DSP-Based Automated Error-Reducing Flux-Linkage-Measurement Method for Switched Reluctance Motors

The switched reluctance motor (SRM) has received considerable attention from researchers for its many inherent advantages, and thus, it has become a popular research topic in the field of variable-speed drives as well as servo drives. Research on SRMs mainly includes their design, modeling and performance analysis, control, as well as applications. However, for verification of design, performance prediction, as well as development of a high-performance sensorless control algorithm, accurate measurement of the magnetic characteristics of the SRM is most critical. Hence, one of the most important problems in the field of SRMs is a practical and accurate instrumentation system for the measurement of the SRM magnetic characteristics. This paper first describes an accurate and fully automated digital method for the measurement of the magnetic characteristic of SRMs, which includes online offset-error removal and winding resistance estimation. In this method, a digital-signal-processor-based virtual instrumentation for measurement of flux linkage is developed. Then, the results of the measurement conducted on a four-phase SRM are presented. The accuracy of the measurement system is verified by comparing with that found via a magnetic analyzer. Finally, the various sources of errors and their contributions to the errors are discussed. The scheme can also be used, in general, for transformers or inductors.     

Band analysis of temperature-dependent near-infrared spectra of oleic acid in the pure liquid state by the analytic geometric approach

The applicability of the band-stripping and complementary matching method has been demonstrated by the analysis of temperature-dependent near-infrared (NIR) absorption spectra in the 7500-6500 cm(-1) region of oleic acid (cis-9-octadecenoic acid) in the pure liquid state. This method is based on first derivative-second derivative pair (D1-D2) plots and a new concept called the complementary band, cBDi, created by subtracting all the rest of the bands, exclusive of the ith estimated band, eBDi, from an experimental spectrum. The degree of coincidence of both band shapes provides a suitable measure for the quality of fit for each individual component band. It has been confirmed from the present analysis of the NIR spectra of oleic acid measured over a temperature range of 16-79 degrees C that the change of the peak intensity of the component band at around 6915 cm(-1) due to the first overtone of an O-H stretching vibration of the monomer has two transition points around 35 and 55 degrees C. Moreover, the present study has provided new insight into the analysis of temperature-dependent spectral variations of oleic acid. Among the three temperature ranges, 16-35 degrees C, 35-55 degrees C, and 55-79 degrees C, in the first range the band near 6915 cm(-1) shows a slight increase and in the second range it has a linear intensity change with a slope of 0.002 a.u./degree C. In the third range, a rapid increase of the peak intensity is observed. This band exists even at 15 degrees C (just below the melting point) and shows a shift from 6910 to 6915 cm(-1) and a band narrowing from 85 to 80 cm(-1) (full width at half-height) over a temperature range of 16 to 79 degrees C. Furthermore, it has been found that there are two broad bands at around 6835 and 6778.     

Standard reference material 2036 near-infrared reflection wavelength standard

Standard Reference Material 2036 (SRM 2036) is a certified transfer standard intended for the verification and calibration of the wavelength/wavenumber scale of near-infrared (NIR) spectrometers operating in diffuse or trans-reflectance mode. SRM 2036 Near-Infrared Wavelength/Wavenumber Reflection Standard is a combination of a rare earth oxide glass of a composition similar to that of SRM 2035 Near-Infrared Transmission Wavelength/Wavenumber Standard and SRM 2065 Ultraviolet-Visible-Near-Infrared Transmission Wavelength/Wavenumber Standard, but is in physical contact with a piece of sintered poly(tetrafluoroethylene) (PTFE). The combination of glass contacted with a nearly ideal diffusely reflecting backing provides reflection-absorption bands that range from 15% R to 40% R. SRM 2036 is certified for the 10% band fraction air wavelength centroid location, (10%)B, of seven bands spanning the spectral region from 975 nm to 1946 nm. It is also certified for the vacuum wavenumber (10%)B of the same seven bands in the spectral region from 10 300 cm(-1) to 5130 cm(-1) at 8 cm(-1) resolution. Informational values are provided for the locations of thirteen additional bands from 334 nm to 804 nm.     

