THE USE OF A SPOUTED BED IN THE FERTILIZER COATING OF SOYBEAN SEEDS

ABSTRACT

Soybean seeds were coated with fertilizer by the atomization of a fertilizer suspension using a spouted bed. The efficiency of coating adhesion was measured as the coating mass adhering to the seeds and the sprayed solids mass. The change in moisture mass between coated and uncoated seeds was considered in the evaluation of yield. A study of binder concentration and process time was conducted in order to discover conditions under which germination of coated seeds was feasible. Final experiments were done in order to quantify the influences of spouted bed air temperature and fertilizer suspension flowrate on the process yields and the germination capacity of coated seeds. Two empirical equations resulted from the use of Myers' surface technique (1976). These equations predict yield and germination for the range of variables studied.     

THE USE OF A SPOUTED BED IN THE FERTILIZER COATING OF SOYBEAN SEEDS

Soybean seeds were coated with fertilizer by the atomization of a fertilizer suspension using a spouted bed. The efficiency of coating adhesion was measured as the coating mass adhering to the seeds and the sprayed solids mass. The change in moisture mass between coated and uncoated seeds was considered in the evaluation of yield. A study of binder concentration and process time was conducted in order to discover conditions under which germination of coated seeds was feasible. Final experiments were done in order to quantify the influences of spouted bed air temperature and fertilizer suspension flowrate on the process yields and the germination capacity of coated seeds. Two empirical equations resulted from the use of Myers' surface technique (1976). These equations predict yield and germination for the range of variables studied.     

Three-dimensional simulation of the effect of draft tube on minimum fluidization velocity in a spouted bed

The granular Eulerian model is used in three-dimensional hydrodynamic simulation of spouted bed to calculate the minimum fluidization velocity. Air is used as the main fluid and soybean seeds as the fluidized particles. The results of simulation are compared with the experimental data, and good agreement is obtained. In this simulation the effect of draft tube and its distance from the bed inlet at minimum fluidization velocity is studied. The results showed that the existence of draft tube decreases the minimum fluidization velocity and the increase of draft tube distance from the bed inlet increases this velocity.     

Study on the Efficiency of Hard Gelatin Capsules Coating in a Spouted Bed

Abstract

The aim of this work was to study the process of capsules coating in a lab-scale spouted bed. A conventional spouted bed (CSB) with 9.5 cm column diameter and 60° conical base was used in the experiments. The spouting fluid dynamics of capsules with different sizes were determined. In the equipment used only capsules size 03 (outer diameter: 5.82 cm; length: 15.9 mm) presented stable spouting. The effect of capsules load in the column, coating suspension viscosity, and coating time on the coating efficiency were studied in a factorial experimental design. Typical efficiencies for the process were found to be in the range of 69.54–84.88%. The efficiencies increased with bed load at 1% significance level, but were not affected by coating time and suspension viscosity. CBS is a promising method for the HGC coating that eliminates preliminary sealing steps.     

Influence of Polymeric Suspension Characteristics on the Particle Coating in a Spouted Bed

The influence of the coating suspensions and particle properties on the coating process in a conventional spouted bed is presented. Glass beads were coated at fixed operating conditions with different formulations of aqueous polymeric coating suspensions in a spouted bed of laboratory scale. The wettability of the solids by the liquid was quantified by the contact angle and surface tension of the coating suspensions. The coating efficiency and particle growth were correlated with the adhesion of the coating suspension to the solid particle, which is a function of the solids and liquid characteristics. The physical properties of the coated particles—particle mean diameter, sphericity, bulk, absolute and apparent densities, porosity and flow velocity—were determined and compared to the properties of uncoated particles.     

Influence of Polymeric Suspension Characteristics on the Particle Coating in a Spouted Bed

Abstract

The influence of the coating suspensions and particle properties on the coating process in a conventional spouted bed is presented. Glass beads were coated at fixed operating conditions with different formulations of aqueous polymeric coating suspensions in a spouted bed of laboratory scale. The wettability of the solids by the liquid was quantified by the contact angle and surface tension of the coating suspensions. The coating efficiency and particle growth were correlated with the adhesion of the coating suspension to the solid particle, which is a function of the solids and liquid characteristics. The physical properties of the coated particles—particle mean diameter, sphericity, bulk, absolute and apparent densities, porosity and flow velocity—were determined and compared to the properties of uncoated particles.     

