Zwillingsbildung bei der thermischen Ermüdung der Mg‐Basislegierung AZ31

Twinning at thermal fatigue of magnesium alloy AZ31 In this paper results of thermal fatigue tests of the magnesium base alloy AZ31 carried out in a temperature range between ‐50 °C and +290 °C are presented. Specimens were loaded under constant total strain and uniaxial homogeneous stresses. The resulting materials behaviour is described by stress amplitudes, plastic strain amplitudes and mean stresses as a function of the number of thermal loading cycles. It is well known that AZ31 shows different stress‐strain behaviour during tensile and compressive loading resp. at lower temperatures due to the fact that mechanical twinning depends on the loading direction. However untwinning processes may occur during unloading and reloading in the opposite direction. As a consequence, during the first thermal loading cycles, typical consequences of the formation and the dissolution of twins are observed. The interaction of deformation, recovery and recrystallization processes, characteristic for individual temperature ranges are discussed in detail to analyze the damage progress during thermal fatigue.     

Einfluss von Randschichtzustand und Haltezeit auf die thermische Ermüdung der Magnesiumbasislegierung AZ31

In this paper thermal fatigue of magnesium base alloy AZ31 in the temperature range between +50°C and +290°C is investigated. Experiments were carried out under constant total deformation (out‐of‐phase loading) and the resulting stress amplitudes as well as the plastic strain amplitudes were recorded as a function of the number of thermal loading cycles. In particular the consequences of mechanical surface treatments (deep rolling) and of hold‐times were investigated. In both cases no particular influence compared with untreated specimens loaded without hold‐times was observed, which is due to the interaction of deformation and recrystallization processes during thermal fatigue.     

AZ91D室温环境棘轮及其低周疲劳行为

通过AZ91D室温环境应力控制下的低周疲劳试验,对铸造镁合金棘轮及其低周疲劳行为进行了研究,讨论了室温环境下材料的应力循环特性、棘轮行为、塑性应变范围、全应变范围等疲劳参量随载荷水平和加载历史的变化规律,同时基于平均应力修正对材料的应力-寿命曲线进行了讨论。研究结果表明:AZ91D在室温环境下的应力循环呈循环硬化,材料的棘轮行为和塑性应变范围、全应变范围等疲劳参量依赖于载荷水平和加载历史,另外考虑平均应力修正后的应力-寿命曲线预测效果有明显改观。     

Ermüdungslebensdauer der Magnesiumlegierung AZ91: Experiment und Modellierung

Fatigue Life of the Die‐Cast Magnesium Alloy AZ91: Experiments and Modelling The cyclic deformation behaviour of the die‐cast magnesium alloy AZ91HP was investigated under total strain control at constant total strain amplitudes between 1.4 × 10⁻³ to 2 × 10⁻² at room temperature and at 130°C. Microstructural investigations in combination with the determination of crack‐growth behaviour using the replica technique and measurements of changes of the stiffness (compliance) of the specimen during a fatigue experiment led to a detailed understanding of the evolution of damage and the main damage mechanisms. Based on these findings, a microstructurally based life‐prediction concept was formulated.     

Cyclic deformation behaviour and fatigue crack propagation in AZ91HP and AM50HP

Abstract

The purpose of the present work was to investigate room temperature cyclic deformation and crack propagation behaviour in the most widely used die casting magnesium alloy AZ91HP with different heat treatments. In addition, examination of the low cycle fatigue properties of solid solution treated alloy AZ91HP-T4 was emphasised in comparison with AM50HP. Obvious cyclic strain hardening was found in low cycle fatigue tests, especially for AZ91HP-T4 at high cyclic strain amplitudes. Nevertheless, it was very difficult to evaluate differences in low cycle fatigue behaviour between die casting alloy AZ91HP-F, artificially aged alloy AZ91HP-T6, solution treated alloy AZ91HP-T4, and AM50HP(-F) because of the scatter of test data. However, it may be concluded that the last two alloys had greater plastic strain components during cyclic deformation, and AZ91HP-T4 exhibited a longer fatigue life than that of AM50HP at the highest strain amplitude. According to results of tests carried out on AZ91HP compact tension (CT) specimens, it was concluded that solution treatment could reduce the fatigue crack propagation rate, and plasticity induced crack closure was considered to have a predominant effect on fatigue crack propagation.     

