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分散染料在超临界CO2中的溶解性研究进展 总被引:1,自引:0,他引:1
介绍了目前国内外分散染料在超临界CO2中溶解度的测定装置及其各自的优缺点,同时列出了通过不同的方法测得的分散染料在超临界CO2中的溶解度;分析了计算溶解度的主要模型和影响分散染料在超临界CO2中溶解度的主要因素。 相似文献
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超临界CO2萃取大蒜提取物的研究 总被引:5,自引:2,他引:5
研究了超临界二氧化碳萃取大蒜精油的可行性,其最佳的提取工艺条件为15MPa,40℃;若只需得到蒜素可采用发酵醇提法预处理,这样所得蒜素得率最高,可达44.57%;若要得到大蒜精油还必须进一步利用有机溶剂萃取,每千克大蒜可得大蒜精油1.8克。本文还对制得的大蒜精油进行了红外吸收光谱定性分析。 相似文献
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超临界CO2流体萃取米糠油研究 总被引:1,自引:2,他引:1
通过超临界CO2流体萃取米糠油研究,总结萃取压力、萃取温度、萃取时间和物料水分含量对米糠出油率影响。结果表明,最适宜萃取条件为:萃取压力30 MPa、萃取温度45℃、萃取时间80 min、物料水分含量为5%~6%,出油率达14.32%;同时测定超临界CO2流体萃取米糠油中脂肪酸甘油酯组成,得出油酸甘油酯、亚油酸甘油酯和棕榈酸甘油酯占总脂肪酸甘油酯90%以上,其中,油酸甘油酯和亚油酸甘油酯占总脂肪酸甘油酯70%以上;通过超临界CO2法与压榨法比较,超临界CO2流体法萃取米糠油不饱和脂肪酸含量较高,理化指标也优于压榨法,因萃取温度低,防止提取过程中油脂氧化,因此超临界CO2流体萃取是一种较好提取米糠油方法。 相似文献
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Soon‐Nam Ko Tae‐Yeoul Ha Seung In Hong Sung Won Yoon Junsoo Lee Yangha Kim In‐Hwan Kim 《International Journal of Food Science & Technology》2012,47(4):761-767
An efficient process was developed for enrichment of tocols from rice germ oil (RGO) using supercritical carbon dioxide (SC‐CO2). Tocols were efficiently enriched in residue by removal of fatty acid methyl ester from the esterified RGO using SC‐CO2. The enrichment of tocols was carried out at an operating pressure of 12.4–15.8 MPa, an operating temperature of 40–60 °C and a carbon dioxide flow rate of 5.0 L min?1. The combination of 13.8 MPa pressure and 60 °C temperature was selected as the most suitable for efficient enrichment of tocols. The level of tocols (1270 mg/100 g) in the residue obtained at these operating conditions was six times higher than the tocols level (192 mg/100 g) of the starting material, namely esterified RGO. There were no significant differences in relative percentages of tocols homologues between esterified RGO and the residue obtained by SC‐CO2 extraction. 相似文献
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超临界CO2萃取大蒜提取物的研究 总被引:1,自引:0,他引:1
研究了超临界二氧化碳萃取大蒜精油的可行性,其最佳的提取工艺条件为15MPa,40℃;若只需得到蒜素可采用发酵醇提法预处理,这样所得蒜素得率最高,可达44.57%;若要得到大蒜精油还必须进一步利用有机溶剂萃取,得率为1.8 g/kg. 相似文献
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Kyo-Yeon Lee Khalid Gul Ah-Na Kim M. Shafiur Rahman Myoung Hee Lee Jung In Kim Doyeon Kwak Eui-Cheol Shin Hyun-Jin Kim William L. Kerr Sung-Gil Choi 《International Journal of Food Science & Technology》2020,55(1):183-191
The objective of this study was to determine the efficacy of supercritical carbon dioxide turmeric extract (STE) on the oxidative stability of perilla oil (PO), as measured by acid value (AV), peroxide value (PV) and oxidation induction time and compared to control and α-tocopherol containing PO as a positive control. The antioxidant activity was determined by DPPH, ABTS and FRAPS assays and individual bioactive compounds identified by chromatography. STE demonstrated significantly higher antioxidant activity than the α-tocopherol. The major components of the STE were identified as ar-turmerone, turmerone, curlone and bisabolene by GC-MS and curcumin and demethoxycurcumin by UPLC-Q-TOF MS. During thermal treatment at 65 °C for 24 h, the PO containing STE at different concentrations (100, 300, 500 and 1000 μg mL−1) had significantly lower AV and PV, and at least 1.5 times higher induction period than those of the control and α-tocopherol-incorporated PO. 相似文献
