聚乙烯自增强复合材料损伤过程的声发射特征

复合材料在承受外载时, 声发射可产生于基体破裂、纤维-基体界面脱粘和纤维断裂等。测定了U HMWPE/ HDPE 复合材料在拉伸载荷作用下的声发射(AE) 振幅信号。对特殊试样, 即预测到断裂有明确方式, 如纤维-基体界面脱粘、基体破裂、纤维断裂和分层等的试样, 实施加载直至破坏。用扫描电子显微镜(SEM) 观测试样的断裂表面, 对产生于若干特殊损伤类型的AE 信号进行了鉴别。在相同加载条件下, 完成了不同种类的U HMWPE/ HDPE 准各向同性层合板声发射检测。结果在特殊试样损伤类型与声发射信号事件振幅之间建立了对应关系, 揭示了上述各种准各向同性层合板损伤扩展过程的AE 特征与损伤破坏机制。各种准各向同性层合板试样的声发射事件累计数对拉伸应力关系曲线相异, 其相同损伤类型发生时所对应的拉伸载荷水平不等, 表明它们的铺设角度和铺设顺序对损伤演变过程有显著的影响。结果证实了它们的最终破坏由严重层间分层造成。      

Damage Mode Identification for the Clustering Analysis of AE Signals in Thermoplastic Composites

An objective analytical procedure for the investigation of damage mechanisms in the thermoplastic self-reinforced polyethylene (UHMWPE/PE) composites under quasi-static tensile load has been established, using Unsupervised Pattern Recognition (UPR) technique for the clustering task of Acoustic Emission (AE) signals. Focus is on the correlating between the obtained classes and their specific damage mechanisms. This was carried out by waveform visualization and Fast Fourier Transform analysis. Pure resin and fiber bundles were tested to collect typical waveforms of matrix cracking and fiber fracture respectively, in order to label the signal classes in the composites. The evolution process of various damage mechanisms in the composites revealed that the correlating method was effective. The AE characteristics of different damage modes found out in this study can be used as the reference for identifying unknown AE signals in the UHMWPE/PE composites. The established procedure is also potential in the investigation of failure mechanisms for composite materials with UPR technique.     

Effects of fiber orientation on the acoustic emission and fracture characteristics of composite laminates

The effects of fiber orientation on acoustic emission (AE) characteristics have been studied for various composite laminates. Reflection and transmission optical microscopy were used to investigate the damage zone of specimens. AE signals were classified through short time Fourier transform (STFT) as different types: AE signals with a high intensity and high frequency band were due to fiber fracture, while weak AE signals with a low frequency band were due to matrix cracking and/or interfacial cracking. Characteristic feature in the rate of hit-events having high amplitudes showed a procedure of fiber breakages, which expressed the characteristic fracture processes of notched fiber-reinforced plastics with different fiber orientations. As a consequence, the behavior of fracture in the continuous composite laminates could be monitored through nondestructive evaluation (NDE) using the AE technique.     

超高分子量聚乙烯(UHMWPE)纤维表面处理对UHMWPE/环氧树脂复合材料界面性能的影响机制

从工程化应用角度研究了常压空气等离子体改性对超高分子量聚乙烯（UHMWPE）纤维/环氧树脂复合材料界面性能的调节机制,主要分析了不同处理时间对UHMWPE纤维表面状态变化的影响,及其对UHMWPE/环氧树脂复合材料界面黏结性能的影响规律。采用SEM及纤维吸水测试研究了等离子体处理对UHMWPE纤维表面物理形貌及纤维表面浸润性能的影响,分别以拉伸和弯曲的方式,通过纤维表面脱黏力及层合板层间剪切强度对UHMWPE/环氧树脂复合材料的界面黏结性能进行表征。结果表明,仅经过4 s的空气等离子体处理之后,UHMWPE纤维表面脱黏力的提高幅度为84.0%,UHMWPE/环氧树脂复合材料层合板的层间剪切强度由未处理的7.01 MPa提高至15.81 MPa,增幅高达125.5%。研究发现,通过常压空气等离子体处理改变了UHMWPE纤维的表面状态,可以显著高效地调节UHMWPE/环氧树脂复合材料的界面性能,为扩大该材料的后续工程化应用提供了理论基础。      