Fatigue lifetime of AZ91 magnesium alloy subjected to cyclic thermal and mechanical loadings

In the present paper, thermo-mechanical fatigue (TMF) and low cycle fatigue (LCF) or isothermal fatigue (IF) lifetimes of a cast magnesium alloy (the AZ91 alloy) were studied. In addition to a heat treatment process (T6), several rare elements were added to the alloy to improve the material strength in the first step. Then, the cyclic behavior of the AZ91 was investigated. For this objective, strain-controlled tension–compression fatigue tests were carried out. The temperature varied between 50 and 200 °C in the out-of-phase (OP) TMF tests. The constraint factor which was defined as the ratio of the mechanical strain to the thermal strain, was set to 75%, 100% and 125%. For LCF tests, mechanical strain amplitudes of 0.20%, 0.25% and 0.30% were considered at constant temperatures of 25 and 200 °C. Experimental fatigue results showed that the cyclic hardening behavior occurred at the room temperature in the AZ91 alloy. At higher temperatures, this alloy had a brittle fracture. But also, it was not significantly clear that the cyclic hardening or the cyclic softening behavior would be occurred in the material. Then, the high temperature LCF lifetime was more than that at the room temperature. The OP-TMF lifetime was the least value in comparison to that of LCF tests. At the end of this article, two energy-based models were applied to predict the fatigue lifetime of this magnesium alloy.     

Thermisch‐mechanisches Ermüdungsverhalten der partikelverstärkten Aluminiumknetlegierung EN AW‐6061‐T6 und die Entwicklung von Eigenspannungen im Matrixwerkstoff unter thermisch‐mechanischer Beanspruchung

Thermal mechanical fatigue behaviour of particle reinforced EN AW‐6061‐T6 and development of residual stresses in the matrix material by thermal mechanical loading The behaviour of non reinforced and 15 Vol.‐% α‐alumina particle reinforced wrought aluminium alloy EN AW‐6061‐T6 in thermal mechanical fatigue loading was investigated at different maximum temperatures. The tests were performed in strain controlled mode by means of an electro‐mechanical testing machine. Alternating load deformation and life cycle behaviour either materials were compared. It came out, that the reinforcement leads to an decreasing thermal mechanical fatigue life cycle while keeping constant the maximum temperature and mechanical loading. The two materials showed softening behaviour due to high maximum temperatures of 573 K to 673 K. However, there is an intense scatter of the number of cycles to failure of the non reinforced alloy aggravating the interpretation of the results. On the other hand the thermal mechanical life cycle increases in combination with increasing maximum temperatures. Simultaneously the part of plastic deformation in mechanical loading increases for both materials, while for a constant total strain range the effective maximum and minimum stresses are decreasing. Furthermore, the development of residual stresses in the matrix of the reinforced alloy by thermal mechanical fatigue loading was analysed. It was observed that only small absolute values of residual stresses will be obtained for these loads. Nevertheless, tendencies of mounting tensile residual stresses can be identified in the direction of thermal mechanical fatigue loading and subsequently reduction of the residual stresses.     

AZ91镁合金抗高温蠕变性能的研究和发展

综述了国内外AZ91镁合金抗高温蠕变性能的研究进展,重点讨论了其蠕变机理及提高其抗高温蠕变性能的方法,对AZgl镁合金抗高温蠕变性能的研究方向提出了一些看法和展望.     

Structural durability of magnesium alloys and components

The fatigue behaviour of the magnesium die cast alloys AZ91, AE42 and AM50 was investigated at constant amplitude and in variable amplitude tests. The ambient conditions of these tests varied between laboratory air at room temperature, at 125 °C and a permanent influence of NaCl‐solution at room temperature. More than 40 test series were analysed in a generalized way to determine standardized slopes of S‐N curves and mean stress sensitivity. The behaviour of the three alloys was investigated also in strain‐controlled cyclic tests at normal and elevated temperature. Based on this substantial data set several variants of methods following both the nominal‐stress concept and the local‐strain approach were applied to determine guidelines to improve the reliability of lifetime estimation of components made of magnesium. The corrosion fatigue behaviour of these magnesium alloys was extensively investigated under rotating bending to clarify the damaging influence of the corrosive load component. Under simultaneous action of corrosion and cyclic mechanical loading several influencing factors have to be considered which attain special importance during the testing of magnesium alloys.     

