轧制工艺对AZ31B镁合金薄板组织与性能的影响

研究了轧制温度和轧制速度对AZ31B镁合金薄板微观组织演变和力学性能的影响。结果表明,轧辊加热有利于镁合金薄板成型;AZ31B镁合金在低温或低速轧制时薄板纵向组织为大量的切变带,切变带区域包含大量孪晶组织,横向组织为含极少量孪晶的等轴晶组织;在轧制温度为400℃和轧制速度为16m/min轧制时,由于动态再结晶,横纵截面组织均为等轴晶。AZ31镁合金薄板的最佳轧制制度为轧辊温度为70℃、轧制温度为400℃、轧制速度为6m/min,此工艺轧制的薄板横向抗拉强度、屈服强度和伸长率分别为350MPa、300MPa和12%,纵向为345MPa、290MPa和11.2%,纵向与横向性能差别明显减小。     

轧制方式对AZ31镁合金薄板组织和性能的影响

研究轧制方式对AZ31镁合金薄板组织和性能的影响.交叉轧制可使材料的延伸率显著提高,σ0.2和σb明显下降,加强了组织的均匀性和等轴性.交叉轧制的AZ31镁合金薄板具有良好的深冲性能.     

温轧AZ31镁合金薄板的快速退火处理

对1 mm厚温轧AZ31镁合金薄板进行快速退火处理,退火温度350～500 ℃,保温时间0.5～60 min,研究了不同快速退火工艺下材料力学性能与微观组织的变化。结果表明：在退火温度为350～500 ℃时,保温时间为0.5～1 min即可使材料的伸长率大幅提高;在退火过程中,材料经亚动态再结晶、静态再结晶和长大3个阶段,其中亚动态再结晶阶段时间较短,约0.5～1 min,此阶段对材料力学性能的变化起主要影响。     

Microstructure and texture evolution of AZ31 magnesium alloy during rolling

The production of magnesium alloy sheets normally involves several processing stages including hot rolling,cold rolling and intermediate annealing.The microstructure and texture evolution of AZ31 magnesium alloy sheets in different processing states were investigated by optical microscopy and X-ray diffraction technique.It is found that the microstructure of hot-rolled sheets is dominated by recrystallized equiaxed grains,while that of cold-rolled sheets is dominated by deformation twins.With final annea...     

等通道角轧制对汽车车身用轻质镁合金板微观组织与力学性能的影响

采用等通道角轧制工艺(ECAR)对AZ31镁合金板进行轧制变形,结合光学显微镜、EBSD、杯突实验机和拉伸实验机等检测方法,研究了不同ECAR工艺对镁合金板微观组织及力学性能的影响。实验结果表明,AZ31镁合金板经ECAR工艺处理后,板材的平均晶粒尺寸出现下降,且板材的基面织构出现了明显地降低,由母材的8.187降低为4.537。此外,镁合金板材的综合性能得到显著提高,板材的杯突值由母材的2.72 mm增加到4.22 mm,n值由母材的0.27增加到0.46,抗拉强度由母材的275 MPa增加到294 MPa。综上所述,等通道角轧制工艺可以有效细化镁合金板材的微观组织,提高镁合金板材的综合力学性能。     

Comparison of microstructure and properties of AZ31 Mg alloy sheet produced through different routes

Slabs fabricated by means of three different ingot breakdown modes:hot-rolling,extrusion-rolling and twin-roll strip continuous casting-cum-rolling,were rolled into sheets and then annealed.Both the rolled and annealed sheets were investigated by SEM-EBSP,BSE,X-ray diffraction and tensile test,and compared in terms of microstructure,texture,and mechanical properties. Effects of different processing methods on the microstructure,texture and the related mechanical properties were discussed based on the exp...     

非对称轧制AZ31镁合金板材组织与性能

采用商用连铸连轧AZ31镁合金板材,通过小辊径非对称轧制工艺,研究在150,200,250℃温度条件下多道次非对称轧制对镁合金板材组织、织构和力学性能的影响。结果表明,不同轧制温度下,镁合金板材的晶粒细化机理不同,150℃时以孪晶细化为主,部分晶粒发生动态再结晶,200和250℃时板材晶粒细化机理为动态再结晶。对比分析了对称轧制和非对称轧制板材织构演化规律,随着轧制温度的升高,非对称轧制板材基面织构依次增强,但明显低于对称轧制板材。     

