Fretting fatigue crack analysis in Ti–6Al–4V

A study was conducted to verify the efficacy of a fracture mechanics methodology to model the crack growth behavior of fretting fatigue-nucleated cracks obtained under test conditions similar to those found in turbine engine blade attachments. Experiments were performed to produce cracked samples, and fretting fatigue crack propagation lives were calculated for each sample. Cracks were generated at 10⁶ cycles (10%-of-life) under applied stress conditions previously identified as the fretting fatigue limit conditions for a 10⁷ cycle fatigue life. Resulting cracks, ranging in size from 30 to 1200 μm, were identified and measured using scanning electron microscopy. Uniaxial fatigue limit stresses were determined experimentally for the fretting fatigue-cracked samples, using a step loading technique, for R=0.5 at 300 Hz. Fracture surfaces were inspected to characterize the fretting fatigue crack front indicated by heat tinting. The shape and size of the crack front were then used in calculating ΔKth values for each crack. The resulting uniaxial fatigue limit and ΔKth values compared favorably with the baseline fatigue strength (660 MPa) for this material and the ΔKth value (2.9 MPa√m) for naturally initiated cracks tested at R=0.5 on a Kitagawa diagram.Crack propagation lives were calculated using stress results of FEM analysis of the contact conditions and a weight function method for determination of ΔK. Resulting lives were compared with the nine million-cycle propagation life that would have been expected in the experiments, if the contact conditions had not been removed. Scatter in the experimental results for fatigue limit stresses and fatigue lives had to be considered as part of an explanation why the fatigue life calculations were unable to match the experiments that were modeled. Analytical life prediction results for the case where propagation life is observed to be very short experimentally were most accurate when using a coefficient of friction, μ=1.0, rather than for the calculations using μ=0.3     

Hypervelocity impact damage to Ti–6Al–4V meshes reinforced Al–6Mg alloy matrix composites

An Al–6Mg alloy matrix composite reinforced with Ti–6Al–4V meshes was fabricated by pressure infiltration method; its damage behaviors impacted by hypervelocity aluminum projectiles were investigated. Results showed that the thin Ti_f/Al–6Mg composite target exhibits better protection efficiency and energy absorption ability than Al–6Mg alloy target. With projectile sizes increasing, bulge and spallation were observed on the back of the composite target. The Ti–6Al–4V meshes were tensed and deformed drastically in the spallation region, where micro-damages such as interfacial debonding and cracks were dominant. Shear localization was the primary failure characteristic for thin Al–6Mg alloy target. The adiabatic shear bands were observed near the crater of Al–6Mg alloy, not in Ti_f/Al–6Mg composite target. It was ascribed to the Ti–Al interfacial bonding strength and the high temperature strength for Ti–6Al–4V alloy.     

Superplastic Property of the Ti–6Al–4V Alloy with Ultrafine‐Grained Heterogeneous Microstructure

Ti–6Al–4V alloy having a heterogeneous microstructure composed of ultrafine‐equiaxed‐α‐grains and fine‐lamellar‐α‐grains is investigated for microstructural changes during superplastic deformation at temperature of 700 °C. The Ti–6Al–4V alloy having an optimum fraction of fine‐lamellar‐α‐grains exhibits an excellent superplastic property and the highest elongation of 583% (tested at 700 °C 10^?3 s^?1). This is mainly due to the optimized activation of grain‐boundary‐sliding and additional accommodation mechanism associated with frequent occurrences of dynamic recrystallization and β precipitation at boundaries during deformation of the heterogeneous starting microstructure. The present result suggests the possibility that optimizing the starting microstructure so as to have an optimum heterogeneous‐microstructure serves as an additional stress accommodation mechanism and leads to a large superplastic elongation.

     

Probabilistic modeling of fatigue crack growth in Ti–6Al–4V

This paper proposes an approximate approach to efficient estimation of some variabilities caused by the material microstructural inhomogeneities. The approach is based on the results of a combined experimental and analytical study of the probabilistic nature of fatigue crack growth in Ti–6Al–4V. A simplified experimental fracture mechanics framework is presented for the determination of statistical fatigue crack growth parameters from two fatigue tests. The experimental studies suggest that the variabilities in long fatigue crack growth rate data and the Paris coefficient are well described by the log-normal distributions. The variabilities in the Paris exponent are also shown to be well characterized by a normal distribution. The measured statistical distributions are incorporated into a probabilistic fracture mechanics framework for the estimation of material reliability. The implications of the results are discussed for the probabilistic analysis of fatigue crack growth.     

