Mode I and mixed mode fracture of polysilicon for MEMS

An experimental study was carried out to investigate the local and effective fracture behaviour of polycrystalline silicon for microelectromechanical systems (MEMS). The apparent mode I critical stress intensity factor was determined from MEMS‐scale tension specimens containing atomically sharp edge pre‐cracks, while local deformation fields were recorded near the crack tip, with high resolution by the in situ Atomic Force Microscopy (AFM)/Digital Image Correlation (DIC) method previously developed by this group. The effective mode I critical stress intensity factor varied in the range 0.843–1.225 MPa√m. This distribution of values was attributed to local (in grain) cleavage anisotropy and to enhanced grain boundary toughening. The same sources resulted in very different local and macroscopic (apparent) stress intensity factors, which, combined with the small grain size of polysilicon (0.3 μm,) were the reason for subcritical crack growth that was evidenced experimentally by AFM topographic and AFM/DIC displacement measurements. The effect of local in‐grain anisotropy and granular inhomogeneity was stronger under mixed mode loading of edge cracks inclined at angles up to 55° with respect to the applied far‐field load. The K_I–K_II locus was characterized by scatter in the K_Ic values but on average it followed the curves calculated by the maximum tensile stress and the maximum energy release rate criteria calculated assuming isotropy.     

Mechanisms for corrosion fatigue crack propagation

ABSTRACT The corrosion fatigue crack growth (FCG) behaviour, the effect of applied potential on corrosion FCG rates, and the fracture surfaces were studied for high‐strength low‐alloy steels, titanium alloys, and magnesium alloys. During investigation of the effect of applied potential on corrosion FCG rates, polarization was switched on for a time period in which it was possible to register the change in the crack growth rate corresponding to the open‐circuit potential and to measure the crack growth rate under polarization. Due to the higher resolution of the crack extension measurement technique, the time rarely exceeded 300 s. This approach made possible the observation of a non‐single mode effect of cathodic polarization on corrosion FCG rates. Cathodic polarization accelerated crack growth when the maximum stress intensity (K_max) exceeded a certain well‐defined critical value characteristic for a given material‐solution combination. When K_max was lower than the critical value, the same cathodic polarization, with all other conditions (specimen, solution, pH, loading frequency, stress ratio, temperature, etc.) being equal, retarded or had no influence on crack growth. The results and fractographic observations suggested that the acceleration in crack growth under cathodic polarization was due to hydrogen‐induced cracking (HIC). Therefore, critical values of K_max, as well as the stress intensity range (ΔK) were regarded as corresponding to the onset of corrosion FCG according to the HIC mechanism and designated as K_HIC and ΔK_HIC. HIC was the main mechanism of corrosion FCG at K_max > K_HIC (ΔK > ΔK_HIC). For most of the material‐solution combinations investigated, stress‐assisted dissolution played a dominant role in the corrosion fatigue crack propagation at K_max < K_HIC (ΔK < ΔK_HIC).     

Threshold and growth mechanism of fatigue cracks under mode II and III loadings

ABSTRACT The fatigue crack growth behaviour of 0.47% carbon steel was studied under mode II and III loadings. Mode II fatigue crack growth tests were carried out using specially designed double cantilever (DC) type specimens in order to measure the mode II threshold stress intensity factor range, ΔK_IIth. The relationship ΔK_IIth > ΔK_Ith caused crack branching from mode II to I after a crack reached the mode II threshold. Torsion fatigue tests on circumferentially cracked specimens were carried out to study the mechanisms of both mode III crack growth and of the formation of the factory‐roof crack surface morphology. A change in microstructure occurred at a crack tip during crack growth in both mode II and mode III shear cracks. It is presumed that the crack growth mechanisms in mode II and in mode III are essentially the same. Detailed fractographic investigation showed that factory‐roofs were formed by crack branching into mode I. Crack branching started from small semi‐elliptical cracks nucleated by shear at the tip of the original circumferential crack.     

Cyclic corrosion crack-growth resistance of 26KhN3M2FA steel

We present results of an investigation of the cyclic corrosion crack-growth resistance of 26KhN3M2FA steel under conditions of the water-vapor phase transition and plot invariant dependences (pH _t = const) of the corrosion-fatigue crack-growth rate on the stress intensity factors for various stress ratios and temperatures of the medium under extreme electrochemical conditions at the tip of a corrosion-fatigue crack and taking the influence of an inhibitor (NaH₂PO₄ · 12H₂O) into account. We also study the behavior of electrochemical characteristics on the specimen surface and at the tip of a propagating corrosion-fatigue crack, quantitatively determine the intensity of local anode dissolution and hydrogen embrittlement in the course of crack propagation, and compare cyclic corrosion cracking resistances of 26KhN3M2FA and 34KhN1M steels.Translated from Fiziko-Khimicheskaya Mekhanika Materialov, Vol. 30, No. 5, pp. 19–27, September – October, 1994.     