退火工艺对AZ31B温轧薄板组织和性能的影响

分析不同的退火时间对AZ31B镁合金温轧薄板的组织和性能的影响。通过试验和分析发现:镁合金温轧薄板在退火温度为573 K、退火时间为60 min时,能够获得较好的综合力学性能;进一步延长退火时间到120 min,塑性进一步改善,r值基本保持不变,n值增加。     

AZ31镁合金高应变速率轧制边裂及力学性能各向异性

在300~400 ℃对铸态AZ31镁合金进行平均应变速率为10~29 s^-1的高应变速率轧制,研究轧制后镁板边裂、组织及力学性能的各向异性。结果表明:随着平均应变速率的增加,轧制边裂得到改善,350 ℃和400 ℃下边裂长度变化相比300 ℃时更加平缓;晶粒尺寸在温升和应变速率综合作用下并不随平均应变速率的增加而减小,反而出现波动;在相对较低的应变速率下,由于组织中长条形晶粒的存在,导致板材的各向异性明显;随着平均应变速率的增加,长条形晶粒减少,再结晶完全,组织趋于均匀,轧板的各向异性得到改善;轧板拉伸断口中可观察到撕裂棱和韧窝,以韧性断裂方式为主。     

多道次温轧对AZ31镁合金组织和性能的影响

以AZ31镁合金为实验材料,通过多道次温轧工艺,研究低温时效处理对温轧板材组织和性能的影响。结果表明:经5道次温轧后合金组织得到明显细化,从初始态38μm细化至2.2μm;在随后120～160℃时效过程中,晶粒并未发生显著长大。经低温时效处理后,合金在基本保持温轧态拉伸强度的同时,其塑性得到明显提升。由晶界强化和位错强化模型定量描述发现,经5道次温轧后合金显微硬度增量为30HV。然而随着时效温度的升高,位错强化贡献显著降低,而晶界强化由于晶粒长大不明显而几乎无显著变化。合金经160℃时效2 h后,两种主要强化机制对显微硬度的贡献为16HV。     

脉冲电流轧制对AZ31镁合金微观组织与力学性能的影响

对比研究脉冲电流轧制工艺与温轧工艺对AZ31镁合金板材的力学性能、织构、微观组织与沉淀相等方面的影响。结果表明：脉冲电流具有促进冷轧AZ31镁合金低温再结晶能力的作用。脉冲电流轧制后的镁合金板材组织由细小的等轴再结晶粒与析出相构成,没有发现孪晶组织,并且完全再结晶,原始晶粒均被细小的再结晶晶粒取代,再结晶晶粒内的位错密度低。而温轧镁合金组织则由稍拉长变形孪晶、粗大的再结晶晶粒和析出相构成,再结晶的晶粒内位错密度高。两种轧制方式下的镁合金析出相均为Mg17Al12。脉冲电流轧制后镁合金的织构具有典型基面织构的特征,而脉冲电流轧制镁合金的织构则出现横向偏转;脉冲电流轧制后镁合金的屈服强度与伸长率均比温轧镁合金的大,但抗拉强度正好相反。     

异步轧制AZ31镁合金板材室温冲压性能研究

文章主要对异步轧制AZ31镁合金板材室温冲压性能进行了研究,以探讨提高镁合金板材冲压性能的途径。结果表明,异步轧制有利于板材的晶粒细化,其晶粒尺寸约为7.6μm,明显小于普通轧制板材的12.5μm;而由于异步轧制过程中剪切变形的作用,异步轧制使板材的(0002)基面晶粒取向减弱;与普通轧制相比,异步轧制板材的应变硬化能力增加,屈服强度降低,制耳参数减小,但塑性应变比也降低,这可归因于异步轧制所导致的晶粒细化和晶粒取向的改变。     

Influence of rolling route on microstructure and mechanical properties of AZ31 magnesium alloy during asymmetric reduction rolling

Four different routes of asymmetric reduction rolling were conducted on AZ31 magnesium alloy to investigate their effect on the microstructure evolution and mechanical properties. Route A is the forward rolling; while during routes B and C the sheets are rotated 180° in rolling direction and normal direction, respectively; route D is the unidirectional rolling. The strain states of rolled sheets were analyzed by the finite element method, while the microstructure and texture were observed using optical microscopy, X-ray diffraction and electron back-scattered diffraction techniques, and the mechanical properties were measured by tensile test. The results show that route D produced the largest effective strain. Compared with other samples, sample D exhibited a homogeneous microstructure with fine grains as well as a weak and tilted texture, in corresponding, it performed excellent tensile properties, which suggested that route D was an effective way to enhance the strength and plasticity of AZ31 sheet.     