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Buffalo butter oil was fractionated by supercritical carbon dioxide into four fractions (F1-F4). Fractionation was performed at 50 and 70 °C over a pressure range of 10.9-40.1 MPa. Short chain fatty acids (C4-C8), medium chain fatty acids (C10-C14) and saturated fatty acids were decreased from F1 to F4, while long chain fatty acids (C16-C18:3) and unsaturated fatty acids were increased. Triacylglycerol molecular species exhibited a similar trend as fatty acids. Cholesterol was concentrated in F1, and with increasing the fluid density, it decreased by more than 50% in F4. Substantial changes occurred in the chemical composition of the fractions led to distinctive differences in their thermal profile and solid fat content. Fractions obtained in the initial stages of the fractionation exhibited lower melting behavior that obtained in the late stages. 相似文献
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近年来以超临界CO_2流体作为反应介质已成为化学和生物化学反应研究一个热点,以超临界CO_2流体为介质进行酶催化脂质水解反应,与其它非水相酶催化介质相比,有其独特优越性。该文介绍超临界CO_2流体特性及在超临界CO_2流体中影响酶催化脂质水解因素。 相似文献
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Alessandra Aiello Fabiana Pizzolongo Giorgio Scognamiglio Annalisa Romano Paolo Masi Raffaele Romano 《International Journal of Food Science & Technology》2020,55(6):2472-2480
The increase in the popularity of hemp-based products is mainly linked to the presence of non-psychoactive cannabinoids that provide relief from aches, pain and anxiety. In this study, hemp seed oils were produced by two innovative and environmentally friendly extraction techniques: supercritical and liquid carbon dioxide (CO2) extraction. The chemical composition of the two oils was analysed and compared with that of a control oil obtained by solvent (n-hexane) extraction. Both oils obtained by liquid and supercritical CO2 extraction presented interesting compositions: they contained large amounts of cannabinoids, polyphenols and tocopherols and were less oxidised than the control and contained a large amount of hexanal, which provided a pleasant aroma. The maximum cannabinoid content was found in the oil obtained by liquid CO2 extraction (71.51 mg of cannabidiol per kg of oil and 113.92 mg of cannabinol per kg of oil). Carotenoids were prevalent in the oil obtained by supercritical CO2 extraction (61.00 mg kg−1 of oil). 相似文献
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使用超临界二氧化碳技术对经过超声-微波处理过的黄柏中的挥发油进行萃取,并对萃取工艺进行响应面优化。在单因素预实验的基础上,以萃取压力、萃取温度、萃取时间为响应因素,黄柏挥发油的萃取量为响应值,根据中心组合(Box-Behnken)实验设计原理,采用三因素三水平的响应面分析法,确定各工艺条件对萃取量的影响,并用扫描电子显微镜(SEM)对萃取前、未超声-微波处理超临界萃取后及超声-微波处理超临界萃取后的黄柏进行比较观察,对萃取效果进行了微观解释。结果表明,经过超声-微波处理过的黄柏中的挥发油超临界二氧化碳萃取最佳工艺条件为:萃取压力为34MPa,萃取温度为41℃,萃取时间为66min,萃取率达6.03%。 相似文献
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本运用均匀试验设计研究了超临界CO2流体萃取姜黄油的工艺条件,试验结果表明:最佳的萃取工艺条件为萃取压力36MPa,萃取温度50℃,CO2流量15kg/h,萃取时间3h。 相似文献
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Response Surface Methodology was used to determine the effects of solvent flow rate (1, 3 and 5 g/min), pressure (300, 375 and 450 bar) and temperature (40, 50 and 60 °C) on hazelnut oil yield in supercritical carbon dioxide (SC-CO2). Oil yield was represented by a second order response surface equation (R2=0.997) using Box-Bhenken design of experiments. Oil yield increased with increasing SC-CO2 flow rate, pressure and temperature. The maximum oil yield was predicted from the response surface equation as 0.19 g oil/g hazelnut (34% of initial oil) when 4 g hazelnut particles (particle diameter<0.85 mm) were extracted with 5 g/min SC-CO2 flow rate at 450 bar, and 60 °C for 10 min. Total extraction time at these conditions was predicted to be 35 min. 相似文献