Fatigue strength of Ti–6Al–4V at very long lives

The objective of this research was to investigate the fatigue strength of Ti–6Al–4V using an ultrasonic fatigue system. Fatigue testing up to 10⁹ cycles under fully reversed loading was performed to determine the ultra-high cycle fatigue behavior of Ti–6Al–4V. Endurance limit results were compared to similar data generated on conventional servohydraulic test systems and electromagnetic shaker systems to determine if there are any frequency effects. Fatigue specimens were tested with and without cooling air to determine the effects of increased specimen temperature caused by internal damping due to cycling at a very high frequency. An infrared camera was also used to record specimen temperatures at various load levels. Results indicate that the effects of frequency, including internal heating, on the very high cycle fatigue behavior of Ti–6Al–4V are negligible under fully reversed loading conditions.     

Microstructure and superplasticity of laser welded Ti–6Al–4V alloy

In this paper laser beam welding (LBW) was used to join Ti–6Al–4V alloy as a pre-forming operation before superplastic deformation (SPF) process. Superplastic deformation behavior of laser welded Ti–6Al–4V alloy was investigated. The results indicated that the welded Ti–6Al–4V alloy had good superplasticity when deformed at temperature range of 870–920 °C and strain rate range of 10⁻³–10⁻² s⁻¹, and the elongation was 233–397%. The microstructure observation indicated that dynamic recrystallization happened in the weld bead, and the acicular structure of weld bead was transforming into equiaxed grains during tensile process.     

Fretting fatigue behavior of shot-peened Ti–6Al–4V under seawater environment

The fretting fatigue behavior of the shot-peened titanium alloy, Ti–6Al–4V, was investigated under a seawater environment using a servo-hydraulic fatigue test machine equipped with a rigid fretting fixture. Fretting fatigue tests were performed over a wide range of stress levels to characterize the effects of seawater at high and low cycle fatigue regimes. The results of this study showed that (1) seawater reduces the fretting fatigue life of shot-peened Ti–6Al–4V in both high and low cycle fatigue regimes relative to their counterparts in ambient laboratory condition, and (2) shot-peening increases the fretting fatigue life of Ti–6Al–4V when tested under dry or seawater condition relative to its counterpart of unpeened Ti–6Al–4V. The seawater environment promotes an increase in crack propagation rate; however the crack initiation depends upon the combination of the detrimental effect from seawater environment and the beneficial effect from the residual compressive stress from shot-peening. In the present study, it appears that their cumulative effects were dominated by the residual compressive stress in both low cycle and high cycle fatigue regimes. On the other hand, the seawater environment has detrimental effect on the fretting fatigue life of unpeened Ti–6Al–4V than that in ambient laboratory condition in the low cycle fatigue regime while it improves slightly the life in the high cycle fatigue regime.     

Numerical analysis of superplastic blow forming of Ti–6Al–4V alloys

The superplastic blow forming of a Ti–6Al–4V sheet into a cylindrical cup has been numerically analysed based on the actual forming process using ABAQUS. A detailed element type study has been performed to eliminate the element dependency in the finite element analysis. The accuracy and reliability of the proposed finite element model has been validated in comparison with experimental data. The validation proves that, there is a good agreement between the simulation and the experiment. In addition, the best prediction of the thickness distribution can be obtained using the continuum element. Furthermore, the effects of major factors such as friction coefficient and the strain rate sensitivity index upon the optimum forming pressure-time and thickness distribution of the component have been studied systematically using the proposed finite element model.     

Surface hardening of biomedical Ti–29Nb–13Ta–4.6Zr and Ti–6Al–4V ELI by gas nitriding

The microstructure and hardness near the surface of a biomedical titanium alloy, Ti–29Nb–13Ta–4.6Zr (TNTZ), subjected to gas nitriding at 1023–1223 K was investigated in comparison with the conventional biomedical Ti–6Al–4V ELI (Ti64). After gas nitriding, the microstructure near the specimen surface was observed by optical microscopy, X-ray diffraction (XRD), Auger electron spectroscopy (AES), and X-ray photoelectron spectroscopy (XPS). In both alloys, two types of titanium nitrides (TiN and Ti₂N) are formed and the phase is precipitated by gas nitriding. Furthermore, the oxygen impurity in the gas nitriding atmosphere reacts with the titanium nitrides; thus, TiO₂ is formed at the outermost titanium nitride layer. The surface hardening was also evaluated by Vickers hardness measurement. The Vickers hardness near the surface of TNTZ and Ti64 increases significantly by gas nitriding.     