Interface crack in periodically layered bimaterial composite

A directional crack growth prediction in a compressed homogenous elastic isotropic material under plane strain conditions is considered. The conditions at the parent crack tip are evaluated for a straight stationary crack. Remote load is a combined biaxial compressive normal stress and pure shear. Crack surfaces are assumed to be frictionless and to remain closed during the kink formation wherefore the mode I stress intensity factor K _I is vanishing. Hence the mode II stress intensity factor K _II remains as the single stress intensity variable for the kinked crack. An expression for the local mode II stress intensity factor k ₂ at the tip of a straight kink has been calculated numerically with an integral equation using the solution scheme proposed by Lo (1978) and refined by He and Hutchinson (1989). The confidence of the solution is strengthened by verifications with a boundary element method and by particular analytical solutions. The expression has been found as a function of the mode II stress intensity factor K _II of the parent crack, the direction and length of the kink, and the difference between the remote compressive normal stresses perpendicular to, and parallel with, the plane of the parent crack. Based on the expression, initial crack growth directions have been suggested. At a sufficiently high non-isotropic compressive normal stress, so that the crack remains closed, the crack is predicted to extend along a curved path that maximizes the mode II stress intensity factor k ₂. Only at an isotropic remote compressive normal stress the crack will continue straight ahead without change of the direction. Further, an analysis of the shape of the crack path has revealed that the propagation path is, according the model, required to be described by a function y=cx , where the exponent is equal to 3/2. In that case, when =3/2, predicts the analytical model a propagation path that is self-similar (i.e. the curvature c is independent of any length of a crack extension), and which can be described by a function of only the mode II stress intensity factor K _II at the parent crack tip and the difference between the remote compressive normal stress perpendicular to, and parallel with, the parent crack plane. Comparisons with curved shear cracks in brittle materials reported in literature provide limited support for the model discussed.     

Micro-mechanical analysis and TEM study of crack initiation in dislocation free zone

Dislocation emission, dislocation-free zone (DFZ) formation and crack initiation in the DFZ and/or at the crack tip were analyzed by micromechanics. The results show that a DFZ is formed after dislocation emission under constant load. The DFZ size decreases with increase in the applied stress intensity factor K _Ia or lattice friction stress _f. There are two stress peaks ahead of the crack tip. The first one is located at the blunt crack tip and the second one in the DFZ. With increasing in the applied stress intensity factor K _Ia, the peak stress at the crack tip may decrease while the peak stress in the DFZ increases monotonically. Microcrack will initiate when the peak stress is equal to the cohesive strength. In situ tensile tests in a transmission electron microscope (TEM) show that microcrack initiates in DFZ or/and at a blunt crack tip after dislocation emitting and DFZ formation.     

Prediction of fatigue crack growth under constant amplitude loading and a single overload based on elasto-plastic crack tip stresses and strains

It is generally accepted that the fatigue crack growth (FCG) depends mainly on the stress intensity factor range (ΔK) and the maximum stress intensity factor (K_max). The two parameters are usually combined into one expression called often as the driving force and many various driving forces have been proposed up to date. The driving force can be successful as long as the stress intensity factors are appropriately correlated with the actual elasto-plastic crack tip stress-strain field. However, the correlation between the stress intensity factors and the crack tip stress-strain field is often influenced by residual stresses induced in due course.A two-parameter (ΔK_tot, K_max,tot) driving force based on the elasto-plastic crack tip stress-strain history has been proposed. The applied stress intensity factors (ΔK_appl, K_max,appl) were modified to the total stress intensity factors (ΔK_tot, K_max,tot) in order to account for the effect of the local crack tip stresses and strains on fatigue crack growth. The FCG was predicted by simulating the stress-strain response in the material volume adjacent to the crack tip and estimating the accumulated fatigue damage. The fatigue crack growth was regarded as a process of successive crack re-initiations in the crack tip region. The model was developed to predict the effect of the mean and residual stresses induced by the cyclic loading. The effect of variable amplitude loadings on FCG can be also quantified on the basis of the proposed model. A two-parameter driving force in the form of: was derived based on the local stresses and strains at the crack tip and the Smith-Watson-Topper (SWT) fatigue damage parameter: D = σ_maxΔε/2. The effect of the internal (residual) stress induced by the reversed cyclic plasticity manifested itself in the change of the resultant (total) stress intensity factors controlling the fatigue crack growth.The model was verified using experimental fatigue crack growth data for aluminum alloy 7075-T6 obtained under constant amplitude loading and a single overload.     