The modified temperature term on Johnson Cook model for AZ31 magnesium alloy

The quasi‐state and dynamic mechanism of AZ31 magnesium alloy at a strain rates range of 0.001 s^‐1–2500 s^‐1 under a temperature range of 20 °C–250 °C were researched by compression tests using the electronic universal testing machine and split Hopkinson pressure bar system. The true stress‐strain curves at different strain rates and evaluated temperatures were obtained. The result shows that the thermal soften effect of AZ31 magnesium alloy is significant. By modifying the temperature term of the original Johnson Cook model of AZ31 magnesium alloy, a modified Johnson Cook model of AZ31 magnesium alloy has been proposed to reveal thermal soften effect on the deformation behavior of AZ31 magnesium alloy more precisely. With the modified Johnson Cook model and fracture model, the finite element method simulation of AZ31 magnesium alloy hat shaped specimen under impacting was conducted. The numerical simulation result is consistent with the experimental result, which indicates that the modified Johnson Cook model and fracture model are greatly valid to predict the deformation and fracture behavior of the AZ31 magnesium alloy hat shaped specimen under impacting.     

Evaluation of a phenomenological elastic‐plastic approach for magnesium alloys under multiaxial loading conditions

Magnesium alloys are greatly appreciated due to their high strength to weight ratio, stiffness, and low density; however, they can exhibit complex types of cyclic plasticity like twinning, de‐twinning, or Bauschinger effect. Recent studies indicate that these types of cyclic plastic deformations cannot be fully characterized using the typical tools used in cyclic characterization of steels and aluminium alloys; thus, it is required new approaches to fully capture their cyclic deformation and plasticity. This study aims to propose and evaluate a phenomenological cyclic elastic‐plastic approach designed to capture the cyclic deformation of magnesium alloys under multiaxial loading conditions. Series of experimental tests were performed to characterize the cyclic mechanical behaviour of the magnesium alloy AZ31BF considering proportional loadings with different strain amplitude ratios and a nonproportional loading with a 45° phase shift. The experimental results were modulated using polynomial functions in order to implement a cyclic plasticity model for the AZ311BF based on the phenomenological approach proposed. Results show good correlations between experiments and estimates.     

挤压对AZ91铸造镁合金力学性能的影响

对挤压变形前后的AZ91镁合金进行了微观组织和力学性能研究.结果表明:挤压成形后合金的抗拉强度和塑性均得到提高;孪晶的产生,导致挤压合金室温压缩的应力-应变曲线上有屈服平台出现;晶粒尺寸强烈影响合金的强度.室温时,挤压合金的流变强度较铸态的高,而高温压缩的强度则较铸态的低.     

Characterization of the fatigue behaviour of the magnesium alloy AZ91D by means of mechanical hysteresis and temperature measurements

Stress-controlled load increase and constant amplitude tests were performed on the cast magnesium alloy AZ91D. Rather small values of the plastic strain amplitude reflect the very localised plastic deformation predominant in the _I-phase. The cyclic deformation and temperature curves of the load increase tests exhibit cyclic yield strength values which allow a good estimation of the endurance limit. Stress amplitudes above the endurance limit lead to cyclic hardening. As compared to the behaviour under monotonic tensile loading, the alloy exhibits cyclic hardening. Microscopic investigations illustrate the different influences of the - and β-phase in respect to crack initiation.     

Untersuchung des Sputter‐Ätzens auf die Eigenschaften von PVD‐CrN Hartstoffschichten auf Magnesium AZ91hp

Investigating the Influence of the Sputter Etching Process on the Properties of PVD‐CrN Coatings on Magnesium Die Cast Alloy AZ91hp A common method prior to the PVD deposition is the sputter etching process of the substrate itself to clean the surface from adhesion products and to improve the coating adhesion. This report deals with the sputter etching of magnesium die cast alloy AZ91hp to investigate the influences on the coating‐substrate interface, the surface properties and the mechanical properties of PVD‐CrN hard coatings. The coating‐substrate interface of the Cr‐AZ91 coating systems was investigated with XPS and SIMS. Surface studies were carried out by high resolution electron microscopy and AFM. The characterization of the mechanical properties of the CrN‐AZ91 compound systems includes thickness, coating hardness and hardness depth profiles, coating adhesion, structure and residual stresses. Some properties show a strong dependency of the etching time, especially the mechanical properties and the coating roughness. Increasing etching times lead to an improvement of the coating quality.     

Betriebsfestigkeit von Magnesium‐Gussbauteilen unter schlagartigen und zyklischen Beanspruchungen ohne und mit plastischen Vorverformungen infolge von Sonderbelastungen

Structural Durability of Cast Magnesium Components under Impact and Cyclic Loading without and with Plastic Pre‐Deformations due to Special Events Specimens and engine brackets manufactured by the high pressure die cast magnesium alloy MRI‐4 showed superior fatigue properties under constant amplitude loading compared to AZ‐91. No significant differences were observed by impact tests with components. However MRI‐4 components presented a lower fatigue life under variable amplitude loading and a real damage sum, which was significantly lower than 1. A plastic pre‐deformation of the MRI‐4 components increased their fatigue strength, while the components of AZ‐91 revealed a neutral behaviour.     

