫-溴化十六烷基三甲基铵-氯酸钾的极谱测定体系的报道;经试验,我们发现在这体系中Mo(Ⅵ)产生良好的二阶导数极谱波,其峰电位为-0.58V(vs.SCE),向体系加入一定量EDTA后,Fe(Ⅲ)的干扰被消除,不用分离可直接用于钢中微量铝的测定,结果满意。1实验部分1.1主要仪器和试剂JP-2型示波极谱仪,三电极系统;pHS-2型酸度计。邻苯二酚紫:0.02%溶液;溴化十六烷基三甲基铵:0.06%溶液;氯酸钾… 相似文献
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本文以Pt电极作指示电极,W电极作参比电极,在氨性介质中,以K_3Fe(CN)_6滴定Co ̄(2+)以后,继而利用Fe(CN)/Fe(CN)作指示离子,在pH5.5~6.0,用Zn ̄(2+)返滴定EDTA,连续测定Ni ̄(2+)或Ni ̄-Cu含量,再用硫酸肼作Cuy ̄(2-)的释放剂,Zn ̄(2+)返滴定释放出的EDTA测定Cu ̄(2+),实现了Co-Ni-Cu连续测定。镍精矿样分析的相对标准偏差和试样中标准回收率分别为Co:1.4%,99.5±1.2%。Ni:1.1%,100.1±0.9%。Cu:2.0 相似文献
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在聚乙烯醇(PVAVA)存在下,铱与钼酸盐和罗丹明B(RB)形成离了缔合物。缔台物的最大吸收位于570nm摩尔吸光系数ε8.36×10 ̄5’L·mol ̄-1·cm ̄-1,服从比尔定率范围为0~2.75μglr/25ml。测定2.0μg铱的相对标准偏差为2.5%(n=7),检出限43n/ml(n=12)。测定铱的适宜条件为CHClO_4=0.93mol/L,C_MoO ̄2-_49.0×10~-4mol/L,C_RB=3.3×l0 ̄-5mol/L,PVAO08%。试验了30多种共存离子的影响,除形成杂多酸元素 相似文献
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实验结果表明,M17铸造高温合金(%:0.16C、8.79Cr、5.79A1、4.93Ti、3.29Mo、15.20Co、0.78V、0.015B、0.073Zr、0.002S、0.001P、0.001 1O、0.001 0N)经25 kg真空感应炉返回重熔后,Si含量随重熔次数的增加而略有增加,合金中主要元素和其它杂质元素S、P、H的含量变化不大,而氧、氮略有增加;合金中初生碳化物由新合金中的草书体逐渐向返回合金块状转变,初生碳化物的遗传性堵塞合金凝固时的补缩通道,使返回料合金的疏松倾向增大,高温塑性下降较大。 相似文献
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<正>Minmetals Resources acquired the world’s largest copper mine under construction for USD5.85 billion.One after another,listed companies Jien Nickle,China Molybdenum and Chihong Zinc and Germanium raised money to get involved in overseas mining projects…SOEs and private enterprises are engaged in a frenzy of overseas mine purchasing.A reporter with Economic 相似文献
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正Judging from China’s copper consumption field,the biggest consumption unit is electric power,which accounts for 47%of total consumption;it is followed by light industry sector,including household electrical appliance,machinery,durable goods and hardware etc,which accounts for 22%of total consumption;followed by transportation field, 相似文献
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《China Nonferrous Metals Monthly》2014,(10)
正In 2013,the Central Geological Prospecting Fund(CGPF)Project newly discovered 15 ore fields,including 3 large above ore fields,and 5medium sized ore fields.The reporter learned from the recently published"Annual Report of Central Geological Prospecting Fund Project(2013)"that,from 2006 to 2013 the CGPF 相似文献
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《China Nonferrous Metals Monthly》2014,(10)
正This year,the investment growth rate of real estate industry continued to slow down,sold area of commercial housing also dropped significantly,which brought huge pressure to the domestic air conditioning manufactures.In the first half of the year,by relying on high growth in national financial expenditure,along with investment in public infrastructure 相似文献
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《China Nonferrous Metals Monthly》2014,(10)
正Kang Yi,Honorary Chairman of China Nonferrous Metals Industry Association,said recently at the Forum on Development of the Non-ferrous Metals Industry in Central and Western China held in Zhengzhou that,as more and more electrolytic aluminum factories in Xinjiang came into operation,the electrolytic aluminum output of Xinjiang had reached2,275,000 tons in the first 7 months this year, 相似文献
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《China Nonferrous Metals Monthly》2014,(12)
正"Xinjiang project has been completed according to schedule,but total completion and total start of production are two different concepts,after completion it still needs a gradual process of reaching production target."On the morning of November 3,Shenhuo Coal Industry and Electricity Power told investors the above statement on the investor interaction platform. 相似文献
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正The reporter learned from Guangdong Province Precious Metal Transaction Center that in 2013the Center maintained healthy development momentum,and had become the second largest precious metal transaction platform in China in terms of market size;currently Guangdong is quickening steps of financial innovation for the Center,aiming to build a transaction center with international core competitiveness. 相似文献