超高分子量聚乙烯纤维/水性聚氨酯复合材料层压板抗软钢芯弹侵彻性能及其损伤机制

选用碳纳米粒子(CNPs)原位改性和未改性的超高分子量聚乙烯(UHMWPE)纤维作为增强纤维,水性聚氨酯(WPU)作为树脂基体,采用缠绕-复合-热压工艺制备单向(UD)正交结构的UHMWPE纤维/WPU复合材料层压板。基于X射线计算机断层扫描(CT)技术,研究UHMWPE纤维/WPU复合材料层压板在7.62 mm×39 mm软钢芯弹以弹速为(720±10) m/s侵彻下的弹道响应。结果表明,UHMWPE纤维的CNPs原位改性提高了CNPs-UHMWPE纤维/WPU复合材料层压板抗单发侵彻性能,但会降低其抗多发打击的能力。对于未被穿透的层压板,其被侵彻过程可分为三个阶段,依次为剪切冲塞、断裂破坏和剩余子层的塑性变形,且每个阶段的厚度比依次为11.51%、44.40%和44.09%;层压板的分层响应主要发生在第二阶段,并集中在弹着点附近;每发弹丸侵彻导致层压板的破坏区域包含在以弹着点为圆心、直径约为70 mm的圆内。      

Effect of Reactive Graphitic Nanofibers (r-GNFs) on Tensile Behavior of UHMWPE Fiber/Nano-Epoxy Bundle Composites

Ultra-high molecular weight polyethylene (UHMWPE) fibers have good mechanical and physical properties and effective radiation shielding functions, which are significant for aerospace structures. In our previous work, nano-epoxy matrices were developed based on addition of reactive graphitic nanofibers (r-GNFs) in a diluent to form a blend. It is found that improved wettability and enhanced adhesion of the matrices to UHMWPE fibers can be obtained. In this study, a series of nano-epoxy matrices with different concentrations of r-GNFs (up to 0.8 wt%) and different weight ratios of r-GNFs to a reactive diluent (1:4, 1:6, 1:7, and 1:9) were prepared. Composite bundle specimens of UHMWPE fiber/nano-epoxy were fabricated and their tensile behavior was investigated. All load-displacement curves of the UHMWPE/nano-matrix bundle composites under tensile loading showed three regions corresponding to the three deformation and failure stages of the materials: 1) elastic deformation stage, 2) plateau stage, and 3) UHMWPE fiber failure stage. The nano-epoxy with 0.3 wt% of r-GNFs and with 1:6 ratio of r-GNFs to the diluent proved to be the best matrix for UHMWPE fiber composites with enhanced tensile properties. For the resulting composite, the load level and consumed energy in the plateau stage were increased by 8% and 30% over the UHMWPE fiber/pure-epoxy specimens, respectively. This UHMWPE fiber composite with the optimized nano-epoxy matrix also possesses the highest initial stiffness and ultimate tensile strength among all the resulting UHMWPE fiber composites. These results laid a foundation for us to fabricate UHMWPE fiber reinforced composite laminates in the near future.     

Damage growth analysis of low velocity impacted composite panels

Low velocity impact loading in aircraft composite panels is a matter of concern in modern aircraft and can be caused either by maintenance accidents with tools or by in-flight impacts with debris. The consequences of impact loading in composite panels are matrix cracking, inter laminar failure and, eventually, fiber breakage for higher impact energies. Even when no visible impact damage is observed on the surface at the point of impact, matrix cracking and inter laminar failure can occur, and the carrying load of the composite laminates is considerably reduced. The greatest reduction in loading is observed in compression due to laminae buckling in the delaminated areas.

The objective of this study is to determine the limit loading capacity and the damage growth mechanisms of impacted composite laminates when subjected to compression after impact loading. For this purpose a series of impact and compression after impact tests were carried out on composite laminates made of carbon fiber reinforced epoxy resin matrix. Four stacking sequences representative of four different elastic behaviours were used. Results show that the compressive, after impact, failure stress is influenced by the stacking sequence but a relatively independent strain to failure is observed.     