Fatigue crack growth testing at negative stress ratios: discussion on the comparability of testing results

It is an accepted fact in fatigue community that compressive loads contribute to fatigue crack growth. Evidences range from fatigue crack growth under fully compressive loads to effects of compressive underloads to negative stress ratio loading. Because the crack closes under compression and the crack flanks transmit compressive stresses, the loading situation is completely different to those of tensile loading. The present paper addresses the comparability of crack growth testing procedures at negative stress ratios. It reveals that compressive loading at the crack tip differs in different specimens for an equal maximum stress intensity factor K_max and negative stress ratio R. Furthermore, the crack length can significantly influence the loading conditions at the crack tip for tension–compression loading. Depending on the specimen type and crack length, a negative force ratio may lead to a change of algebraic sign of the stresses at the crack tip or not. As a consequence, the comparability of available literature results for R ≤ 0 tests is not ensured. Proposals to improve the comparability of tension–compression crack growth testing will be given.     

Shear mode threshold for a small fatigue crack in a bearing steel

The fatigue behaviour of small, semi‐elliptical surface cracks in a bearing steel was investigated under cyclic shear‐mode loading in ambient air. Fully reversed torsion was combined with a static axial compressive stress to obtain a stable shear‐mode crack growth in the longitudinal direction of cylindrical specimens. Non‐propagating cracks less than 1 mm in size were obtained (i) by decreasing the stress amplitude in tests using notched specimens and (ii) by using smooth specimens in constant stress amplitude tests. The threshold stress intensity factor ranges, ΔK_IIth and ΔK_IIIth, were estimated from the shape and dimensions of non‐propagating cracks. Wear on the crack faces was inferred by debris and also by changes in microstructure in the wake of crack tip. These effects resulted in a significant increase in the threshold value. The threshold value decreased with a decrease in crack size. No significant difference was observed between the values of ΔK_IIth and ΔK_IIIth.     

Crack growth behavior and fatigue-life prediction based on worst-case near-threshold data of a large crack for 9310 steel

ABSTRACT Both experimental and analytical investigations were conducted to study crack initiation and growth of small cracks, near‐threshold growth behavior of large cracks at constant R‐ratio/decreasing ΔK and constant K_max/decreasing ΔK, respectively, for 9310 steel. The results showed that a pronounced small‐crack effect was not observed even at R = ?1, small cracks initiated by a slip mechanism at strong slip sites. Worst‐case near‐threshold testing results for large cracks under several K_max values showed that an effect of K_max on the near‐threshold behavior does not exist in the present investigation. A worst‐case near‐threshold test for a large crack, i.e. constant K_max/decreasing ΔK test, can give a conservative prediction of growth behavior of naturally initiated small cracks. Using the worst‐case near‐threshold data for a large crack and crack‐tip constraint factor equations defined in the paper, Newman's total fatigue‐life prediction method was improved. The fatigue lives predicted by the improved method were in reasonable agreement with the experiments. A three‐dimensional (3D) weight function method was used to calculate stress‐intensity factors for a surface crack at a notch of the present SENT specimen (with r/w = 1/8) by using a finite‐element reference solution. The results were verified by limited finite‐element solutions, and agreed well with those calculated by Newman's stress‐intensity factor equations when the stress concentration factor of the present specimen was used in the equations.     

Characterization of the nonlinear fracture resistance parameters for an aviation GTE turbine disc

The effects of crack growth rate model formulation, based on the elastic‐plastic and undamaged/damaged creep crack tip fields on the behaviour of low‐cycle fatigue and creep fracture resistance parameter behaviour, are represented by numerical calculations. The crack growth rate models include the fracture process zone size and damage parameters. An aviation gas turbine engine (GTE) rotating turbine disc is the focus of this innovative application of basic analytical and numerical solutions. For the GTE turbine disc, the constraint parameters, local fracture process zone sizes, and nonlinear plastic (K_p) and creep (K_cr) stress intensity factors are calculated by finite element analysis to characterize the fracture resistance along the semielliptical crack front as a function of the flaw aspect ratio, operation temperature, and disc rotation speed. Predictions of the creep‐fatigue crack growth rate and residual lifetime are given for different combinations of operation loading conditions and damage of the GTE turbine disc.     