Coal gasification in a spouted bed

Low Btu gas has been produced by gasifying coal in a spouted bed reactor. Coal of size 0.8-3.6 mm is fed continuously to a 0.15 m diameter spouted bed of inerts and gasified using mixtures of steam and air. Tests of the process with Western Canadian coals of free swelling index 0, 4 and 7 are reported. Gases of heating value to 3.61 MJ/m³ were produced at coal throughputs of 0.188 kg/m²s with the reactor operating at atmospheric pressure and temperatures to 930°C. Characteristics of the spouted bed gasifier are presented and results compared to commercial moving and fluidized bed systems. A simple mathematical model based on the two-region spouted bed model of Mathur and Lim is used to predict the effect on steam utilization of bed composition, bed height and diameter, and particle size.     

Statistical modelling of the spouted bed coating process using positron emission particle tracking (PEPT) data

Coating of particles larger than about 1 mm can be achieved in a spouted bed, a particle mobilization device in which a strong particle circulation occurs, rapidly upwards in a lean central “spout” region and downwards in a slowly moving annular settled bed. In a spouted bed coater, a spray nozzle is placed at the base of the spout, spraying upwards into a distinct coating zone. The coating formation in a spouted bed is inter alia a function of (i) the particle motion, that is, how often and where particles enter and traverse the coating zone and (ii) the extent of droplet collection by individual particles passing through the coating zone. The coating model proposed here is based on the statistical history of individual particles, whose projected area governs the collection of spray droplets in the coating zone. Positron emission particle tracking (PEPT) has been used to determine the particle trajectories, the distribution of cycle times and the size and voidage of the spout. Whilst the model is not capable of delivering absolute values of coating mass a priori, it can predict deviations from a mean, which can itself be determined from an overall mass balance. To validate the model, a spouted bed coating process was studied in which coarse PVC spheres were coated with the hot‐melt coating material polyethylene glycol (PEG) 1500. Coating mass distributions, derived from the weight data of individual particles before and after manual coating removal, compared (for the studied conditions) very well with the predictions of the model.     

浅喷动床内多气体入口对颗粒涂敷层的影响

本文介绍了一种应用于核燃料颗粒涂敷的具有多气体入口的浅喷动床,研究了其中的气体入口和反应气体的布置,通过控制涂敷反应发生区域,提高了颗粒涂敷层厚度和颗粒直径分布的均匀性.     

Pressure drop,bed expansion and liquid holdup in a three phase spouted bed contactor

Data on the pressure drop, bed expansion and liquid holdup in a three phase spouted bed contactor with an initial bed height of 243 mm. were obtained as a function of the gas and liquid flowrate. Polyethylene spheres 10 mm. in diameter with a density of 320 kg/m³ were spouted in a 194 mm. column using a 30 mm. nozzle. The spouted bed contactor with gas and liquid mass flow-rates of 2.18 and 1.88 kg/m² sec, respectively had similar pressure drop per unit area of particle surface, total liquid holdup per unit volume of operating bed, and “active” holdup, as a fluidized contactor.     

Purple-Fleshed Sweet Potato Cubes Drying in a Microwave-Assisted Spouted Bed Dryer

Purple-fleshed sweet potatos (PFSP) were loaded into a laboratory-scale, microwave-assisted spouted bed with a coating of sodium alginate (SA) of 0, 0.2%, 0.4%, 0.8% (w/w) for both steam-blanching pretreated and fresh-cut raw samples. The drying curves, rehydration ratio, and maximum penetrating forces were studied for final products; color changes and anthocyanin level were also taken into consideration. It was concluded that coating processing forms barriers to moisture content, which changes the dielectric properties of PFSP cubes and shortens the drying time; however, coating PFSP cubes with SA did not lead to a porous microstructure in the final products. The final hardness was high and rehydration ratio was low. Steam-blanching was helpful for color and anthocyanin-level retention compared with raw samples. In sum, microwave-assisted spouted bed (MWSB) drying of PFSP cubes is not an ideal processing method, even with coating treatment, but blanching is an approach to obtain products with high anthocyanin level and fine purple color.     