Acoustic Emission as a Tool for Damage Identification and Characterization in Glass Reinforced Cross Ply Laminates

Loading of cross-ply laminates leads to the activation of distinct damage mechanisms, such as matrix cracking, delaminations between successive plies and fibre rupture at the final stage of loading. This study deals with the investigation of the failure of cross ply composites by acoustic emission (AE). Broadband AE sensors monitor the elastic waves originating from different sources of failure in coupons of this material during a tensile loading-unloading test. The cumulative number of AE activity, and other qualitative indices based on the waveforms shape, were well correlated to the sustained load and mechanical degradation as expressed by the gradual decrease of elastic modulus. AE parameters indicate the succession of failure mechanisms within the composite as the load increases. The proposed methodology based on Acoustic Emission for the identification of the damage stage of glass reinforced cross ply laminates is an initial step which may provide insight for the study of more complex laminations.     

APMOC/环氧复合材料层板破坏过程声发射特征

本文利用声发射测试技术,对APMOC/环氧复合材料各种铺层的单层板、层合板的损伤机理和破坏过程进行了详细的研究。结果表明,在不同的声发射信号参量特征与不同的损伤机理之间存在对应关系。声发射信号参量的变化过程能够描述层板的动态损伤过程,不同的声发射参量表征层板的不同损伤过程与机理。     

Detection of microfracture processes in composite laminates by thermo-acoustic emission

The damage process in composite laminates subjected to cryogenic cooling was monitored employing a thermo-acoustic emission (AE) technique. The thermo-AE signals processed with a short-time Fourier transform could be classified into three different types which were correlated with individual microfracture processes. In the initial stage of cryogenic cooling, very strong AE signals with low and high frequency bands were dominantly detected showing that large cracks accompanying fiber breakages were developed mainly. With an increase in the cooling time, weak emissions with low frequency bands became prevalent indicating the propagation of microfractures in the matrix and/or fiber-matrix interface. Similar types of AE signals, however, having weak amplitudes, were also observed for the cryogenically-treated specimens during thermal heating and cooling load cycles. Thus, analysis of thermo-AE behavior through the thermal load cycle led to the nondestructive evaluation for the cryogenic damage of composites.     

Damage sequence in thin-ply composite laminates under out-of-plane loading

The study of the damage sequence in polymer-based composite laminates during an impact event is a difficult issue. The problem can be more complex when the plies are thin. In this paper, quasi-static indentation tests were conducted on thin-ply laminates to understand qualitatively the damage mechanisms and their sequence during low-velocity impact loading. TeXtreme® plain weave plies were used with two different thicknesses, 0.08 mm and 0.16 mm (referenced as ultra-thin-ply and thin-ply, respectively), and tested under different load levels. Load–displacement curves were analyzed and the extent of damage was inspected using optical microscopy and ultrasonic technique. The results showed that the damage onset occurs earlier in thin-ply laminates. The damage onset in thin-ply laminates is matrix cracking which induces delaminations, whereas for ultra-thin-ply laminates is due to delaminations which are induced by shear forces and small amount of matrix cracking. Moreover, the fiber breakage appears earlier in ultra-thin-ply laminates.     

Time-Dependent Deformation and Damage Growth in a Rubber-Toughened Fiber Composite

Time-dependent deformation and damage growth was studied in arubber-toughened carbon fiber composite. Cyclic creep/recovery loading wasperformed on unidirectional off-axis coupons to derive the transverse andshear moduli. Constant stress-rate experiments were also performed usingmodal acoustic emission monitoring. This monitoring provides indirectevidence of what is believed to be the primary damage mechanisms in thematerial studied, matrix cracking and fiber/matrix debonding.Three significant findings from this study are emphasized in this paper.The first is the viscoelastic and viscoplastic behavior of the material withgrowing damage. Although a complete characterization has not beenperformed, emphasis is on material behavior believed to be not previouslyreported in the literature. The second is a new Damage Effect Study thatquickly identifies the material parameters in a nonlinear viscoelasticconstitutive theory that are affected by damage. This study can assist instreamlining the characterization process. Finally, a simplified materialmodel for the microstructure is developed based on AE monitoring of damagegrowth. This results in damage evolution equations based on AE data andviscoelastic fracture mechanics. The damage equations correlate AE data fordifferent loading histories. The use of direct monitoring to develop damageevolution equations and the Damage Effect Study reflect a new approach tocharacterization testing of time-dependent materials.     