Fatigue crack growth in fibre metal laminates with multiple open holes

The fatigue crack growth behaviour of hybrid S2‐glass reinforced aluminium laminates (Glare) with multiple open holes was investigated experimentally and analytically. It was observed that the presence of multiple‐site fatigue damage would increase crack growth rates in the metal layers as two propagating cracks converged. An analytical crack growth model was established for predicting crack growth rates based on empirical Paris equation. The effective stress intensity factor at crack tips is a function of mode I far‐field stress intensity factor, crack opening stress intensity factor and effective non‐dimensional stress intensity factor that incorporated the crack‐bridging effect in fibre metal laminates. The predicted results under different applied stress can capture the trend of averaged crack growth rates in experiments, although deviation exists in the predictions.     

Dynamic stress intensity factor due to concentrated loads on a propagating semi-infinite crack in orthotropic materials

The elastodynamic response of an infinite orthotropic material with a semi-infinite crack propagating at constant speed under the action of concentrated loads on the crack faces is examined. Solution for the stress intensity factor history around the crack tip is found for the loading modes I and II. Laplace and Fourier transforms along with the Wiener-Hopf technique are employed to solve the equations of motion. The asymptotic expression for the stress near the crack tip is analyzed which lead to a closed-form solution of the dynamic stress intensity factor. It is found that the stress intensity factor for the propagating crack is proportional to the stress intensity factor for a stationary crack by a factor similar to the universal function k(v) from the isotropic case. Results are presented for orthotropic materials as well as for the isotropic case.     

Fretting fatigue limit as a short crack problem at the edge of contact

This paper proposes a local stress concept to evaluate the fretting fatigue limit for contact edge cracks. A unique S–N curve based on the local stress could be obtained for a contact edge crack irrespective of mechanical factors such as contact pressure, relative slip, contact length, specimen size and loading type. The analytical background for the local stress concept was studied using FEM analysis. It was shown that the local stress uniquely determined the ΔK change due to crack growth as well as the stress distribution near the contact edge. The condition that determined the fretting fatigue limit was predicted by combining the ΔK change due to crack growth and the ΔK_th for a short crack. The formation of a non‐propagating crack at the fatigue limit was predicted by the model and it was experimentally confirmed by a long‐life fretting fatigue test.     

Micromechanisms of fatigue crack growth in a forged Inconel 718 nickel-based superalloy

The micromechanisms of fatigue crack propagation in a forged, polycrystalline IN 718 nickel-based superalloy are evaluated. Fracture modes under cyclic loading were established by scanning electron microscopy analysis. The results of the fractographic analysis are presented on a fracture mechanism map that shows the dependence of fracture modes on the maximum stress intensity factor, K_max, and the stress intensity factor range, ΔK. Plastic deformation associated with fatigue crack growth was studied using transmission electron microscopy. The effects of ΔK and K_max on the mechanisms of fatigue crack growth in this alloy are discussed within the context of a two-parameter crack growth law. Possible extensions to the Paris law are also proposed for crack growth in the near-threshold and high ΔK regimes.     

Fatigue crack growth through particulate clusters in polycarbonate material

The interaction of a crack with a perfectly bonded inclusion or a cluster of inclusions in polycarbonate matrix was investigated through both numerical simulations and fatigue tests. Stress intensity factors (K_I) were evaluated by boundary element method for several particle sizes, position and finally for inclusion cluster as a precursor study for the experiments. The numerical simulation has shown the crack tendency to circumvent the inclusions with consequential reduction of the growth rate. Fatigue crack growth tests were carried out on several particle-filled specimens at constant value of the applied stress intensity factor range (ΔK_Iapp) highlighting the crack delay due to the presence of the stiff second phase. The experiments demonstrated that the inclusion effect on the crack growth rate can be explained with a model based on the crack shielding effect in which the particle would act to reduce the effective stress intensity factor at crack tip (K_Ieff). Finally, the crack growth rate was predicted with an analytical model, and then compared to that obtained by the fatigue testing. Possible explanations for differences are discussed.     