Hydrodynamic study of fine metallic powders in an original spouted bed contactor in view of chemical vapor deposition treatments

An original gas-solid contactor was developed so as to treat by chemical vapor deposition, fine (mean diameter 23 μm) and dense (bulk density 7700 kg/m³) NiCoCrAlYTa powders with large size distribution. In order to avoid the presence of a distributor in the reactive zone, a spouted bed configuration was selected, consisting in a glass cylindrical column associated through a 60° cone to an inlet tube, connected at its bottom to a grid so as to support the powders at rest. A hydrodynamic study was conducted at ambient temperature and pressure, combining pressure drop measurements and visual observations as a function of gas velocity and of the ratio H/D of the height of the bed at rest over the bed diameter. Using conventional alumina particles belonging to Geldart's group B, it was shown that this equipment is able to ensure conventional spouted bed behavior, especially for H/D ratio equal to 1. From numerous experiments conducted with the fine metallic powders of interest, it was shown that (i) conventional pressure drop curves for spouted beds are obtained for H/D ratios between 1 and 1.8, (ii) due to the large grain size distribution of particles, minimum spouted bed velocities occur in a range rather than at precise values. Visual observations reveal the presence of the spout and fountain at the minimum spouted bed velocity and for H/D equal to 1.     

Simulations of flow behavior of gas and particles in spouted bed with a porous draft tube

Flow behaviors of particles in a two-dimensional spouted bed with a porous draft plates are studied using a fluid dynamic computation with kinetic-frictional stresses models. Gas flow through the porous draft tube is simulated by Brinkman-Darcy-Forchheimer formulation. The distributions of concentration and velocities of particles are predicted. Simulated results predict the solid circulation rate and gas flux rate measured in the spouted bed with a porous draft tube (Ishikura et al., 2003). The solid circulation rate in the spouted bed with a porous draft tube is larger than that with a non-porous draft tube. The predicted bed pressure drop with the porous draft tube is high in comparison to the spouted bed with non-porous draft tube. The effect of the porosity of the porous draft tube on distributions of gas flux rate through the annulus and solid circulation rate are discussed.     

The Gas-to-Particle Heat Transfer and Hydrodynamics in Spouted Bed Drying of Sawdust

Abstract

This article presents experimental results for spouted bed drying of sawdust, carried out in a full-scale as well as in a laboratory-scale dryer using air as well as steam as drying media. The aim is to present design parameters for a spouted-bed sawdust dryer that can be used by the industry in designing full-scale dryers. A hydrodynamically stable spouted jet spouted bed was obtained. The heat transfer characteristics of the bed were represented in terms of a volumetric heat transfer coefficient (VHC). When sawdust is dried in a spouted bed, the mean VHC is increasing up to fiber saturation level (20–25% wb) from 40 to 110 W/m³ K. The VHC decreases with the residence time and with an increased static bed height. Gas temperature profiles are also presented for the bottom part of the drying chamber.     

Modeling of Seed Coating in a Spouted Bed

In this work, a model based on population balance equations applied to perfect mixture domains has been employed to represent the coating of soybeans with fertilizer in a conical–cylindrical spouted bed. The results of the present model provided explicit equations for the coating mean and variance. The coating mass distribution function was validated against experimental data. The effect of operational time on the distributions was analyzed, showing that the coating uniformity can be improved by increasing the operating time.     