A study on the failure mechanisms of carbon fiber/epoxy composite laminates using acoustic emission

The complex failure mechanisms that are commonly considered as the distinctive characteristic of composites are being amenable to nondestructive test advance. This research adopts the acoustic emission technique to study the failure mechanisms and damage evolution of carbon fiber/epoxy composite laminates. Effects of different lay-up patterns and hole sizes on the acoustic emission response are studied to set up the mapping between the failure properties and the acoustic signal features such as the energy, counting and amplitude. Moreover, the microscopic properties of different composite specimens after fracture are watched and analyzed by scanning electron microscope (SEM). Based on the mapping conception, the controlling microscopic failure mechanisms of composites including the splitting matrix cracking, fiber/matrix interface debonding, fiber pull-out and breakage as well as delamination are identified. It is expected the influence of complex lay-up patterns and sizes on the damage and failure properties of composites is represented by creating true mapping based on the acoustic emission technique.     

Influence of fabric structure and thickness on the ballistic impact behavior of Ultrahigh molecular weight polyethylene composite laminate

This paper presents the influence of fabric structure and thickness on the ballistic impact behavior of Ultrahigh molecular weight polyethylene (UHMWPE) composite laminate. UHMWPE composite laminates, reinforced by three kinds of fabric structures, unidirectional prepreg, 2D plain-woven and 3D single-ply orthogonal woven fabrics, were fabricated via hot pressing curing process. Through a series of standard ballistic tests, we demonstrated that unidirectional composite laminates exhibit higher ballistic impact velocity and absorbed energy capacity compared to others. A bi-linear relationship was found between the ballistic limit velocity and specimen thickness. Furthermore, the dominant failure mechanisms of unidirectional composite laminates were identified to be plugging and hole friction for thin laminates, whereas delamination, fiber tension and bulging for thick ones.     

弹道防护用超高分子量聚乙烯纤维增强热塑性树脂基复合材料的拉伸力学行为

以弹道防护用超高分子量聚乙烯(Ultra-high molecular weight polyethylene,UHMWPE)纤维增强热塑性树脂基复合材料作为研究对象,通过热压工艺制备单向正交结构的复合材料层压板。基于自主设计的拉伸试验装置,开展UHMWPE纤维增强热塑性树脂基复合材料在宏观尺度和准细观尺度上的面内拉伸试验,研究其面内拉伸力学性能及失效模式。研究结果显示：弹道防护用UHMWPE纤维增强热塑性树脂基复合材料在准细观尺度上的面内拉伸力学性能是其本征性能;随着偏轴角度的增加,拉伸断裂强度呈现指数型下降,这是由于失效模式由纤维的拉伸断裂破坏转变为纤维-树脂基体的界面破坏;此外,其在宏观尺度上的拉伸破坏强度比在准细观尺度上的拉伸断裂强度降低了50.52%,这是由于宏观尺度上的面内拉伸力学响应是其面内拉伸变形和层间分层破坏的耦合结果,即层压板的叠层效应。     

Damage evaluation of laminated composite material using a new acoustic emission Lamb-based and finite element techniques

In this paper, a very promising procedure is proposed to evaluate delamination using Acoustic Emission (AE) technique in composite laminates. First, a new procedure was developed to decompose the fundamental Lamb wave modes in small size specimens. The damage mechanisms in End Notched Flexure (ENF) in woven and unidirectional specimens were then discriminated using Fuzzy Clustering Method (FCM). Afterwards, the crack-arrest phenomenon was examined in each specimen. After that, experimental and Cohesive Zone Modeling (CZM) techniques were conducted to characterize the delamination using ENF specimens. The results showed how, it is possible to successfully decrease the effect of propagating media such as attenuation of AE signals using the new proposed methodology. As a final point, the results of this study could lead to efficiently distinguishing different damages in laminated composite using AE Lamb-based technique.     