Elastodynamic forms of caustics for running cracks under constant velocity

For the study of elastodynamic problems of propagating cracks it is necessary to evaluate the dynamic stress intensity factor K^d_I, which depends on the form of expressions for the stress components existing at the running crack tip at any instant of the propagation of the crack and the corresponding dynamic mechanical and optical properties of the material of the specimen under identical loading conditions. In this paper the distortion of the form of the corresponding reflected caustic from the lateral faces of a dynamically loaded transparent and optically inert specimen containing a transverse crack running under constant velocity was studied on the basis of complex potential elasticity theory and the influence of this form on the value of the dynamic stress intensity factor was given. The method was applied to the study of a propagating under Mode I crack in a PMMA specimen under various propagation velocities and the corresponding dynamic stress intensity factor K^d_I, evaluated.     

Question of determining the electrochemical condition in a developing crack in investigating the crack resistance in a corrosive medium

Conclusions The proposed method of crack resistance testing of constructional materials in corrosive media provides determination of the electrochemical condition at the tip of not only a steady but also of a propagating crack. The values of pH and at the tip of the crack change with growth of it.For an investigated material-medium system at the tip of a developing crack in cyclic loading the minimum pH of the medium pH _min ^tc is –0.4, which is much lower than the corresponding parameter for a statically loaded steady crack (pH _min ^{ts 2.3} ). Together with the stress intensity factor, the electrochemical condition at the crack tip determines the fatigue crack growth rate in a corrosive medium.Translated from Fiziko-Khimicheskaya Mekhanika Materialov, Vol. 18, No. 3, pp. 42–49, May–June, 1982.     

Mode I fatigue crack growth under biaxial loading

This paper is centred on the role of the T-stress during mode I fatigue crack growth. The effect of a T-stress is studied through its effect on plastic blunting at crack tip. As a matter of fact, fatigue crack growth is characterized by the presence of striations on the fracture surface, which implies that the crack grows by a mechanism of plastic blunting and re-sharpening (Laird C. The influence of metallurgical structure on the mechanisms of fatigue crack propagation. In: Fatigue crack propagation, STP 415. Philadelphia: ASTM; 1967. p. 131–68 [8]). In the present study, plastic blunting at crack tip is a global variable ρ, which is calculated using the finite element method. ρ is defined as the average value of the permanent displacement of the crack faces over the whole K-dominance area. The presence of a T-stress modifies significantly the evolution of plastic deformation within the crack tip plastic zone as a consequence of plastic blunting at crack tip. A yield stress intensity factor K_Y is defined for the cracked structure, as the stress intensity factor for which plastic blunting at crack tip exceeds a given value. The variation of the yield stress intensity factor was studied as a function of the T-stress. It is found that the T-stress modifies significantly the yield point of the cracked structure and that the yield surface in a (T, K_I) plane is independent of the crack length. Finally, a yield criterion is proposed for the cracked structure. This criterion is an extent of the Von-Mises yield criterion to the problem of the cracked structure. The proposed criterion matches almost perfectly the results obtained from the FEM. The evolution of the yield surface of the cracked structure in a (T, K_I) plane was also studied for a few loading schemes. These results should develop a plasticity model for the cracked structure taking into account the effect of the T-stress.     

Determining cyclic corrosion cracking resistance for titanium alloys with allowance for electrochemical conditions at the fatigue corrosion crack tip

Published data are examined on how various factors affect fatigue crack growth rates. Basic diagrams have been constructed for the cyclic cracking resistance in Ti-6AI-4V and Ti-6AI-6V-2Sn alloys in air, distilled water, and 3.5% NaCl for use in working-life calculations. Appropriate heat treatment can produce two microstructures in a titanium alloy, one of which has the largest cyclic cracking resistance, while in the second, the cracks grow at the lowest rate. The cyclic corrosion cracking resistance for a titanium alloy should be determined in relation to the state of stress and strain and to the electrochemical conditions at the corrosion fatigue crack tip, while the variations in fatigue crack growth rate for a given stress intensity factor in a corrosive medium are due to differing electrochemical conditions at the crack tip during the testing on different specimens. Basic diagrams can be derived for titanium alloys by using a physically sound methodology developed previously for steels, which is based on invariant diagrams for cyclic cracking resistance in air and in the corresponding medium, which can be constructed in relation to extremal working and electrochemical conditions at corrosion-fatigue crack tips.Translated from Problemy Prochnosti, No. 12, pp. 3–11, December, 1993.