Fe－Nb－C合金的高温内耗

测量了高纯Ｆｅ－Ｎｂ－Ｃ合金的４００－８５０℃内耗，发现一个峰温度随测量应变振幅变化的高温（６６６－７４０℃）磁机械滞后阻尼内耗峰。研究了峰的特征、出现、消失条件及升降温、频率、振幅、变形与退火等因素对峰的影响．提出了用内耗实验确定材料中阻碍铁磁畴壁Ｂａｒｋｈａｕｓｅｎ跳动应力的方法和合金中产生磁机械滞后阻尼－温度峰（Ｑ_ｍ~（－１）－Ｔ）的物理机制。     

Fe－Nb－C合金的高温内耗SCIEI

测量了高纯Ｆｅ－Ｎｂ－Ｃ合金的４００－８５０℃内耗，发现一个峰温度随测量应变振幅变化的高温（６６６－７４０℃）磁机械滞后阻尼内耗峰。研究了峰的特征、出现、消失条件及升降温、频率、振幅、变形与退火等因素对峰的影响．提出了用内耗实验确定材料中阻碍铁磁畴壁Ｂａｒｋｈａｕｓｅｎ跳动应力的方法和合金中产生磁机械滞后阻尼－温度峰（Ｑ_ｍ^（－１）－Ｔ）的物理机制。     

变形Fe-Nb-C合金的室温至180℃内耗

测量了700℃，30min水冷后变形Fe－Nb-C合金室温至180℃的内耗，发现除Snoek峰外，合金在此温度区还有阻尼峰。测量了合金经过980℃，2h中间处理样品的内耗，并给出变形及室温原位时效的汽车钢ST14与GBPH340的内耗结果。认为Fe-Nb-C合金的变形“B”峰。是被饱和Cotterll气团碳原子团簇钉扎的位错段拖曳碳的稀Cottrell气团运动引起的，是合金在变形时碳原子稀Cottrell气团择优分布在位错上的结果。     

快速凝固Fe—C—Sn合金的显微组织

研究了经激光表面熔化处理的Fe-4％C-10％Sn合金的显微组织,发现在激光熔化区上部存在一种非晶相,而在其底部存在由α-Fe和一种bct相组成的显微组织,在熔化区其它区域存在含细小孪晶的马氏体。     

Fe—Mn—C合金奥氏体强化对马氏体相变的影响

测定了5种Fe-Mn-C合金的M_s温度及奥氏体在M_s温度时的屈服强度,结果表明两者成线性关系。还研究了奥氏体固溶强化对马氏体形态的影响,提出存在一个奥氏体强化特征温度T_c,当M_s>T_c时,马氏体形态主要为位错型条状马氏体,当M_s相似文献   

MnCu合金马氏体相变和马氏体的内耗

本文对含Mn60-90wt-％的MnCu合金在123—423K温度范围内进行了低频和声频内耗测量,研究马氏体相变和马氏体中各种界面对内耗的贡献.结果指出,马氏体相变内耗可分解为两部分,即相变中的稳定内耗峰(阶梯变温测量时,T=0)和低温背景内耗.相变内耗主要是由马氏体和母相界面的运动产生的;低温背景内耗是由马氏体片间界面的运动产生的,且表现出强烈的振幅效应,其强弱决定于马氏体片间界面的数量.马氏体片间界面的运动产生的非线弹应变导致了附加的模量亏损和非线性共振行为.高Mn合金(Mn>80wt-％)中的弛豫型内耗峰研究指出,该峰的弛豫时间分布参数服从β=|β_0-β_Q/k_B T|.     

铸态Mn-Cu合金的马氏体相变内耗的研究

对含Mn量为90%的铸态Mn-Cu合金的马氏体相变内耗进行了研究.用低频测量时,稳定峰(变温速率T=0)的峰温与频率无关,峰高随f的增加而减小,因而不是静滞后型内耗.连续变温的相变峰高与T,f有关,但峰高Q_m~(-1)与T,1/f或T/f都不满足线性关系;在一定振幅范围内(A_ε:1×10~(-5)—1×10~(-4)),峰高与应变振幅基本无关.因而,认为低频变温马氏体相变内耗的大小与相变中共格界面有关,即马氏体相变内耗不仅有体积效应的贡献,而且有界面效应的贡献.     