Annealing behavior of rolled AZ31 alloy sheet

The annealed microstructures of the rolled AZ31 alloy sheets were examined by using light optical microscopy. The mechanical properties were measured by tensile testing, with their crystal orientations analyzed by X-ray diffraction （XRD）. After the annealing treatment, the elongated grains were transformed to equiaxed grains with uniform and homogeneous structures. The changes of microstructure decreased the yield strength and enhanced the elongation. The analysis of XRD shows that the AZ31 alloy sheet possesses intense basal-texture, which is weakened during the recrystallization while reinforced during the grain growth. The intense basal-texture induces low ductility, which hence makes the further rolling more difficult. The results indicate that the optimum annealing treatment during AZ31 alloys sheet rolling is at about 300 ℃ for 60-120 min.     

AZ31镁合金铸轧和常规轧制板的变形组织及形变特征

在变形温度为150～400 ℃、应变速率为0.3～0.000 3 s~(-1)条件下,在Gleeble1500热模拟机上采用等温拉伸试验对AZ31镁合金铸轧和常规轧制板的高温塑性及组织演变进行研究.结果表明:两种AZ31镁合金板的峰值应力和峰值应变均随着变形温度的降低和应变速率的增加而逐渐增大.铸轧板的应变硬化指数和应变速率敏感系数均大于常规轧制板的.在高温低应变速率变形条件下,铸轧板的晶界滑移引起的空洞尺寸、体积分数和密度均大于常规轧制板的.低应变速率下拉伸变形后的动态再结晶晶粒尺寸随温度的升高逐渐增加;不同变形条件下铸轧板的晶粒尺寸均小于常规轧制板的;再结晶晶粒尺寸和Z参数呈幂律关系.     

AZ31镁合金大压下率轧制的研究

对AZ31镁合金的大压下率轧制进行了研究,分析进行大压下率轧制的途径,并对轧制后材料的微观组织和力学性能进行分析.研究发现只要选用合适的工艺条件,AZ31镁合金可以进行大压下率轧制.在300℃和400℃温度下大压下率轧制得到的AZ31镁合金,都具有细小均匀的微观组织和良好的力学性能.     

AZ31B镁合金轧制板材室温动态拉伸的SEM观察

利用动态拉伸台和扫描电镜(SEM)对AZ31B镁合金轧制板材进行了动态拉伸的微观形貌观察。试验证明,材料宏观织构和显微组织都会对镁合金轧制板材的室温拉伸性能产生影响;在轧制镁合金拉伸变形时滑移和孪生同时存在;裂纹的产生和扩展具有明显的方向性。轧制组织中大量的变形孪晶与应力方向的位向关系,是轧向和横向上裂纹产生及扩展机制产生较大差异的主要原因。     

AZ31镁合金挤压薄板织构及力学各向异性

研究AZ31镁合金挤压薄板的显微组织、织构及室温下板面内各不同方向的力学性能。织构分析表明,挤压薄板主要有{0002}<1-010>和{10-10}<11-20>2种织构组分。拉伸测试结果显示,沿挤压方向屈服强度最高,达到200.4MPa,这是由于这种取向基面滑移和{1-012}锥面孪生均不能开动,发生织构强化的结果;与挤压方向呈45°方向伸长率最高达19.0%,这是由于具有{10-10}<11-20>织构组分晶粒的基面滑移开动;与挤压方向呈90°方向屈服强度最低仅为挤压方向相应值的一半左右,这是由于具有{10-10}<11-20>织构组分晶粒发生了{10-12}锥面孪生。     

等径角轧制AZ31镁合金板材的组织与性能

采用等径角轧制工艺制备了AZ31镁合金板材.结果表明:经等径角轧制后的板材,晶粒取向由等径角轧制前的(0002)基面取向演化为基面与非基面共存的取向.与等径角轧制前的板材相比,板材晶粒尺寸略有长大并有孪晶出现,但强度却明显提高,而断裂延伸率变化不大,尤其是1个道次轧制的板材其抗拉强度由等径角轧制前的240增大到275 MPa,屈服强度由193.8增大到239.2 MPa;随着等径角轧制道次的增加,板材的强度逐渐降低,至第4个道次其抗拉强度仅为250 MPa,屈服强度为207.3 MPa.