Summarizing the effectiveness of supercritical fluid extraction of polycyclic aromatic hydrocarbons from natural matrix environmental samples

A summary of the supercritical fluid extraction (SFE) of polycyclic aromatic hydrocarbons (PAHs) from four natural matrix Standard Reference Materials (SRMs) is presented. The work involved the investigation of the effects of extraction fluid [carbon dioxide (CO(2)), chlorodifluoromethane (R22), and 1,1,1,2-tetrafluoroethane (HFC134a)], fluid modifier (dichloromethane and aniline), temperature (60, 150, and 200 °C) and added water on the SFE recoveries of PAHs compared to certified results from Soxhlet extractions. For SRM 1649a (Urban Dust/Organics), R22 yielded excellent recoveries (>90% of certified concentrations) of all PAHs measured, while results for the same SRM using HFC134a as the fluid were typically <80% of the certified concentrations for most of the PAHs measured. For SRM 1941a and 1944, both aquatic sediments with similar physical and chemical compositions, extractions of the wet materials with dichloromethane-modified CO(2) (10%, v/v) yielded quantitative recoveries of all PAHs for SRM 1944 but an obvious trend of lower recoveries for higher molecular weight PAHs (≥228 amu) for SRM 1941a. Results of SFEs of SRM 1650 (Diesel Particulate Matter) showed that this material is the most refractory of the SRMs investigated in this study, with recoveries of indeno[1,2,3-cd]pyrene and benzo[ghi]perylene at <20% of the Soxhlet results.     

Massic Activity Ratios of the NBS/NIST Tritiated-Water Standards Issued Between 1954 and 1999

As part of the preparation and calibration of three new National Institute of Standards and Technology (NIST) tritiated-water radioactivity Standard Reference Materials (SRMs), the massic-activity (activity of the sample divided by the mass of the sample) ratios of all of the available NBS/NIST tritiated-water SRMs issued between 1954 and 1999 were measured using liquid-scintillation (LS) counting. Four of the tritiated-water standards (SRMs 4361, 4926B, 4927C, and 4927D) were not available for measurement. All of the other tritiated-water standards (SRMs 4361B, 4361C, 4926, 4926C, 4926D, 4926E, 4927, 4927B, 4927E, and 4927F) were available, having been stored in flame-sealed glass ampoules. Where possible, massic-activity ratios measured by liquid-scintillation counting are compared with massic-activity ratios calculated from gravimetric dilution factors. The agreement is well within the stated uncertainties. For two of the tritiated-water standards that were not available for measurement (SRMs 4361 and 4926B), massic-activity ratios calculated from gravimetric dilution factors are available.     

Temperature Rise Analysis of Switched Reluctance Motors Due to Electromagnetic Losses

We present a finite-element analysis of the temperature rise of switched reluctance motors (SRM) due to electromagnetic losses. We estimate the various components of electromagnetic losses, including core loss in the lamination as well as copper and eddy-current losses in windings, and then predict the temperature rise within the motor due to these losses. We present simulation results for an 8/6 SRM and discuss various aspects of thermal design of SRMs. To validate the procedure for the estimation of electromagnetic losses, we compare predicted and measured losses.      

Determination of polycyclic aromatic hydrocarbons with molecular weight 300 and 302 in environmental-matrix standard reference materials by gas chromatography/mass spectrometry

An analytical approach based on gas chromatography/ mass spectrometry (GC/MS) is presented for the measurement of polycyclic aromatic hydrocarbons with molecular weight (MW) 300 and 302 in environmental samples. Three different GC stationary phases [5% and 50% phenyl methylpolysiloxane and dimethyl (50% liquid crystalline) polysiloxane] were compared, and retention indexes (RI) are given for 23 individual MW 302 isomers. Identification of MW 300 and 302 isomers in four environmental-matrix Standard Reference Materials (SRMs) (SRM 1597, coal tar extract; SRM 1648 and SRM 1649a, air particulate matter; and SRM 1941, marine sediment) was based on the comparison of RI data and mass spectra from authentic standards. Dibenzo[a,l]pyrene, which is of considerable interest because of its high carcinogenicity, was identified and quantified in the four environmental-matrix SRMs. A total of 23 isomers of MW 302 and four isomers of MW 300 were quantified in four different environmental-matrix SRMs, and the results are compared to previously reported results based on liquid chromatography with fluorescence detection.     

Analysis and characterization of switched reluctance motors: Part II. Flow, thermal, and vibration analyses

