共查询到15条相似文献,搜索用时 78 毫秒
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用Y、Ba、Cu的三氟乙酸盐溶液,通过MOD法在SrTiO3(100)衬底上成功地制得了黑色的、表面光滑的YBCO超导薄膜。研究了两种理想的成膜烧结工艺,对膜进行了物相研究。结果表明:在850℃,潮湿氧气氛中烧结的薄膜具有一定的择优取向;而在750℃,潮湿的低氧气氛中烧结的薄膜则具有高度的c轴织构,前者的Tc(onse)≈90K,Tc0≈79K,较低的氧分压似乎有利于c轴结构。 相似文献
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FAN Yongnian TANG Baozhen QIAO Guiwen Institute of Metal Research Academia Sinica Shenyang China Associate Professor Institute of Metal Research Academia Sinica Shenyang China 《金属学报(英文版)》1993,6(7):21-24
Interfaces and surfaces of YBa_2Cu_3O_(7-x)(YBCO)-Ag have been studied by SEM-EDXand AES.No effect of Ag on 123 structure in X-ray diffraction pattern was observedfor 0.4 mol Ag doped YBCO.AES analysis indicated that Ag segregated on surfaceof YBCO and resulted in decrease of YBCO-metal lead resistance.In addition,solutionand segregation of Ag as elemental state were often appeared on interfaces and surfacesof high temperature annealed YBCO,whether elemental Ag or compound Ag_2O andAgNO_3 adopted as doping material. 相似文献
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采用密度泛函理论(DFT)中的BLYP和ROBLYP交换.相关泛函,基于YBa2Cu3O7单晶胞即39个原子组成的团簇模型,计算了其能隙、磁化系数、电子比热及比热系数随温度的变化关系,并分析了在不同温度下其最高占据态的分子轨道图。结果表明,YBa2Cu3O7存在3个特征温度Tc、T^*和T^0,在正常态存在赝能隙,并且其超导能隙和赝能隙均具有d波对称性。 相似文献
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采用脉冲激光沉积技术(PLD)在{001}LaAlO3(LAO)衬底上生长YBa2Cu3O7-x(YBCO)薄膜,并通过极图、摇摆曲线以及倒易空间图谱等高分辨X射线衍射技术(HRXRD)对其微结构进行表征。结果表明,YBCO薄膜的晶粒取向主要为{001}YBCO//{001}LAO,〈100〉YBCO//〈100〉LAO,但还有2%的{001}YBCO//{001}LAO,〈110〉YBCO//〈100〉LAO取向。摇摆曲线结果表明,YBCO的面外取向有一定的漫散(宽度为0.75°);薄膜面内存在90°±0.65°〈110〉孪晶畴结构,主要是由四方到正交的相变过程中较大的局部应力以及〈100〉和〈010〉方向应力差异引起的。 相似文献
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LI Ying WANG Xiaotian JIN Zhihao Xi''''an Jiaotong University Xi''''an China SHl Guoshun Beijing Measuring Analysing Center.Beijing China 《金属学报(英文版)》1992,5(12):516-520
The effect of subzero treatment on the microstructure and mechanical properites of Y_2O_3-ZrO_2 ceramic have been investigated by TEM,X-ray diffraction and test of mechanicalproperties.It was shown that the microstructre of 3Y-PSZ after subzero treatment byliquid nitrogen exhibits very long and parallel laths of m-phase and some microcracksaround the larger and finer lath of m-phase may be discovered.Suitable subzero treatmentcan improve the strength and toughness of Y-PSZ efficiently because of decreasing thestability of t-phase and incresing the amount of t-m transformation when exerting astress.However,when the time of subzero treatment exceeds,the over aging effect mayarise.which can decrease the strength and toughness of the material. 相似文献