紫草油及紫草素油的含量测定方法研究

目的:建立紫草油及紫草素油的含量测定方法。方法:紫草油采用RP-HPLC法,C18色谱柱(4.6×250mm,5μm),检测波长为516nm;紫草素油采用RP-HPLC法,C18色谱柱(4.6×250mm,5μm),检测波长为516nm或277nm,紫草素油也可采用UV-Vis法,检测波长516nm。结果:对各种方法进行专属性、线性、精密度、重复性、溶液稳定性、回收率、检测限、定量限的验证,结果均良好。结论:紫草油的质量控制方法可采用RP-HPLC法;紫草素油的质量控制方法可采用RP-HPLC法及UV-Vis法,优先使用UV-Vis法。     

紫草烧伤喷雾剂研制及药效学实验

目的研制紫草烧伤喷雾剂并进行初步药效学实验。方法选择最优工艺制备紫草烧伤喷雾剂,对其有效成分左旋紫草素进行定性鉴别和含量测定作为质量控制,采用实验性烧烫伤模型考察喷雾剂的治疗作用。结果工艺流程合理,制剂质量稳定,质检方法可控;动物实验表明,其具有抗炎促进创伤愈合的作用,缩短烫伤愈合时间显著提高。结论紫草烧伤喷雾剂工艺合理,质量可控,对烧烫伤具有治疗作用。     

吸附树脂R－A在提取紫草细胞培养液中紫草色素上的应用

采用吸附树脂Ｒ－Ａ回收紫草细胞培养液中的紫草色素．与传统石油醚萃取法相比有机溶剂节约５０倍，且操作简单，生产设备缩小．同时为Ｒ－Ａ树脂的应用增添了一项新内容．     

顶空气相色谱法测定紫草素中的乙醇残留

建立一种用于测定紫草素中的乙醇含量的顶空气相色谱法,采用异丙醇为内标,内标曲线法进行测定.对溶剂、色谱柱温度、样品的平衡温度、样品的平衡时间等因素进行考察,筛选出最合适的条件.对分析方法的专属性、线性、重复性、回收率、溶液稳定性、检测限、定量限进行验证.结果表明,本法专属性良好,在0.1mg·mL-1～2mg·mL-1...     

冷轧薄宽带钢局部型中浪瓢曲变形行为研究

针对薄宽带钢冷轧过程中易发多发的局部型中浪瓢曲缺陷,引入非均匀载荷宽度、弹性约束系数及平均张应力建立了屈曲变形的解析计算模型。应用能量最低原理对屈曲变形区域进行搜索求解,得到了局部型中浪屈曲临界条件(包括临界应力、屈曲波长和屈曲波宽),获得了其与非均匀载荷宽度、弹性约束系数、平均张应力的关系,并发现平均张应力是产生局部型中浪的重要影响因素。应用样条有限元方法对局部型中浪进行数值仿真分析,验证了屈曲解析计算方法的正确性。在实验轧机上进行了轧制研究,通过轧制获得了局部型中浪屈曲模态,对实验结果分析得到了相对应的屈曲临界条件,与解析法和样条有限元法结果基本吻合,证明了样条有限元计算方法与解析计算方法的正确性及其工程应用价值。     

A VIBRATION RECOGNITION METHOD BASED ON DEEP LEARNING AND SIGNAL PROCESSING

Effective vibration recognition can improve the performance of vibration control and structural damage detection and is in high demand for signal processing and advanced classification.Signal-processing methods can extract the potent time-frequency-domain characteristics of signals;however,the performance of conventional characteristics-based classification needs to be improved.Widely used deep learning algorithms(e.g.,convolutional neural networks(CNNs))can conduct classification by extracting high-dimensional data features,with outstanding performance.Hence,combining the advantages of signal processing and deep-learning algorithms can significantly enhance vibration recognition performance.A novel vibration recognition method based on signal processing and deep neural networks is proposed herein.First,environmental vibration signals are collected;then,signal processing is conducted to obtain the coefficient matrices of the time-frequency-domain characteristics using three typical algorithms:the wavelet transform,Hilbert-Huang transform,and Mel frequency cepstral coefficient extraction method.Subsequently,CNNs,long short-term memory(LSTM)networks,and combined deep CNN-LSTM networks are trained for vibration recognition,according to the time-frequencydomain characteristics.Finally,the performance of the trained deep neural networks is evaluated and validated.The results confirm the effectiveness of the proposed vibration recognition method combining signal preprocessing and deep learning.     

