Experimental study on tensile property of AZ31B magnesium alloy at different high strain rates and temperatures

As the lightest metal material, magnesium alloy is widely used in the automobile and aviation industries. Due to the crashing of the automobile is a process of complicated and highly nonlinear deformation. The material deformation behavior has changed significantly compared with quasi-static, so the deformation characteristic of magnesium alloy material under the high strain rate has great significance in the automobile industry. In this paper, the tensile deformation behavior of AZ31B magnesium alloy is studied over a large range of the strain rates, from 700 s⁻¹ to 3 × 10³ s⁻¹ and at different temperatures from 20 to 250 °C through a Split-Hopkinson Tensile Bar (SHTB) with heating equipment. Compared with the quasi-static tension, the tensile strength and fracture elongation under high strain rates is larger at room temperature, but when at the high strain rates, fracture elongation reduces with the increasing of the strain rate at room temperature, the adiabatic temperature rising can enhance the material plasticity. The morphology of fracture surfaces over wide range of strain rates and temperatures are observed by Scanning Electron Microscopy (SEM). The fracture appearance analysis indicates that the fracture pattern of AZ31B in the quasi-static tensile tests at room temperature is mainly quasi-cleavage pattern. However, the fracture morphology of AZ31B under high strain rates and high temperatures is mainly composed of the dimple pattern, which indicates ductile fracture pattern. The fracture mode is a transition from quasi-cleavage fracture to ductile fracture with the increasing of temperature, the reason for this phenomenon might be the softening effect under the high strain rates.     

Constitutive modeling of deformation in high temperature of a forging 6005A aluminum alloy

The 6005A aluminum alloy is one of the most widely used alloys in aeronautic and railway industries, yet its plastic deformation behavior under hot compression is still not fully understood. Isothermal compression tests of 6005A aluminum alloy were performed using a Gleeble-1500 device, up to a 70% height reduction of the sample at strain rates ranging from 0.01 s⁻¹ to 10 s⁻¹, and deformation temperatures ranging from 573 K to 773 K. Several modeling approaches, including flow stress–strain curves, a constitutive Arrhenius-type equation model, and processing maps were used to characterize the deformation behavior of the isothermal compression of 6005A aluminum alloy in this study. The related material constants (i.e. A, β and α) as well as the activation energy Q for 623–773 K and 573–623 K temperature regimes were determined. Two sets of constitutive exponent-type equations for the 6005A aluminum alloy were proposed. Furthermore, a change in deformation mechanism occurred when changing the temperature range from 623–773 K to 573–623 K.     

Hot tensile deformation behaviors and constitutive model of 42CrMo steel

The hot tensile deformation behaviors of 42CrMo steel are studied by uniaxial tensile tests with the temperature range of 850–1100 °C and strain rate range of 0.1–0.0001 s⁻¹. The effects of hot forming process parameters (strain rate and deformation temperature) on the elongation to fracture, strain rate sensitivity and fracture characteristics are analyzed. The constitutive equation is established to predict the peak stress under elevated temperatures. It is found that the flow stress firstly increases to a peak value and then decreases, showing a dynamic flow softening. This is mainly attributed to the dynamic recrystallization and material damage during the hot tensile deformation. The deformation temperature corresponding to the maximum elongation to fracture increases with the increase of strain rate within the studied strain rate range. Under the strain rate range of 0.1–0.001 s⁻¹, the localized necking causes the final fracture of specimens. While when the strain rate is 0.0001 s⁻¹, the gage segment of specimens maintains the uniform macroscopic deformation. The damage degree induced by cavities becomes more and more serious with the increase of the deformation temperature. Additionally, the peak stresses predicted by the proposed model well agree with the measured results.     

The mechanical properties of ionoplast interlayer material at high strain rates

Ionoplast material has been recently introduced and extensively used as interlayer material for laminated glass to improve its post-glass breakage behavior. Due to its sound mechanical performance, the applications of laminated glass with ionoplast interlayer have been widely extended to the protection of glass structures against extreme loads such as shock and impact. The properties of this material at high strain rates are therefore needed for properly analysis and design of such structures. In this study, the mechanical properties of ionoplast material are studied experimentally through direct tensile tests over a wide strain rate range. The low-speed tests are performed using a conventional hydraulic machine at strain rates from 0.0056 s⁻¹ to 0.556 s⁻¹. The high strain-rate tests are carried out with a high-speed servo-hydraulic testing machine at strain rates from approximately 10 s⁻¹ to 2000 s⁻¹. It is found that the ionoplast material virtually exhibits elasto-plastic material properties in the strain rate range tested in this study. The testing results show that the material behavior is very strain-rate dependent. The yield strength increases with strain rate, but the material becomes more brittle with the increase in strain rate, with the ultimate strains over 400% under quasi-static loading, and decreasing to less than 200% at strain rate around 2000 s⁻¹. The testing results indicate that simply applying the static material properties in predicting the structure responses of laminated glass with ionoplast interlayer subjected to blast and impact loads will substantially overestimate the ductility of the material and lead to inaccurate predictions of structure response. The testing results obtained in the current study together with available testing data in the literature are summarized and used to formulate the dynamic stress–strain curves of ionoplast material at various strain rates, which can be used in analysis and design of structures with ionoplast material subjected to blast and impact loads.     

