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Experimentally determined p,V,T data are reported for toluene, trichloromethane, dichloromethane, acetonitrile, aniline, and n-dodecane at 278, 288, 298, 313, and 323 K, except for dichloromethane, for which the highest temperature was 298 K. At each temperature, measurements were done at pressures up to about 280 MPa or (for aniline and n-dodecane) at a lower pressure slightly below the freezing pressure at the temperature of measurement. Values of the isobaric expansivity isothermal compressibility and (for toluene, trichloromethane, dichloromethane, and acetonitrile) internal pressure, derived from the p,V,T data, are presented. 相似文献
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通过优化微波消解条件,并根据不同元素性质,调谐ICP-AES工作条件至最佳,实现了茶叶中K、Na、P、S以及Fe、Mn、Cu、Zn、Ca、Mg 10种元素的同时测定。10种元素测定结果 RSD%为0.67(Cu)~5.57(Na),回收率为84.0%(Na)~101.5%(Fe),检出限为0.001(Mn)~0.029(S)μg·g-1,表明该方法准确可靠,能够满足茶叶中K、Na、P、S、Fe、Mn、Cu、Zn、Ca、Mg分析要求。 相似文献
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Optical properties of the metals Al, Co, Cu, Au, Fe, Pb, Ni, Pd, Pt, Ag, Ti, and W in the infrared and far infrared 总被引:5,自引:0,他引:5
Infrared optical constants collected from the literature are tabulated. The data for the noble metals and Al, Pb, and W can be reasonably fit using the Drude model. It is shown that -epsilon1(omega) = epsilon2(omega) approximately omega(2)(p)/(2omega(2)(tau)) at the damping frequency omega = omega(tau). Also -epsilon1(omega(tau)) approximately - (1/2) epsilon1(0), where the plasma frequency is omega(p). 相似文献
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Vilas G. Pol Swati V. Pol Aharon Gedanken 《Advanced materials (Deerfield Beach, Fla.)》2011,23(10):1179-1190
This review compiles various nanostructures fabricated by a distinct “dry autoclaving” approach, where the chemical reactions are carried out without solvents; above the dissociation temperature of the chemical precursor(s) at elevated temperature in a closed reactor. The diversity to fabricate carbides (SiC, Mo2C, WC), oxides (VOx‐C, ZnO, Eu2O3, Fe3O4, MoO2), hexaborides (LaB6, CeB6, NdB6, SmB6, EuB6, GdB6), nitrides (TiN, NbN, TaN), phosphides (PtP2, WP), sulfides (ZnS, FeS/C, SnS/C, WS2, WS2/C), and selenides (Zn1‐xMnxSe/C, Cd1‐xMnxSe/C), with various shapes and sizes is accounted with plausible applications. This unique single‐step, solvent‐free synthetic process opens up a new route in the growing nanomaterials science; owing to its considerable advantages on the existing approaches. 相似文献
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蔡旭平 《现代测量与实验室管理》2002,10(4):61-63
我所2001年9月份顺利地通过了中国实验室认可委紧张而严格的评审,得到了权威机构认可,成为西南地区较早通过国家实验室认可的省级计量校准机构.在建立质量体系、运行质量体系走过了艰辛之路,我们将全所职工的艰辛之路介绍给大家,希望能给将要申请认可的实验室得以参考. 相似文献
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《中国标准化(英文版)》2012,(2):5-9
Standards IGRS:First Complete International Standards System in 3C Collaboration Field After ISO and IEC released three international standards of Intelligent Grouping and Resource Sharing (IGRS) including Core Protocol,File Communication Framework and Device Validation,four standards of IGRS,Application Framework,Basic Application,Service Types and Devices Types,got approved with high passing rate in the voting of Final Draft International Standard (FDIS) and will be officially issued soon around the world. It symbolizes that all 相似文献
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W. Wong-Ng J. A. Kaduk I. Levin W. Greenwood J. Dillingham 《Journal of research of the National Institute of Standards and Technology》2001,106(4):691-707