INFLUENCE OF DAMPING MODELS ON DYNAMIC ANALYSES OF A BASE-ISOLATED COMPOSITE STRUCTURE UNDER EARTHQUAKES AND ENVIRONMENTAL VIBRATIONS

Structural design simultaneously governed by earthquakes and environmental vibrations has received a lot of attention in recent years.Base-isolated composite structures are typically used in the above-mentioned structural design.The corresponding analysis involves validating structural safety under earthquakes and human comfort under environmental vibrations through a time-history analysis.Thus,a reasonable damping model is essential.In this work,the representatives of viscous damping model and rate-independent damping model,namely the Rayleigh damping model and uniform damping model,were adopted to investigate the influence of damping models on the time-history analysis of such structural designs.The energy dissipation characteristics of the above-mentioned damping models were illustrated via a dynamic test of recycled aggregate concrete specimens.A case study was performed on a base-isolated steelconcrete composite structure.The dynamic responses under the excitation of earthquakes and environmental vibrations were compared using different damping models.The uniform damping model was found to be more flexible than the Rayleigh damping model in dealing with excitations with different frequency components.The uniform damping model is both theoretically advantageous and easy to use,demonstrating its potential in dynamic analysis of structures designed simultaneously governed by earthquakes and environmental vibrations.     

数字3D电影最新动向

全球数字3D电影领域的领头羊Real D公司于10月17日与欧洲投资商Terra Firma公司旗下在泛西欧拥有1600块银幕的Odeon院线以及UCI院线签署协议,将于未来2年中在英国、爱尔兰、德国、奥地利以及葡萄牙合作安装500块数字3D银幕.     

第十二届中国建筑企业高峰论坛在绍兴市举行王治安主持会议并致辞

<正>本刊讯2014年12月23日,由中国建设报社、浙江省住房和城乡建设厅、绍兴市人民政府主办的第十二届中国建筑企业高峰论坛在绍兴市举行。来自全国各地的建筑行业主管部门、行业协会负责人,专家学者及企业代表等300余人齐聚一堂,围绕"创新融合,开放共赢"主题,共同分享了一场建筑行业思想盛宴。中国建设报社党委书记杜久才、社长翟建和中国建筑装饰协会会长李秉仁、中国土木工程协会副理事长刘     

9.3大阅兵:高标准让军魂荡气回肠

<正>阅兵是展示辉煌的时刻,而为这一辉煌采取的所有的标准,不啻也是宝贵的财富,应当成为践行标准的榜样……这个月最令人难忘、最引人自豪、最提振国威的事情,当属"9.3"大阅兵,它有着以往没有的多重的亮点:首次以纪念抗日战争暨世界反法西斯战争胜利为阅兵主题,彰显维护和平是全世界人民共同的愿望。首次邀请外国军队代表参加分列式,体现纪念大会的国际性。首次组织抗战老兵包括国民党老兵参加,体现了对历史的尊重,体现全民族抗战的特色。首次编组英模部队方队受阅,展示中国共产党在抗战中定海     

Insertion of triangulated surfaces into a meccano tetrahedral discretization by means of mesh refinement and optimization procedures

In this paper, we present a new method for inserting several triangulated surfaces into an existing tetrahedral mesh generated by the meccano method. The result is a conformal mesh where each inserted surface is approximated by a set of faces of the final tetrahedral mesh. First, the tetrahedral mesh is refined around the inserted surfaces to capture their geometric features. Second, each immersed surface is approximated by a set of faces from the tetrahedral mesh. Third, following a novel approach, the nodes of the approximated surfaces are mapped to the corresponding immersed surface. Fourth, we untangle and smooth the mesh by optimizing a regularized shape distortion measure for tetrahedral elements in which we move all the nodes of the mesh, restricting the movement of the edge and surface nodes along the corresponding entity they belong to. The refining process allows approximating the immersed surface for any initial meccano tetrahedral mesh. Moreover, the proposed projection method avoids computational expensive geometric projections. Finally, the applied simultaneous untangling and smoothing process delivers a high‐quality mesh and ensures that the immersed surfaces are interpolated. Several examples are presented to assess the properties of the proposed method.     