Texture evolution and dynamic mechanical behavior of cast AZ magnesium alloys under high strain rate compressive loading

In this study, texture and compressive mechanical behavior of three cast magnesium alloys, including AZ31, AZ61 and AZ91, were examined over a range of strain rates between 1000 and 1400 s⁻¹ using Split Hopkinson Pressure Bar. Texture measurements showed that after shock loading, initial weak texture of the cast samples transformed to a relatively strong (00.2) basal texture that can be ascribed to deformation by twinning. Furthermore, increasing the aluminum content in the alloys resulted in increase in the volume fraction of β-Mg₁₇Al₁₂ and Al₄Mn phases, strength and strain hardening but ductility decreased at all strain rates. Besides, it was found for each alloy that the tensile strength and total ductility increased with strain rate. By increasing the strain rate, the maximum value of strain hardening rate occurred at higher strains. Also, it is suggested that a combination of twinning and second phase formation would affect the hardening behavior of the cast AZ magnesium alloys studied in this research.     

High temperature tensile deformation behavior and failure mechanisms of an Al–Si–Cu–Mg cast alloy — The microstructural scale effect

In this study the high temperature tensile deformation behavior of a commercial Al–Si–Cu–Mg cast alloy was investigated. The alloy was cast with two different cooling rates which resulted in average secondary dendrite arm spacing of 10 and 25 μm, which is typical of the microstructure scale obtained from high pressure die casting and gravity die casting. Tensile tests were performed at different strain rates (10^− 4 s^− 1 to 10^− 1 s^− 1) and over a wide temperature range from ambient temperature to 500 °C. The fine microstructure had superior tensile strength and ductility compared to the coarse microstructure at any given temperature. The coarse microstructure showed brittle fracture up to 300 °C; the fracture mode in the fine microstructure was fully ductile above 200 °C. The fraction of damaged particles was increased by raising the temperature and/or by microstructure coarsening. Cracks arising from damaged particles in the coarse microstructure were linked in a transgranular-dominated fashion even at 500 °C. However, in the fine microstructure alloy the inter-dendritic fracture path was more prevalent. When the temperature was raised to 300 °C, the concentration of alloying elements in the dendrites changed. The dissolution rates of Cu- and Mg-bearing phases were higher in the fine microstructure.     

The hot deformation behavior and processing map of Ti–47.5Al–Cr–V alloy

The high temperature flow behavior of as-extruded Ti–47.5Al–Cr–V alloy has been investigated at the temperature between 1100 °C and 1250 °C and the strain rate range from 0.001 s^− 1 to 1 s^− 1 by hot compression tests. The results showed that the flow stress of this alloy had a positive dependence on strain rate and a negative dependence on deformation temperature. The activation energy Q was calculated to be 409 kJ/mol and the constitutive model of this material was established. By combining the power dissipation map with instability map, the processing map was established to optimize the deformation parameters. The optimum deformation parameter was at 1150 °C–1200 °C and 0.001 s^− 1–0.03 s^− 1 for this alloy. The microstructure of specimens deformed at different conditions was analyzed and connected with the processing map. The material underwent instability deformation at the strain rate of 1 s^− 1, which was predicted by the instability map. The surface fracture was observed to be the identification of the instability.     

Effects of initial grain size on hot deformation behavior of commercial pure aluminum

The effects of initial grain size of commercial pure aluminum on hot deformation behavior were investigated using hot compression tests. The hot compression tests were carried out on the pure aluminum samples with the initial grain sizes of 50, 150 and 450 μm using various strains, strain rates and different deformation temperatures. It was found that the hot deformation behavior of used material was sensitive to deformation conditions and initial microstructure. Results indicate that the initial grain size has significant effect on the flow stress. Flow stress decreases when the grain size decreases from 450 to 50 μm and when strain rate is lower than 0.05 s⁻¹. This procedure is reversed at strain rate of 0.5 s⁻¹. Furthermore, effects of other parameters like the strain rates and deformation temperatures on the flow stresses and hardening rates were investigated. It was also found that the inhomogeneity of microstructure distribution at different positions of the deformed specimens depended on the amount of deformation concentration at particular points and other processing parameters such as initial grain sizes, strain rates and deformation temperatures. In addition the geometric dynamic recrystallization (GDRX) was observed in the specimens highly strained (0.7) at elevated temperature (500 °C) using polarized light microscope and sensitive tint (PLM + ST).     