Investigation into the viability of a liquid-film three-phase spouted bed biofilter

A variety of technologies exist for the treatment of malodorous air streams, including adsorption, absorption, catalytic combustion, biofiltration and bioscrubbing. Conventional packed bed biofiltration of malodorous substances from waste gas streams has the disadvantages of large unit surface area and relatively uncontrolled design principles. The large bed surface area leads to difficulties in maintaining even moisture and temperature profiles. In addition, the control of such biologically important parameters as pH is difficult. Novel fluidized/spouted beds were studied for biological treatment of gases because of their high specific gas flowrate and vigorous mixing which facilitates enhanced gas–biomass contact. Trials of a range of fluidized and spouted beds, with gas loadings of up to 14000 m³-gas m⁻²-bed h⁻¹, were carried out on various biofilm support media including glass ballotini, rice hulls, plastic discs and granules, silica gel, molecular sieves, vermiculite, perlite, activated carbon, cork, polystyrene and expanded clay. Severe aggregation and wall adhesion restricted the operational range of the reactors. Particle suitability was based on a combination of shape, density, size, porosity and wettability, with large, heavy clay particles performing best. Limited gas-phase bacterial studies on selected media with ammonia- and nitrite-oxidizing bacteria demonstrated the potential of fluidized/spouted beds for efficient biofiltration of ammonia (20–40 mg dm⁻³). © 1998 Society of Chemical Industry     

DRYING OF OILSEEDS

Drying of oilseeds is a post harvest operation required for safe storage of harvested seeds. Oilseeds have gained importance in India over the last few years. Fluidized bed (FB) drying and Spouted Bed (SB) drying of oilseeds were studied as potential dryers for these seeds. Experimental pilot fluidized bed dryers were developed and a 2 TPH capacity (mustard seed) FB dryer plant was designed and installed in the lab. Experimental units and a pilot spouted bed dryer were also developed. The dryer units and the plant have been extensively tested and satisfactory drying performance has been achieved. Drying data and drying characteristics have been generated for different oilseeds such as mustard, sunflower, soybean and groundnut etc. The drying rates in different regimes of drying characterized by constant rate and falling rate periods have been evaluated. The salient results of the work are briefly outlined.     

Effect of process conditions on particle growth for spouted bed coating of urea

The aim of this work was to analyze the influences of operational variables on particle growth for urea coating in a conventional spouted bed (CSB). An aqueous polymeric suspension was the coating liquid sprayed on the spouted particles. The effects of inlet air temperature, coating suspension flow rate and atomizing air pressure on particle growth were analyzed by a central composite rotatable design (CCRD) of experiments. The results showed particle growth in the range of 1.1–2.6%, therefore, some results below the expected for a film coating (2–8%). A second-order polynomial model was obtained for estimating particle growth as a function of the statistically significant variables: air temperature, suspension flow rate and atomizing air pressure, with percentage of explained variation R² = 90.72%. The urea growth kinetics during coating was analyzed for the optimal operating condition and a linear growth coefficient of 1.13 × 10⁻³ min⁻¹ was obtained. The volatilization analyses showed that the polymer film coating provided a decrease of the nitrogen loss in the range of 3–57%. And, SEM analyses demonstrated a total, uniform and homogeneous covering of the urea particles surface.     

CONVECTIVE HEAT TRANSFER DURING COATING OF PARTICLES IN TWO-DIMENSIONAL SPOUTED BEDS

ABSTRACT

This work deals with the evaluation of gas-to-particle convective heat transfer in a process of coating of particles in two-dimensional spouted beds. A detailed calculus routine is presented and two correlations of heat transfer coefficient, for the spout and annular regions are derived. The study is performed with two, two-dimensional spouted beds with different sizes and with two different particles, placebo and soybean.     

Aerodynamics and heat transfer during coating of tablets in two-dimensional spouted bed

The two-dimensional spouted bed has been pointed out in recent research works as an improved configuration of spouted beds. The main advantages in relation to the conventional spouted beds are the easy construction and scale-up. In this work we begin the study of coating of tablets in two-dimensional spouted beds. An experimental system was constructed and the data obtained were used to determine the values of maximum pressure drop, minimum spout flowrate and gas-to-particle heat transfer coefficient, for 36 process conditions. The experimental results have been correlated with process and geometrical parameters.