X-Ray Rietveld refinements were conducted on a series of eleven lanthanide phases, Sr2RGaCu2Oy (2112 phase, R = Pr, Nd, Sm, Eu, Gd, Dy, Ho, Y, Er, Tm, and Yb) that are structurally related to the high Tc superconductor Ba2YCu3O7 (213). In the 2112 structure, instead of square planar Cu-O chains, tetrahedral GaO4 chains were found to run in a zig-zag fashion along the diagonal of the basal 213 ab-direction. Reference powder patterns for these compounds were prepared by using the Rietveld decomposition technique. The unit cell volume of these compounds follows the expected trend of the lanthanide contraction. The lattice parameters range from a = 22.9694(3) Å, b = 5.5587(2) Å, and c = 5.44743(7) Å for R = Pr, to a = 22.8059(2) Å, b = 5.46031(5) Å, and c = 5.37773(5) Å for R = Yb. An electon diffraction study of the Sm- and Er-analogs showed characteristic diffuse streaks along the b-axis, suggesting some disorder within the GaO4 chains. 相似文献
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Phase-shift interferometry has provided a straightforward method for converting interferograms to phase maps. Unfortunately, some of the most powerful pulsed holographic interferometry techniquesare generally not compatible with phase-shift interferometry. One solution is to employ two reference waves, one for each of the two object waves to be interfered, that can be phase stepped during reconstruction. Practical aberration and alignment problems render this approach difficult. A simple method that employs a second hologram, sandwiched with the first, which produces the required two reference waves during reconstruction, is presented. The process compensates for both chromatic and geometric aberrations that otherwise render the phase-shift method unusable. 相似文献
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D. N. Talwar D. Sofranko C. Mooney S. Tallo 《Materials Science and Engineering: B》2002,90(3):269-277
Simple tight-binding simulations, incorporating only the Herman–Skillman atomic term values, are shown to provide valuable information about the bonding, elastic and structural properties of zinc-blende group III-nitrides. Our calculated values of the elastic parameters (viz., bulk modulus, elastic stiffness constants, Kleinman's internal displacement parameter, Keating force constants, etc.) for BN, AlN, GaN, and InN are shown to exist well within the range of values derived from more sophisticated methods. Despite the crude approximations used, the tight-binding method has clearly provided the meaningful trends to the local distortions around isoelectronic impurities and has described reasonably well the bond length variations as a function of composition in ternary alloys. 相似文献
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N. N. Breslavskaya A. L. Buchachenko 《Fullerenes, Nanotubes and Carbon Nanostructures》2005,12(1):47-52
The equilibrium geometries, electronic structures, and binding energies between the noble gases X (X = He, Ne, Ar) and Cn (n = 20, 24, 30, 32, 40, 50, 60) in X@Cn were calculated at B3LYP level of theory using 6-31G* and 6-311G* basis sets. We expect that the introduction of He, Ne, and Ar into Cn creates molecules with a high energy content. The relative stabilities of Cn fullerenes and corresponding endohedrals X@Cn are discussed. 相似文献
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The state of mineral-like uranovanadates of mono- and bivalent metals in aqueous solutions was studied. Based on experimental solubility data, the reaction equilibria in the crystal uranovanadate-aqueous solution system were described quantitatively, which, in turn, allowed evaluation of the solubility products of uranovanadates and their standard Gibbs energies of formation and prediction of the solubility of these compounds in aqueous solutions of various compositions under the isobaric-isothermal conditions. 相似文献
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商业设计只有第一没有第二 总被引:1,自引:0,他引:1
许多人将设计和艺术、美术划上等号,似乎一件好的设计就应该等于一幅美丽的图稿.其实不然,美术与美学只是设计的基础(也该是一般大众生活的基础),设计的天空相当广阔,与每个人的生活经历和氛围皆有关连;因此我们可以说“设计是生活,生活是一切”。 相似文献
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