Compressive Deformation of Semi-Solid AZ91D Magnesium Alloy

The compression tests of semi-solid AZ91D Mg alloy have been conducted on a parallel-plate viscometer. The results are as follows. With increasing the compression temperature, the deformation rate or the strain rate of the specimens rises, but the compressive stress continuously decreases; the deformation strain is obviously linear with the compressive stress and independent on compression temperature under a given compression load. In the wake of the compression load being added, the compressive strain increases but the compressive stress decreases clearly; the deformation strain is obviously linear with the compressive stress under different compression load. The mathematical apparent viscosity model about the semi-solid compressed AZ91D Mg alloy has been established, i.e. ηapp=2004.2exp(15.61fs)γ1.317fs-1.3511.     

异步轧制AZ31镁合金板材的超塑性工艺及变形机制

经过异步轧制工艺获得AZ31镁合金薄板。在300~450℃范围内,分别通过5×10-3,1×10-3s-1和5×10-4s-1不同应变速率进行高温拉伸实验研究其超塑性变形行为,计算应变速率敏感指数m值、超塑性变形激活能Q及门槛应力σ0值。通过EBSD分析和扫描电镜观察拉伸断裂后的断口形貌,分析AZ31镁合金的超塑性变形机制。结果表明:AZ31镁合金的塑性变形能力随着变形温度的升高及应变速率的降低而增强。当拉伸温度为400℃、m=0.72、应变速率为5×10-4s-1时,AZ31具有良好的超塑性,伸长率最大为206%。温度为400℃时,异步轧制AZ31镁合金的超塑性变形是以晶格扩散控制的晶界滑移和基面滑移共同完成的。     

Cyclic hysteresis of AZ31B extrusion under load‐control tests using embedded sensor technology

The fatigue behaviour of AZ31B extrusion magnesium alloy under load‐control cyclic test conditions is estimated using a combination of simulation and experimental results. The strain measurement of this asymmetric material is found experimentally using a Fibre Bragg Grating (FBG) sensor during rotating bending tests. Then, to analyse applied stresses in the sample – particularly in the plastic deformation range – the Variable Material Property (VMP) method is employed. Using this simulation method, the hysteresis loops of two critical top and bottom elements of the sample's cross section under different bending moments are obtained. Finally, the strain of the sample during rotating bending, as measured by the embedded FBG sensor, is related to the stresses obtained from the modeling using a mapping function. The hystereses obtained from this combination of the modeling and experimental results are compared with the results of a companion strain‐control pull–push test in which the input strain history was that of measured by the FBG sensor. Observations verify that the stresses of the combined VMP‐FBG hysteresis loops have good compatibility with the stress responses obtained through the experiment. The hybrid model introduced in this work can be employed to capture cyclic hysteresis, and hence estimate the fatigue life, under load‐controlled rotating bending tests.     

An experimental study of creep‐ratchetting behavior of rolled AZ31B magnesium alloy at room temperature

To study the interaction effect of creep and ratchetting for rolled AZ31B magnesium alloy at room temperature, a series of stress‐controlled tests were designed. In the tests, four loading types with different mean stresses were considered, and dwell loading was applied to explore the creep effect on the ratchetting. The test results indicated that the sequence of ratchetting and creep loading is crucial for the strain evolution. The amount of twinning/detwinning increased as the mean stress decreased, leading to an exhaustion of nonbasal slip during ratchetting, and then suppressed the creep ductility. However, the creep sequence exerted little influence on the strain shift of ratchetting while large amount of twinning/detwinning was involved.     

Damping behaviour of AZ91 magnesium alloy with cracks

The amplitude-dependent damping of a commercial magnesium cast alloy AZ91 was determined at room temperature by measurement of the logarithmic decrement of free decaying vibrations of bending beams clamped at one side. In order to generate cracks in the specimens they were subjected to (1) isochronal heat treatments for 1 h at temperatures above 400 °C with succeeding quenching in cold water and (2) controlled fatigue bending loading in the same equipment also used for the damping measurements. After both treatments, the amplitude-dependent damping curves show a maximum for strains 10⁻⁵ to 10⁻³, which can be correlated with the presence of cracks and can be explained by a simple rheological model based on crack damping. This maximum is enhanced when the number of loading cycles or the quenching temperature is increased which can be explained by crack nucleation. Crack growth with increasing number of loading cycles shifts the maximum to lower strains.