Formation of nanocrystalline structure of Ti–6Al–4V alloy by cyclic hydrogenation–dehydrogenation treatment

Ti–6Al–4V (Ti64) sheet specimens were cathodically hydrogenated in sulfuric acid solution at ambient conditions. The hydrogenated specimens were then sent to go through the designed thermohydrogen processing (THP) twice to obtain a nano-sized grain structure. The average grain size of resulted microstructure was found to be 10–20 nm obtained by TEM. Qualitative and quantitative analyses performed by employing X-ray diffractometry (XRD) and elemental analysis (EA) showed that the addition of As₂O₃ as hydrogenation promoter in electrolyte significantly increased the hydrogen uptake. The high concentration of hydrogen arising from promoter action is the key factor in grain refinement. The optimal processing parameter found for grain-refining Ti64 was: (1) electrolytic hydrogenation at 100 mA cm⁻² for 3 h in 1 N H₂SO_4(aq) by adding 0.1 g L⁻¹ As₂O₃; (2) β transformation carried out at 850 °C for 1 h in air furnace, followed by a furnace cooling to 590 °C and held for 6 h; (3) oxide film removed and then dehydrogenated at 650 °C and 1.0 × 10⁻⁶ Torr for 10 h; (4) repeated the same processes once more.     

Al–Si coating fused by Al + Si powders formed on Ti–6Al–4V alloy and its oxidation resistance

An Al–Si coating was successfully produced by means of the low oxygen pressure fusing technology for improving the oxidation resistance of Ti–6Al–4V alloy. The Al and Si concentration in coating and coating thickness could be controlled by adjusting powder mixing ratio and changing the technical parameters (fusing temperature and time), respectively. At 1273 K, the weight gain of the Al–20Si coating increased with prolonging fusing time and its equation could be described as Δm² = 3.62t. After 105 h oxidation, the oxidation rate of the Al–20Si coated specimen with fusing time 100 min was about two to four times than that of the Al–10Si coated specimen with fusing time 60 min.     

Electrochemical corrosion properties of Ti–6Al–4V implant alloy in the biological environment

The electrochemical corrosion behavior of Ti–6Al–4V implant alloy was investigated in three biological solutions, i.e. urine, serum and joint fluid. The corrosion properties of Ti–6Al–4V implant alloys were examined by using electrochemical techniques, such as the potentiodynamic method, cyclic voltammetry, electrochemical impedance spectroscopy (EIS). The electrochemical corrosion characteristics of Ti–6Al–4V implant alloys in three biological solutions were measured in terms of the corrosion potential (E_corr), the corrosion current density (i_corr), and ac polarization resistance (R_p). The corrosion kinetic parameters were calculated from both the Tafel plot analyses and EIS analyses. The dependence of impedance versus potentials was studied at 37 °C at various offset potentials in three biological solutions. The ac circuit model for Ti–6Al–4V implant alloy at corrosion interface in biological solution was proposed, which was based on a simple Randles equivalent circuit. It was found that the Ti–6Al–4V implant alloy in three biological solutions showed a characteristic of a capacitive behavior. The experimental results of Tafel plot analyses were found in good agreement with that of EIS analyses.     

A multiphase mechanical model for Ti–6Al–4V: Application to the modeling of laser assisted processing

A multiphase model for Ti–6Al–4V is proposed. This material is widely used in industrial applications and so needs accurate behaviour modeling. Tests have been performed in the temperature range from 25 °C to 1020 °C and at strain rates between 10⁻³ s⁻¹ and 1 s⁻¹. This allowed the identification of a multiphase mechanical model coupled with a metallurgical model. The behaviour of each phase is calibrated by solving an inverse problem including a phase transformation model and a mechanical model to simulate tests under thermomechanical loadings. A scale transition rule (β-rule) is proposed in order to represent the redistribution of local stresses linked to the heterogeneity of plastic strain. Finally this model is applied to two laser assisted processes: direct laser fabrication and laser welding.