This paper presents new approaches for certain mechanical characterizations, such as thermal and vibration analyses, of switched reluctance motors (SRMs). The paper presents, in three parts, the modeling and simulation procedure for three-dimensional (3-D) finite-element analysis (FEA)-based flow analysis, flow-analysis-based thermal analysis, and a realistic vibration analysis. Section I documents a computational fluid dynamics (CFD) flow analysis procedure for the evaluation of the air velocity distribution inside the SRM at any speed. Section II presents a prediction method for steady-state and transient thermal characteristics of an SRM, using 3-D FEA. The convection coefficient at various heat-dissipating surfaces inside SRM, which is not a material property, but a quantity that solely depends on the air velocity at the respective surfaces, is the major parameter to be evaluated for an accurate simulation of heat distribution. The results of CFD analysis are used, for the first time on SRM, for this purpose. Windage loss calculation, one of the other applications of CFD, is introduced. Vibration in electric motors is an inevitable, at the same time undesirable, property that originates from four major sources: mechanical, magnetic, applied loads and, to a smaller extent, the associated electronic devices. Section III presents: 1) a thorough numerical study of vibration analysis in SRMs, using 3-D FEA methodology, covering all the above vibration sources except the electronics; 2) a 3-D modal analysis of SRMs including stator and rotor structures, shaft, end shields, bearings, and housing; 3) an unbalanced rotor dynamics analysis; 4) associated harmonic analysis; and 5) a stress analysis under various loading conditions. The 3-D vibration analyses presented in this paper to examine the vibration in SRM as a whole are new additions to SRM vibration analysis. Section IV concludes the paper. Future work in every section is highlighted.     

Simple model of switched-reluctance Machine based only on aligned and unaligned position data

We propose a simple equivalent circuit and mathematical model for the magnetic system of switched-reluctance machines (SRMs). The saturation effect in the stator yokes is taken into account, and phase inductance is represented as a function of phase current and reluctance in the air gap. We also propose a simple method for measurement and evaluation of the parameters of SRMs based on the model and present results of numerical simulations and real experiments on an SRM as an autonomous single-phase generator.     

Diagnosis of Static Eccentricity in Switched Reluctance Motors Based on Mutually Induced Voltages

This paper presents a novel method for diagnosis of eccentricity in a switched reluctance motor (SRM). The method employs two-dimensional finite-element analysis to calculate mutual fluxes and mutually induced voltages in an 8/6 SRM. An investigation of the effect of static eccentricity on these quantities shows that eccentricity has a considerable effect on them. Since flux measurement is costly, the method introduces mutual voltage as a suitable criterion for diagnosis of eccentricity in SRMs.      

Speciation of elements in NIST particulate matter SRMs 1648 and 1650

X-ray absorption fine structure (XAFS) spectra for S, Cl, V, Cr, Mn, Cu, Zn, As, Br, Cd and Pb and Mossbauer spectra for Fe have been obtained for two National Institute of Standards and Technology (NIST) particulate matter (PM) standard reference materials (SRMs): urban PM (SRM 1648) and diesel PM (SRM 1650). The spectral data, complemented by information on elemental concentrations from proton-induced X-ray-emission (PIXE) spectroscopy, were used to interpret the speciation of these elements in these complex materials. It appears that all the metallic elements investigated occur in oxidized forms, principally as sulfates in the diesel PM SRM and as sulfates, oxides, and possibly other forms (e.g. clays?) in the urban PM. A minor fraction of the sulfur and major fractions of the halogens, Cl and Br, occur as organosulfide (thiophene) and organohalide occurrences, respectively, that must be associated with the abundant carbonaceous matter that constitutes the major component of the two PM SRMs. Most of the sulfur, however, occurs as sulfate in the urban PM and as bisulfate in the diesel PM. In addition, elemental oxidation states have been determined directly by the spectroscopic techniques. Such information is often the key parameter in determining the toxicity and solubility of specific elements in PM, both of which are important in understanding the threat that such elements may pose to human health. For the two HAP elements, Cr and As, for which the toxicity depends greatly on oxidation state, the XAFS data showed that both elements are present in both SRMs predominantly in the less toxic oxidation states, Cr(III) and As(V). The potential of the XAFS spectra for use as source apportionment signatures is illustrated by reference to chromium, which exists in these two PM SRMs in very different forms.     

Preparation of Reference Material 8504, Transformer Oil

A new reference material (RM), RM 8504, has been prepared for use as a diluent oil with Aroclors in transformer oil Standard Reference Materials (SRMs) 3075 to 3080 and SRM 3090 when developing and validating methods for the determination of polychlorinated biphenyls (PCBs) as Aroclors in transformer oil or similar matrices. SRMs 3075-3080 and SRM 3090 consist of individual Aroclors in the same transformer oil that was used to prepare RM 8504. A unit of RM 8504 consists of one bottle containing approximately 100 mL of transformer oil. No additional constituents have been added to the oil.     