Effects of strain rate and temperature on the tension behavior of polycarbonate

Tension stress–strain responses of polycarbonate are presented for strain rates of 1 × 10⁻³ s⁻¹–1700 s⁻¹ and temperatures ranging from −60 to 20 °C. The high rate tension tests are performed using a split Hopkinson tension bar apparatus. The influence of strain rate and temperature on the tension behavior of polycarbonate is investigated. Experimental results indicate that the tension behavior of polycarbonate exhibits nonlinear characteristics and rate-temperature sensitivity. The values of yield strength and strain at yield increase with the increase of strain rate and decrease with increasing temperature. A viscoelastic constitutive model consisting of a nonlinear spring and a nonlinear Maxwell element is proposed to characterize the rate and temperature dependent deformation behavior of polycarbonate prior to yielding.     

Mechanical behavior and deformation micromechanisms of polypropylene nonwoven fabrics as a function of temperature and strain rate

The mechanical behavior and the deformation and failure micromechanisms of a thermally-bonded polypropylene nonwoven fabric were studied as a function of temperature and strain rate. Mechanical tests were carried out from 248 K (below the glass transition temperature) up to 383 K at strain rates in the range ≈10⁻³ s⁻¹ to 10⁻¹ s⁻¹. In addition, individual fibers extracted from the nonwoven fabric were tested under the same conditions. Micromechanisms of deformation and failure at the fiber level were ascertained by means of mechanical tests within the scanning electron microscope while the strain distribution at the macroscopic level upon loading was determined by means of digital image correlation. It was found that the nonwoven behavior was mainly controlled by the properties of the fibers and of the interfiber bonds. Fiber properties determined the nonlinear behavior before the peak load while the interfiber bonds controlled the localization of damage after the peak load. The influence of these properties on the strength, ductility and energy absorbed during deformation is discussed from the experimental observations.     

Effect of the thermal cycle on the hot ductility and fracture mechanisms of a C–Mn steel

Transverse cracking on the surface of continuously cast steel products has been one of the main problems of this stage in steelmaking for many years. The incidence of this problem has been found in microalloyed steels as well as in some plain carbon steels containing residual elements. In this work, the hot ductility and fracture mechanisms of a C–Mn steel containing 0.6%Cu and 0.053%Sn as residual elements have been evaluated. To simulate the thermo-mechanical conditions of the straightening operation, tensile tests were carried out at temperatures ranging from 700 to 1100 °C with an initial strain rate of 5 × 10⁻³ s⁻¹. Specimens were subjected to three different reheating temperatures prior to the hot ductility test, including 1100 °C, 1330 °C and melting. After each test, the reduction in area of the samples tested to fracture was used as a measure of the hot ductility. The fracture surfaces were then examined by scanning electron microscopy. The widest and deepest ductility trough was obtained for the specimens tested after melting; for these conditions brittle fractures are interdendritic showing very low ductility. After reheating at 1330 °C, fracture features showed intergranular fracture combined with some plastic deformation corresponding to the test temperature. Reheating at 1100 °C produced a finer microstructure and the fracture features showed a mixture of intergranular with some interdendritic features. Also, ductile behaviours were associated with void coalescence. The different results obtained depending on the thermal cycle can be attributed to the presence of the residual elements in the steel through different segregation and precipitation patterns.     

Tensile deformation behavior of spray-deposited FVS0812 heat-resistant aluminum alloy sheet at elevated temperatures

The tensile deformation behavior of spray deposited FVS0812 heat-resistant aluminum alloy sheet was studied by uniaxial tension tests at temperatures ranging from 250 °C to 450 °C and strain rates from 0.001 to 0.1 s^− 1. The associated fracture surfaces were examined by scanning electron microscopy (SEM). The results show that the degree of work-hardening increases with decreasing temperature, and exhibits a small decrease with increasing strain rate; the strain rate sensitivity exponent increases with increasing temperature. The flow stress increases with increasing strain rate but decreases with increasing temperature. The total elongations to fracture increase not only with increasing temperature, but also with increasing strain rate, which is in marked contrast with the normal inverse dependence of elongation on the strain rate exhibited by conventional aluminum alloy sheets. The SEM fracture analysis indicates that the dependence of elongation on the strain rate may be due to the presence of a transition from plastic instability at lower strain rates to stable deformation at higher strain rates for fine-grained materials produced by spray deposition.     

