共查询到20条相似文献,搜索用时 171 毫秒
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在乌涤托品硝解制备RDX的工艺基础上,研究结晶过程的几种因素对产品酸度的影响。通过控制析晶点来控制结晶过程的各个因素,可降低大粒度产品的酸度,从而制备出符合美军标的RDX产品。 相似文献
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阐明了通过重结晶法制备5级RDX中试工艺的研究过程,讨论了影响产品质量的因素,确定了适宜的工艺条件。 相似文献
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通过对不同堆密度的RDX的分布图形进行分析,阐述了RDX堆积密度和粒度之产是的相关关系。动用数量统计原理和结晶原理说明RDX的粒度分布是一个态分布和一个F分布构成的联合分布曲线。并对不同堆积密度的RDX进行了粒度的均值和标准差分析。 相似文献
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阐述了TNT、40TNT/60RDX及钝化RDX成型装药(药片)在非密闭条件下受撞击作用时感度的试验研究。计算了50%爆炸概率和小爆炸概率时的撞击比能。同时与文献[1]的数据进行了对比。 相似文献
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阐述了TNT、40TNT/60RDX及钝化RDX成型装药(药片)在非密闭条件下受撞击作用时感度的试验研究。计算了50%爆炸概率和小爆炸概率时的撞击比能。同时与文献[1]的数据进行了对比 相似文献
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铁尾矿黑色玻璃材料的研制 总被引:6,自引:2,他引:4
研究了铁尾矿和工业废渣为主要原料制备黑色玻璃的工艺,采用DTA,SEM,XRD对玻璃的分相、稳定性进行了分析,并对其主要物化性能进行测试。 相似文献
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羟基磷灰石陶瓷成型与烧结工艺研究 总被引:3,自引:0,他引:3
以磷酸钙为原料用煅烧新工艺制备了羟基灰石粉末,并以此为原料采用凝胶浇注成工艺制备了羟基磷灰石陶瓷坯体,研究了不同成型工艺制备的羟基磷灰石陶瓷坯体的性能。借助DTA、XRD等分析了陶瓷坯体在烧结过程中的物理化学和晶相转变。 相似文献
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为了获得粒径分布均匀的细化RDX,在超重力反应器中,以丙酮-水作为溶剂-反溶剂重结晶体系,添加聚乙烯吡咯烷酮(PVP)作为表面活性剂,制备了亚微米级RDX。研究了RDX溶液浓度、PVP含量以及超重力反应器转速对RDX形貌和尺寸的影响,获得最优工艺条件,利用SEM、XRD和FT-IR对其形貌、晶体结构和分子结构进行了表征,并采用DSC研究了RDX的热分解过程。结果表明,在RDX溶液浓度为0.04g/mL、PVP浓度为0.2g/L、超重力反应器转速为1500r/min时,制备了平均粒径为0.54μm的亚微米级RDX,细化处理未改变RDX的晶型;与原料RDX相比,亚微米级RDX的分解峰温提前了1.2℃,热分解活化能从180~250kJ/mol降至约150kJ/mol。 相似文献
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为研究高品质RDX在2,4-二硝基苯甲醚(DNAN)中的溶解及反复熔融特性,采用高效液相色谱法研究了高品质RDX在DNAN中的溶解度及影响因素;通过工艺试验研究了DNAN/高品质RDX熔铸炸药在反复熔融后的不可逆增稠特性;运用热台显微装置研究了高品质RDX在DNAN中的溶解及析出过程,并与普通RDX(3类)进行了对比。结果表明,随着高品质RDX粒度的增大,其在DNAN中的溶解度逐渐减小,呈近似线性关系;高品质RDX在DNAN中的溶解度随温度升高而增大,115℃时高品质RDX(d50=470μm)在DNAN中的最大溶解度达到8.87g/100g,在不同温度下溶解度均小于普通RDX;DNAN/高品质RDX配方在反复熔融后的不可逆增稠程度小于DNAN/普通RDX配方;高品质RDX在DNAN中的溶解首先从晶粒的不规则外沿和晶体凹陷区域开始,溶解速率受颗粒尺寸及不规则程度影响,且明显慢于普通RDX;析出存在两种方式且析出后形状呈不规则变化。 相似文献
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Yanhua Lan Jinxian Zhai Dinghua Li Rongjie Yang 《Propellants, Explosives, Pyrotechnics》2014,39(1):18-23
The influence of dimethyl hydantoin (DMH) on the mechanical properties of GAP/RDX propellant was studied by molecular dynamics (MD) and dissipative particle dynamics (DPD) simulation. The results showed that the binding energies (Ebinding) between GAP and different surfaces of RDX were in the order of (010)>(001)>(100). Compared to GAP/RDX, GAP grafted with DMH (GAP‐DMH) exhibits higher binding energies with RDX, and the sequence of Ebinding turns to (001)>(010)>(100). Radial distribution simulations demonstrated that GAP‐DMH is more close to the surfaces of RDX, increasing the van der Waals energies between GAP‐DMH and RDX. The stress and strain of GAP‐DMH/RDX excel those of GAP/RDX. DPD simulations showed that GAP‐DMH was able to restrain the agglomeration of RDX, to improve the dispersibility and to enlarge the contact surface with RDX, which also increased the mechanical properties of GAP/RDX propellant. 相似文献