Molar mass and molar mass distribution of polystyrene particle size standards

Monodisperse polystyrene microspheres and nanospheres are often used as particle size standards for calibration of size-measuring instruments. They are potentially useful as the mass standards for particle mass spectrometry as well. We demonstrated in this work that it is possible to achieve high-precision mass determination for single polystyrene spheres using a quadrupole ion trap. We introduced the particles into the trap by laser-induced acoustic desorption and probed them with light scattering. Mass-to-charge ratios of the individual particles were determined from applied trap-driving frequencies, voltage amplitudes and the observed starlike oscillatory trajectories projected on the radial plane. Creation of one-electron differentials through charge-state changes by electron bombardment allowed determination for the absolute mass of a single trapped particle to a precision better than 0.1%. Both molar mass and molar mass distribution were deduced from a large number of measurements for NIST polystyrene particle size standards (SRMs 1690 and 1691). Our results are in excellent agreement with the size measurement for the 0.895-microm spheres (NIST SRM 1690), but a small discrepancy (4%) in number-average mass was found for the 0.269-microm spheres (NIST SRM 1691).     

Programmable selectivity for GC with series-coupled columns using pulsed heating of the second column

A series-coupled ensemble of a nonpolar dimethyl polysiloxane column and a polar trifluoropropylmethyl polysiloxane column with independent at-column heating is used to obtain pulsed heating of the second column. For mixture component bands that are separated by the first column but coelute from the column ensemble, a temperature pulse is initiated after the first of the two components has crossed the column junction point and is in the second column, while the other component is still in the first column. This accelerates the band for the first component. If the second column cools sufficiently prior to the second component band crossing the junction, the second band experiences less acceleration, and increased separation is observed for the corresponding peaks in the ensemble chromatogram. High-speed at-column heating is obtained by wrapping the fused-silica capillary column with resistance heater wire and sensor wire. Rapid heating for a temperature pulse is obtained with a short-duration linear heating ramp of 1000 degrees C/min. During a pulse, the second-column temperature increases by 20-100 degrees C in a few seconds. Using a cold gas environment, cooling to a quiescent temperature of 30 degrees C can be obtained in approximately 25 s. The effects of temperature pulse initiation time and amplitude on ensemble peak separation and resolution are described. A series of appropriately timed temperature pulses is used to separate three coeluting pairs of components in a 13-component mixture.     

Vicarious calibration of the moderate-resolution imaging spectroradiometer airborne simulator thermal-infrared channels

We made an experimental vicarious calibration of the Moderate Resolution Imaging Spectroradiometer (MODIS) Airborne Simulator (MAS) thermal infrared (TIR) channel data acquired in the field campaign near Mono Lake, Calif. on 10 March 1998 to demonstrate the advantage of using high-elevation sites in dry atmospheric conditions for vicarious calibration. With three lake-surface sites and one snow-field site, we estimated the MAS noise-equivalent temperature difference as 0.7-1.0 degrees C for bands 30-32 in the 3.68-4.13-microm region and 0.1-0.5 degrees C for bands 42, 45, 46, and 48 in the 8-13.5-microm region. This study shows that the MAS calibration error is within +/-0.4 degrees C in the split-window channels (at 11 and 12 microm) and larger in other TIR channels based on the MAS data over Mono Lake and in situ measurement data over the snow-field site.     

Measuring spatial variations of weak layer and slab properties with regard to snow slope stability

Spatial variations of weak layer and slab properties are believed to affect snow slope stability. To quantify spatial variability at the slope scale, penetration resistance was measured with a high-resolution snow micro-penetrometer (SMP) in a partly randomized grid pattern. The grid design consisted of 46 SMP measurement locations. In addition, a full snow profile and 20 compression tests as well as a Rutschblock test at the snow profile location were performed within the grid. Fifteen slopes of different aspects were sampled of which 11 could be analysed. Weak layer and slab properties were characterised using non-spatial as well as spatial statistics and results were related to slope stability. The geostatistical analysis revealed that in more than half of the cases a range could be determined. Slab layers tended to have more spatial structure than the weak layer. Though some trends are apparent, firm conclusions on the dependence of slope stability on spatial variations were not possible due to the limited range of snow conditions in the dataset, and the fact that the definition of slope stability remains elusive. Based on our limited data set, we can therefore not specify the conditions when spatial variations of weak layer and slab properties are most relevant for snow slab release.     