Experimental study on the dynamic tensile behavior of a poly-crystal pure titanium at elevated temperatures

A new technique for measuring dynamic tensile behavior of metallic materials at elevated temperatures was developed. This technique employs a rapid contact heating method to obtain a stable and nearly homogenous high temperature field in the testing gage of the specimen. As an application of this new technique, a commercially pure titanium (CP-Ti) was tested in the strain rate range of 300 s⁻¹–1400 s⁻¹ and in a temperature range of 298 K–973 K. Quasi-static experiments (10⁻³ s⁻¹, 10⁻² s⁻¹) were also performed in the same temperature range for comparison. The testing results indicated that both temperature and strain rate have pronounced influence on the mechanical behavior of CP-Ti.     

Experimental study on influence of section thickness on mechanical behavior of die-cast AM60 magnesium alloy

Influence of section thickness on mechanical behavior of die-cast AM60 magnesium alloy has been experimentally studied. Tension, compression and shear tests with this material were performed on a universal test machine at strain rates from 5 × 10⁻⁴ s⁻¹ to 5 × 10⁻² s⁻¹. Specimens were cut from plates with five as-cast section thicknesses of 6.5 mm, 5.2 mm, 3.9 mm, 2.6 mm and 1.3 mm. According to the test results, flow stress becomes less sensitive to section thickness with larger section thickness, and the influence of strain rate on flow stress is also decreasing with larger section thickness. At different stress states, the tested material follows the von-Mises yield criterion. And stress state is found to be the main factor influencing the fracture behavior.     

Modeling quasi-static and high strain rate deformation and failure behavior of a (±45) symmetric E-glass/polyester composite under compressive loading

Quasi-static (1 × 10⁻³–1 × 10⁻² s⁻¹) and high strain rate (∼1000 s⁻¹) compressive mechanical response and fracture/failure of a (±45) symmetric E-glass/polyester composite along three perpendicular directions were determined experimentally and numerically. A numerical model in LS-DYNA 971 using material model MAT_162 was developed to investigate the compression deformation and fracture of the composite at quasi-static and high strain rates. The compressive stress–strain behaviors of the composite along three directions were found strain rate sensitive. The modulus and maximum stress of the composite increased with increasing strain rate, while the strain rate sensitivity in in-plane direction was higher than that in through-thickness direction. The damage progression determined by high speed camera in the specimens well agreed with that of numerical model. The numerical model successfully predicted the damage initiation and progression as well as the failure modes of the composite.     

Analytical and experimental studies on mechanical behavior of composites under high strain rate compressive loading

An analytical method is presented for the prediction of compressive strength at high strain rate loading for composites. The method is based on variable rate power law. Using this analytical method, high strain rate compressive stress–strain behavior is presented up to strain rate of 5000 s⁻¹ starting with the experimentally determined compressive strength values at relatively lower strain rates. Experimental results were generated in the strain rate range of 472–1957 s⁻¹ for a typical woven fabric E-glass/epoxy laminated composite along all the three principal directions. The laminated composite was made using resin film infusion technique. The experimental studies were carried out using compressive split Hopkinson pressure bar apparatus. It was generally observed that the compressive strength is enhanced at high strain rate loading compared with that at quasi-static loading. Also, compressive strength increased with increasing strain rate in the range of parameters considered. Analytically predicted results are compared with the experimental results up to strain rate of 1957 s⁻¹.     

Relationship between mechanical properties and microstructural response of 6061-T6 aluminum alloy impacted at elevated temperatures

The high temperature impact properties and microstructural evolution of 6061-T6 aluminum alloy are investigated at temperatures ranging from 100 to 350 °C and strain rates ranging from 1 × 10³ to 5 × 10³ s⁻¹ using a compressive split-Hopkinson pressure bar (SHPB) system. It is found that the flow response and microstructural characteristics of 6061-T6 aluminum alloy are significantly dependent on the strain rate and temperature. The flow stress and strain rate sensitivity increase with increasing strain rate or decreasing temperature. Moreover, the temperature sensitivity increases with both increasing strain rate and increasing temperature. The flow stress–strain response of the present 6061-T6 alloy specimens can be adequately described by the Zerilli–Armstrong fcc model. The grain size and dislocation cell size increase significantly with a decreasing strain rate or an increasing temperature. The higher flow stress is the result of a smaller grain size and smaller dislocation cell size. The stacking fault energy of the deformed specimens has a value of 145.78 mJ/m².     