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根据溶剂对 RDX热分解行为的不同影响可将溶剂分为活性和惰性两类。活性溶剂加速 RDX热分解 ,惰性溶剂对 RDX热分解速率无影响或因其粘度较大而降低了热分解速率。本文用布氏压力法研究了 RDX在惰性溶剂中热分解机理 ,补充了许多二级反应 ,借助这些二级反应用初始步断裂 N- NO2 键机理较好地解释了溶剂粘度对 RDX热分解速率的影响和 RDX在苯中浓度对放气量及反应中间产物亚硝基黑索今得率的影响。所提出的机理丰富、完善、发展了二元硝胺炸药热分解理论 相似文献
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Christian Spyckerelle Genevive Eck Per Sjberg Anna‐Maria Amnus 《Propellants, Explosives, Pyrotechnics》2008,33(1):14-19
In recent years much interest has been generated in a quality of reduced sensitivity RDX (RS‐RDX), like I‐RDX® which, when incorporated in cast cure and even pressable plastic bonded explosives (PBX compositions), can confer reduced shock sensitivity as measured through gap test. At crystal level, lot of work has been done to try to determine which property or properties may explain the behaviour of the corresponding cast PBX composition. But up to now, and despite an international inter‐laboratory comparison (Round Robin) of seven lots of RDX from five different manufacturers conducted from 2003 to 2005, even if some techniques lead to interesting results, there is no dedicated specification to apply to RS‐RDX. This quality (I‐RDX®) has proved to retain its low sensitivity even after ageing, which does not seem to be the case for standard RDX produced by the Bachmann process (when re‐crystallized under I‐RDX conditions in order to obtain RS‐RDX). It has been shown that the higher sensitivity of RDX produced by the Bachmann process, or the evolution of sensitivity after ageing of RS‐RDX produced from Bachmann RDX may be linked to the presence of octogen (HMX) during the crystallization process. In order to check such hypothesis, low HMX content RDX produced by the Bachmann process has been prepared and evaluated in cast PBX composition (PBX N 109). Results of the characterization of such quality of RDX and its evaluation in cast PBX composition as well as ageing behaviour are presented and discussed; there are indications that removal of HMX from Bachmann RDX may lead to RS‐RDX, which retains its RS character even after ageing. 相似文献
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为改善RDX的安全性能和力学性能,采用乳液聚合法制备RDX/聚甲基丙烯酸甲酯/氧化石墨烯(RDX/PMMA/GO)微球,并用相同方法制备了RDX/PMMA复合粒子进行对比;通过扫描电子显微镜(SEM)、X射线衍射仪(XRD)、傅里叶变换红外光谱仪(FT-IR)和差示扫描热量仪(DSC)对样品进行表征,并测试其撞击感度和药柱的静态力学性能。结果表明,包覆后RDX/PMMA微球形貌趋于球形,RDX/PMMA/GO粒子存在明显的层状皱褶;RDX晶型均未发生改变;与原料RDX和RDX/PMMA相比,RDX/PMMA/GO微球的表观活化能分别提高22.16kJ/mol和15.17kJ/mol,升温速率趋近于0时的峰温和热爆炸临界温度与原料RDX相比分别提升6.45℃和6.23℃;特性落高由包覆前的26.74cm分别提至62.95cm和78.52cm,撞击感度明显降低。RDX/PMMA/GO抗压强度比RDX/PMMA增加了7.5MPa,表明GO的加入对复合材料的力学性能提升明显。 相似文献
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RDX降感技术研究进展 总被引:1,自引:0,他引:1
RDX(黑索今)的较高感度使其应用受到一定限制。从RDX的高品质化和RDX钝感包覆两方面对近年来RDX降低感度研究方面的成果进行了评述,指出了我国今后RDX降低感度的研究方向。 相似文献