INTERNAL FRICTION AND ELASTIC CONSTANTS OF Pd-B-H ALLOYS

1.IntroductionInthePd(Hsystemthereexisttwophases:ana-phaseofl0whydrogenconcentrationandahigherconcentratedfi-phase.Ananalysisofactivitymeasurementswithintheframe-workofthequasi-chemicalappr0achsuggeststheexistenceofanattractiveinteractionofhydrogeninterstitialsviaelasticdeformation0fthePdlattice[1].Them0delpredictsthatatemperaturedependentfracti0n0fthehydrogenat0msisc1usteredintopairsorhigheror-derclustersinexcessoftherandomnumber0fpairs.Theapplicati0nofthistheoryt0theanal0gGusbinaryall0yPd-…     

INTERNAL FRICTION OF GRAIN BOUNDARIES IN Fe-P AND Fe-P-La ALLOYS CONTAINING TRACE Cu

The grain boundary internal friction(GBIF)in Fe-P and Fe-P-La alloys containing traceCu has been studied.It is found that an addition of 0.584—0.722 wt-% La obviously reducesthe IF,shifts grain boundary peaks towards higher temperatures,and produces a small addi-tional peak at even higher temperature.The mechanism of GBIF is explained as the movementof defects of atomic size,namely point defects,at gram boundaries and/or their clusters un-der stress.     

含微量Cu的Fe-P及Fe-P-La合金的晶界内耗SCIEI

本文研究了含微量Cu的Fe-P及Fe-P-La合金系的晶界内耗。发现加进0.584—0.722wt-％的La,明显降低了合金的晶界内耗峰,使晶界峰向高温移动,并在高温处产生一个小内耗峰。对结果做了讨论。进一步阐明了晶界内耗机制:晶界中原子尺寸(即点)缺陷或它们的簇,在应力作用下运动引起内耗。     

过掺杂区Y123体系的低温内耗研究

制备了部分Ca替代Y的Y1-xCaxBa2Cu3O7-δ样品，以及通过高温淬火获得了具有不同氧含量的Y0.85Ca0.15Ba2Cu3O7-δ系列陶瓷样品。用双端振动簧法研究了从室温至液氮温区的音频内耗谱。结果表明，未掺杂的YBa2Cu3O7-δ（Y123）)在220K附近有一个内耗峰(记为P3)，随着Ca含量的增加，P3峰的强度逐渐受到了抑制，而峰位稍向低温移动．对于以0．15的Ca替代Y的Y123样品，通过高温淬火减少氧含量，P3峰由抑制逐渐恢复，P3峰依赖于载流子的浓度，在过掺杂区P3峰受到抑制，这表明P3峰与高温超导欠掺杂区的异常有关，进一步的分析认为，P3峰很可能联系于欠掺杂区载流子的异常行为。     

EFFECT OF AGING ON INTERNAL FRICTION,ELASTIC MODULUS AND MECHANICAL PROPERTIES OF TERNARY Mn-Cu-Al ALLOYS

Internal friction and elastic modulus of ternary Mn-Cu-Al alloys containing 56—60wt-% Mn,0-3.59 wt-% Al were measured with acoustic frequency,1 kHz,in the tempera-ture range of-150 to 150℃.It was found that when the specimen was aged in the temperaturerange under the spinodal curve within the miscibility gap(400—500℃),the internal fric-tion increases with an increase of the aging time and reaches a maximum value at a certain ag-ing time which is shorter with a higher aging temperature.Two internal friction peaks whichdid not appear before the aging were observed above room temperature after a definite agingtime.These are respectively the martensitic tranformation peak and the relaxation peak orig-inating from the stress-induced movement of the twin boundaries.The former peak shifts to-ward higher temperatures with an increase of the aging time,whereas the relaxation peak ap-pearing at 15℃,is independent of the aging time and temperature.The activation energy as-sociated with the relaxation peak was found to be 0.56 eV which is about the same as that ofthe relaxation peak in binary alloy containing 90 wt-% Mn.It was also found that thehardness,strength and the brittleness of the specimen increase when aged below the spinodalcurve within the miscibility gap.The addition or Al enhances the strength but reduces the in-ternal friction of the specimen.A choice of suitable aging time and temperature can give anoptimum compromise of high strength and high internal friction.Analysis of experimental re-sults suggests that spinodal decomposition leads to Mn-rich zones in the specimen and thuscauses the phase transformation and the change of mechanical properties of the specimen.     

时效对Mn-Cu-Al三元合金的内耗、杨氏模量和力学性能的影响

测量了Mn-Cu-Al三元合金(含56-60wt-％Mn,0-3.59wt-％Al)在-150—150℃的声频内耗,发现当试样在调幅线的温度范围内进行时效时,内耗随着时效时间的增加而增加,并在特定的时间内达到极大值.时效温度越高,达到极大值的时间越短.在时效一定的时间后出现马氏体相变峰和孪晶界面弛豫峰.相变峰随着时效时间的增加而向高温移动;弛豫峰则出现在15℃左右(频率约1kHz),测得其激活能是0.56eV. 在调幅线内时效使合金的硬度、强度及脆性墙加,Al元素有增加合金的强度而降低其内耗的作用.实验结果表明,在450℃时效2—3h,可得到合金的内耗和强度的最佳综合指标. 根据内耗、模量、金相检验和X射线分析的结果,认为调幅分解后产生的富Mn区是合金发生相变和高内耗的来源,也是合金的强度增加和韧性降低的原因.