Impact and fracture response of sintered 316L stainless steel subjected to high strain rate loading

This paper describes the use of a material testing system (MTS) and a compressive split-Hopkinson bar to investigate the impact behaviour of sintered 316L stainless steel at strain rates ranging from 10^− 3 s^− 1 to 7.5 × 10³ s^− 1. It is found that the flow stress–strain response of the sintered 316L stainless steel depends strongly on the applied strain rate. The rate of work hardening and the strain rate sensitivity change significantly as the strain rate increases. The flow behaviour of the sintered 316L stainless steel can be accurately predicted using a constitutive law based on Gurson's yield criterion and the flow rule of Khan, Huang and Liang (KHL). Microstructural observations reveal that the degree of localized grain deformation increases at higher strain rates. However, the pore density and the grain size vary as a reversible function of the strain rate. Impacts at strain rates higher than 5.6 × 10³ s^− 1 are found to induce adiabatic shear bands in the specimens. These specimens subsequently fail as a result of crack propagation along the dominant band. The fracture surfaces of the failed specimens are characterized by dimple-like structures, which are indicative of ductile failure. The depth and the density of these dimples are found to decrease with increasing strain rate. This observation indicates a reduction in the fracture resistance and is consistent with the observed macroscopic flow stress–strain response.     

Failure of AA 6061 and 2099 aluminum alloys under dynamic shock loading

Microstructural aspects of the deformation and failure of AA 6061 and AA 2099 aluminum alloys under dynamic impact loading are investigated and compared with their responses to quasi-static mechanical loading in compression. Cylindrical specimens of the alloys, heat-treated to T4, T6 and T8 tempers, were subjected to dynamic compressive loading at strain rates of between 2800 and 9200 s⁻¹ and quasi-static compressive loading at a strain rate of 0.0032 s⁻¹. Plastic deformation under the dynamic impact loading is dominated by thermal softening leading to formation of adiabatic shear bands. Both deformed and transformed shear bands were observed in the two alloys. The shear bands offer preferential crack initiation site and crack propagation path in the alloys during impact loading leading to ductile shear fracture. While cracks propagate along the central region of transformed bands in AA 6061 alloy, the AA 2099 alloy failed by cracks that propagate preferentially along the boundary region between the transformed shear bands and the bulk material. Whereas the AA 2099 alloy shows the greatest propensity for adiabatic shear banding and failure in the T8 temper condition, AA 6061 alloy is most susceptible to formation of adiabatic shear bands and failure in the T4 temper. Deformation under quasi-static loading is dominated by strain hardening in the two alloys. Rate of strain hardening is higher for naturally aged AA 6061 than the artificially aged alloy, while the strain hardening rate for the AA 2099 alloy is independent of the temper condition. The AA 2099 alloy shows a superior mechanical behaviour under quasi-static compressive loading whereas the AA 6061 shows a higher resistance to impact damage.     

Effect of Zn addition,strain rate and deformation temperature on the tensile properties of Sn–3.3 wt.% Ag solder alloy

Stress–strain characteristics of the binary Sn–3.3 wt.% Ag and the tertiary Sn–3.3 wt.% Ag–1 wt.% Zn solder alloys were investigated at various strain rates (SR, ε^·) from 2.6 × 10^− 4 to 1.0 × 10^− 2 s^− 1 and deformation temperatures from 300 to 373 K. Addition of 1 wt.% Zn to the binary alloy increased the yield stress σ_y and the ultimate tensile stress σ_UTS while a decrease of ductility (total elongation ε_T) was observed. Increasing the strain rate (ε^·) increased both σ_y and σ_UTS according to the power law σ = C ε^·m. A normal decrease of ε_T with strain rate was observed according to an empirical equation of the form ε_T = A exp (− λε^·); A and λ are constants. Increasing the deformation temperature decreased both σ_y and σ_UTS in both alloys, and decreased the total elongation ε_T in the Zn-free binary alloy, whereas ε_T was increased in the Zn-containing alloy. The activation energy was determined as 41 and 20 kJ mol^− 1 for these alloys, respectively. The results obtained were interpreted in terms of the variation of the internal microstructure in both alloys. The internal microstructural variations in the present study were evaluated by optical microscopy, electron microscopy and X-ray diffraction. The results show the importance of Zn addition in enhancing the mechanical strength of the Sn–3.3 wt.% Ag base alloy.