Certification Institutions Expected to Update and Transfer Information on Present Standards

Standards are the basis for production enterprises to organize production, ex-factory inspection, trade (delivery) and technical exchanges, product certification, quality arbitration and supervision.……     

Flow calorimeter for enthalpy increment measurements on condensed gases

A flow calorimeter for enthalpy increment measurements on condensed gases is presented. A better knowledge of the properties of the liquefied natural gas is needed, and therefore a liquid loop has been designed for our flow calorimeter. The fluid loop in the calorimeter is designed in order to avoid the two-phase region, since two phases would give compositional disturbances in the measurements. The avoidance of the two-phase region is made possible by increasing the pressure of the test fluid after the measurement section, then heating the fluid at super-critical pressure past the critical point. Finally, the fluid is throttled to the low-pressure gas state at the inlet condition of the compressor that circulates the fluid. To perform the pressure increase, a new cryogenic pump has been designed. To evaluate the new equipment, measurements were taken on liquid ethane over the temperature range 146–256 K at pressure between 0.9 and 5.1 MPa.     

Refrigerators Enter a New Era of Health Preservation Frestech initiates the establishment of China's first standard for household sterilization refrigerators

On November 30, 2007, the China Association for Standardization (CAS) held a press conference at Beijing Diaoyutai State Guest House. Leaders from the China Household Electric Appliance Research Institute, the China Household Electric Appliance Association, and the China Consumers' Association attended and made speeches.……     

Optimum-Simulation von Ernteprozessen

Zusammenfassung Bei der Gestaltung von Ernteprozessen — beispielsweise des Prozesses Mähdrusch, Körnertransport und -abnahme — als transportverbundene Fließarbeitsverfahren mit mindestens zwei verschiedenen Arbeitsmitteln gibt es einen großen Optimierungsspielraum. Solche Prozesse sind mehrstufige Bedienungsprozesse mit gemischter Anordnung der Bedienungseinrichtungen. Außerdem besitzen sie stark ausgeprägte räumliche Aspekte. Es wird vor allem gezeigt, welche Merkmale solcher Prozesse in Simulationsmodellen abgebildet sein müssen, welche Zielgrößen in Abhängigkeit von welchen Einflußgrößen unter Berücksichtigung welcher Prozeßbedingungen ermittelt werden sollten und wie der Bewertungsprozeß zur Ermittlung der gewünschten Informationen gestaltet werden muß.     

A study of centrifugal cast high boron high speed steel

In the present study a high‐boron high speed steel (HSS) roll material was designed. Many expensive alloy elements have been substituted by cheap boron alloy, and high‐boron high speed steel roll has been manufactured by centrifugal casting method. The microstructures, mechanical properties and wear resistance of centrifugal casting high‐boron high speed steel roll have been investigated by optical microscopy (OM), scanning electron microscopy (SEM), and X‐ray diffraction (XRD) analysis, hardness test, impact test and wear test. The results indicated that the solidification microstructures of high‐boron high speed steel roll consisted of M₂(B,C), (W,Mo)₂(B,C), M₃(B,C), M₂₃(B,C)₆ type borocarbides and martensite, a small amount of retained austenite. Borocarbides were continuously distributed over the grain boundary. After quenching from 1050 °C, local broken network appeared in partial borocarbides, and fine secondary borocarbide precipitated from the matrix. After tempering from 525 °C, the amount of precipitated borocarbide increased significantly. After heat treatment, the hardness of high‐boron high speed steel roll excelled 60 HRC, and its impact toughness excelled 8.0 J/cm². The single groove steel rolling amount of high‐boron high speed steel rolls increases by 500% than that of bainite cast iron roll, when the rolls are used in K₁ mill housing of bar mill.     

Thixotropy of Systems with Shear Thinning and Plastic Flow Behavior

The definition of the thixotropy is a decrease in viscosity with time in shear and a subsequent recovery of viscosity after the shear deformation is removed.We ...     

Brainstorming for ISO Strategy 2016-2020

正Responding to ISO’s appeal for survey for the to-be-developed ISO Strategy Plan for 2016-2020,SAC hosted a special workshop over the needs and comments of various fi elds on June 8 in Beijing.The workshop was attended by ISO President-elect and Ansteel General Manager Zhang Xiaogang,SAC Vice-Administrator Yu Xinli,and 30 experts from     

CNAS Passes APLAC's PTP Review

正The review group of Asia Pacific Laboratory Accreditation Cooperation(APLAC)carried out a 4-day peer review of the proficiency testing provider(PTP)for China National Accreditation Service for Conformity Assessment(CNAS)from July 28 to 31,2014.CNAS passed the PTP review with excellent performance.Two senior peer reviewers of APLAC made a comprehensive,rigorous and detailed review of CNAS’s PTP accreditation activities,and made the on-spot inspection of the review groups in Shanghai and Shenzhen respectively.