Effect of fibre/matrix adhesion on residual strength of notched composite laminates

Effects of fibre/matrix adhesion and residual strength of notched polymer matrix composite laminates (PMCLs) and fibre reinforced metal laminates (FRMLs) were investigated. Two different levels of adhesion between fibre and matrix were achieved by using the same carbon fibres with or without surface treatments. After conducting short-beam shear and transverse tension tests for fibre/matrix interface characterisation, residual strength tests were performed for PMCLs and FRMLs containing a circular hole/sharp notch for the two composite systems. It was found that laminates with poor interfacial adhesion between fibre and matrix exhibit higher residual strength than those with strong fibre/matrix adhesion. Major failure mechanisms and modes in two composite systems were studied using SEM fractography. The effective crack growth model (ECGM) was also applied to simulate the residual strength and damage growth of notched composite laminates with different fibre/matrix adhesion. Predictions from the ECGM were well correlated with experimental data.     

复合材料层合板多尺度交互渐进损伤分析

纤维增强复合材料强度的准确表征是复合材料力学性能研究的核心问题之一。该文以碳纤维增强树脂基复合材料层合板为研究对象,基于宏观-细观多尺度分析方法,根据复合材料的物理失效模式分别给出了基体和纤维的细观失效准则,同时考虑基体失效对复合材料层合板纤维轴向力学性能的影响。提出了新的刚度退化方式,可准确表征复合材料层合板的损伤演化过程,开展了复合材料层合板四点弯模型的多尺度交互渐进损伤分析和试验验证。结果表明:基于多尺度方法的复合材料层合板宏-细观交互渐进损伤分析结果与试验结果吻合较好,新的刚度退化方式可以准确模拟层合板的失效过程。     

纤维增强树脂基复合材料防弹性能影响因素及破坏机制

以超高分子量聚乙烯(Ultra High Molecular Weight Polyethylene,UHMWPE)纤维、S-玻璃纤维、芳纶1414纤维和杂环芳纶纤维增强聚烯烃(Polyolefin,PO)和水性聚氨酯(Waterborne Polyurethane,WPU)树脂,采用热压工艺制备正交单向无纬(UD)结构复合材料装甲板;通过装甲板弹道极限速度测试,研究了纤维增强树脂基复合材料装甲板防弹性能的影响因素;通过体视显微镜观察装甲板侵彻破坏形貌,分析了纤维增强树脂基复合材料的破坏机制。结果表明:UHMWPE纤维增强PO树脂基复合材料的防弹性能与UHMWPE纤维的强度和模量呈正相关,但纤维模量对复合材料防弹性能的影响随着纤维模量的增大而逐渐变弱;在WPU树脂体系下,四种纤维的防弹性能由高到低依次是UHMWPE纤维、杂环芳纶纤维、芳纶1414纤维、S-玻璃纤维;纤维增强树脂基复合材料装甲板中纤维破坏方式有迎弹面纤维被剪切冲塞、中部被纤维拉伸变形后剪切、背弹面纤维被拉伸断裂,中部纤维拉伸变形是消耗子弹动能的主要方式。     

Micromechanical Modeling of Impact Damage Mechanisms in Unidirectional Composite Laminates

Composite laminates are susceptible to the transverse impact loads resulting in significant damage such as matrix cracking, fiber breakage and delamination. In this paper, a micromechanical model is developed to predict the impact damage of composite laminates based on microstructure and various failure models of laminates. The fiber and matrix are represented by the isotropic and elastic-plastic solid, and their impact failure behaviors are modeled based on shear damage model. The delaminaton failure is modeling by the interface element controlled by cohesive damage model. Impact damage mechanisms of laminate are analyzed by using the micromechanical model proposed. In addition, the effects of impact energy and laminated type on impact damage behavior of laminates are investigated. Due to the damage of the surrounding matrix near the impact point caused by the fiber deformation, the surface damage area of laminate is larger than the area of ??impact projectile. The shape of the damage area is roughly rectangle or elliptical with the major axis extending parallel to the fiber direction in the surface layer of laminate. The alternating laminated type with two fiber directions is more propitious to improve the impact resistance of laminates.