Temperature-dependent near-infrared spectra of bovine serum albumin in aqueous solutions: spectral analysis by principal component analysis and evolving factor analysis

Fourier transform near-infrared (FT-NIR) spectra have been measured for bovine serum albumin (BSA) in an aqueous solution (pH 6.8) with a concentration of 5.0 wt% over a temperature range of 45-85 degrees C. Not only conventional spectral analysis methods, such as second-derivative spectra and difference spectra, but also chemometrics, such as principal component analysis (PCA) and evolving factor analysis (EFA), have been employed to analyze the temperature-dependent NIR spectra in the 7500-5500 and 4900-4200 cm-1 regions of the BSA aqueous solution. Intensity changes of bands in the 7200-6600 cm-1 and 4650-4500 cm-1 regions in the difference spectra indicate variations of the hydration and secondary structure of BSA in the aqueous solution, respectively. The plot of a band intensity at 7080 cm-1 in the different spectra shows a clear turning point at 63 degrees C, revealing that a significant change in the hydration occurs at about 63 degrees C. The forward and backward eigenvalues (EVs) from EFA suggest that marked changes in the hydration and secondary structure of BSA take place in the temperature ranges of 61-65 degrees C and 59-63 degrees C, respectively. In addition, the temperature of 71 degrees C marked in the EFA plots may correspond to the onset temperature of increase in the intermolecular beta-sheet structure.     

基于响应的梁损伤识别

采用扭转弹簧模拟悬臂梁的损伤，导出了损伤梁位移模态和转角模态的近似公式，获得了损伤梁在单点激励下，零初始条件的位移和转角响应。发现损伤梁的转角响应在损伤处发生阶跃变化，而损伤梁的转角响应对位置的一阶偏导数在损伤处有脉冲两数型突变的特点，从而提出了基于损伤梁转角响应的损伤判据函数。通过对损伤梁和损伤桁架结构的数值模拟，表明提出的判据函数不仅可以利用简谐激励下的响应识别梁的损伤，电可以利用冲击激励下的响应识别桁架的损伤。实验结果表明利用所提出的判据函数，可以同时判别损伤的位置和损伤的程度。     

Development of isotope dilution cold vapor inductively coupled plasma mass spectrometry and its application to the certification of mercury in NIST standard reference materials

An isotope dilution cold vapor inductively coupled plasma mass spectrometry (ID-CV-ICPMS) method featuring gaseous introduction of mercury via tin chloride reduction has been developed and applied to the quantification and certification of mercury in various NIST standard reference materials: SRM 966 Toxic Metals in Bovine Blood (30 ng x mL(-1)); SRM 1641d Mercury in Water (1.6 microg x mL(-1)); and SRM 1946 Lake Superior Fish Tissue (436 ng x g(-1)). Complementary mercury data were generated for SRMs and NIST quality control standards using cold vapor atomic absorption spectroscopy (CVAAS). Certification results for the determination of mercury in SRM 1641d using two independent methods (ID-CV-ICPMS and CVAAS) showed a degree of agreement of 0.3% between the methods. Gaseous introduction of mercury into the ICPMS resulted in a single isotope sensitivity of 2 x 10(6) counts x s(-1)/ng x g(-1) for 201Hg and significantly reduced the memory and washout effects traditionally encountered in solution nebulization ICPMS. Figures of merit for isotope ratio accuracy and precision were evaluated at dwell times of 10, 20, 40, 80, and 160 ms using SRM 3133 Mercury Spectrometric Solution. The optimum dwell time of 80 ms yielded a measured 201Hg/202Hg isotope ratio within 0.13% of the theoretical natural value and a measurement precision of 0.34%, on the basis of three replicate injections of SRM 3133.     

Characterization of polyacrylate membrane-coated fibers used in chemical absorption studies with programmed thermal treatment and FT-IR microscopy

A polyacrylate (PA) film was coated onto a fused-silica fiber as a permeation membrane in a membrane-coated fiber (MCF) technique and a solid-phase microextraction technique. The molecular changes of the PA membrane after different temperature treatments were studied with FT-IR microscopy. The absorption bands of the PA aliphatic backbone at 2902, 2795, and 2740 cm(-)(1) remained unchanged over the elevated thermal treatments, indicating that the polymer backbone was stable over these conditions. The spectra of the PA membrane remained unchanged when the thermal treatment temperature was under 150 degrees C. When the temperature was 250 degrees C, the O-H stretching band in the -COOH groups of the poly(acrylic acid) at 3315 cm(-)(1) was significantly reduced. When the temperature was higher than 280 degrees C, this O-H band disappeared. These evidences suggested that the PA membrane underwent dehydroxyl reaction to form an anhydride when the thermal treatments were higher than 250 degrees C. Thermal treatments of a deuterated PA MCF confirmed the anhydride formation mechanism. The anhydride formation explained the absorption property of PA MCFs in GC applications where they must be preconditioned at 300 degrees C. The absorption data suggest that a PA fiber does not preferably absorb polar compounds (with permanent dipole moment); instead, it absorbs preferably aromatic compounds.