铺层方式对CFRP-铝合金单搭接胶接接头低速冲击损伤及剩余拉伸性能的影响

采用热压罐成型方法制备铺层方式为[+45/-45]_4s、[0/+45/-45/90]_2s和[0/90]_4s的碳纤维复合材料层合板,通过胶黏剂与铝合金板进行粘接获得异质材料单搭接胶接接头。利用落锤冲击试验机和万能电子试验机分别对三种接头进行低速冲击与冲击后静态拉伸测试,获得接头接触力-时间曲线和拉伸强度。通过CT扫描技术和数字图像相关(DIC)方法表征接头冲击损伤模式及表面应变演化过程,研究了铺层方式对接头抗冲击性能、冲击损伤模式以及剩余拉伸性能的影响。结果表明,复合材料铺层方式为[+45/-45]_4s时,接头在冲击载荷作用下具有较高的抗冲击性能,但胶层界面脱粘损伤较为严重。与胶层界面脱粘相比,接头剩余强度对层合板分层损伤更为敏感。相较于[+45/-45]_4s,[0/+45/-45/90]_2s和[0/90]_4s铺层方式接头的胶层界面脱粘范围与冲击后失效载荷退化程度较小,同时接头冲击后拉伸载荷主要集中于临近胶层的0°铺层且失效模式较为复杂...     

z-pin增韧复合材料层合板低速冲击损伤过程研究

从z-pin增韧复合材料层合板低速冲击实验出发,考虑了复合材料层合板在受低速冲击时的分层及基体开裂等四种损伤形式,引入适当的损伤判据,对T300/3234碳纤维树脂基复合材料层合板的低速冲击损伤过程进行有限元模拟。结果表明,采用碳纤维钉z-pin增韧使得冲击后层间分层区域面积减小50%左右,有限元结果与实验数据吻合。     

层间颗粒增韧复合材料层压板的损伤阻抗特性

采用热塑性颗粒对HT7/ 5228 、HT3/ N Y9200G和HT3/ 5224 三种高温固化环氧基体复合材料层压板进行层间增韧。为了提高冲击后压缩强度(CAI) 和考察损伤阻抗, 测试了平均分层起始能量e_Ⅱc以及接触力-凹坑深度关系。试验结果表明, 增韧颗粒和基体树脂形成的层间区域能有效地吸收断裂能量并抑制分层的发生, e_Ⅱc显著提高。在静压痕力下, 层间增韧复合材料层压板具有较深的凹坑深度和较小的损伤面积。层间增韧的几何效应、裂纹传播路径控制、颗粒桥联以及裂尖屏蔽是主要的增韧机理, 颗粒的塑性变形和最终失效也耗散了大量断裂能量。      

碳纤维增强聚酰亚胺树脂基复合材料MT300/KH420高温力学性能(I)——拉伸和层间剪切性能

研究了碳纤维增强聚酰亚胺树脂基复合材料MT300/KH420的高温力学性能, 重点揭示了MT300/KH420的[0°]₇、[0°]₁₄ 和[±45°/0°/90°/+45°/0°₂]_s层合板在常温~500 ℃的拉伸和层间剪切性能的变化规律。结果表明:在350 ℃以内,[0°]₇层合板拉伸强度随温度升高有所提高, 拉伸模量几乎不变, 在420 ℃时拉伸强度和模量均出现明显下降, 在500 ℃时分别保持在65%和83%以上, 表现出优异的高温拉伸性能。MT300/KH420的[0°]₁₄层合板层间剪切强度在常温~420 ℃随温度升高不断降低至52.8%, 在高温下呈现出黏弹效应, 且在420 ℃时最为明显。相比于单向层合板, [±45°/0°/90°/+45°/0°₂]_s多向层合板高温力学性能较为稳定, 且由纤维控制的纵向试件力学性能受温度影响较小。      

基于应变能耗散的复合材料层合板面内缺口强度分析CDM模型

基于伴随能量释放的渐进损伤演化思想,建立了复合材料层合板面内失效分析的连续介质损伤力学（CDM）分析模型,该模型包含损伤表征、损伤起始判定和损伤演化法则3个方面。基于CDM模型,通过引入损伤状态变量表征损伤,建立了平面应力状态下的材料损伤本构模型。采用损伤参量 f_E改写Hashin准则,以判定损伤的起始。损伤演化由特征长度内的应变能释放密度控制,建立了损伤状态变量关于等效应变的渐进损伤演化法则。模型中还同时考虑了面内剪切非线性和网格敏感性,并进行了对比分析。对含缺口的[90/0/±45]_3s和[（±θ）₄]_s 2类典型复合材料层合板的面内拉伸失效进行了分析,结果表明,本文中的模型能有效预测复合材料层合板的面内拉伸强度。     

T300/QY8911层合板低速冲击试验及有限元模拟

对T300/QY8911复合材料层合板进行了低速冲击试验研究及数值仿真模拟。通过自由落体装置对层板进行冲击,并使用超声C扫描技术检测了层板冲击后的损伤状态,获得了不同能量下层板内部的损伤面积。建立了用于预测复合材料层合板在低速冲击作用下损伤演化的3D有限元模型,模型包含了用于模拟分层损伤的界面元和用于模拟纤维断裂、纤维挤压、基体开裂、基体挤裂等面内损伤形式的3D实体单元。该模型考虑了面内基体损伤对层间强度的影响。本文中的数值仿真结果和试验结果的对比验证了模型的合理性和有效性,文中还分析了影响低速冲击后层板内部分层面积的主要因素。     

典型螺栓连接CFRP薄壁C型柱轴压失效行为:试验及数值模拟

为了研究典型螺栓连接碳纤维增强树脂复合材料(CFRP)薄壁C型柱的轴压失效模式及吸能特性,进行了5组不同铺层方式C型柱的准静态轴压试验,即[0/90]_4s、[±45]_4s、[±45/90₂/0₄]_s、[±45/90/0₂/90/0₂]_s、[90/±45/0]_2s,获得其失效形貌及载荷-位移曲线。采用Lavadèze单层壳单元模型、Puck-Yamada失效准则、层间胶粘单元及螺栓模型,建立C型柱层合壳模型进行轴压仿真,并与试验失效形貌、载荷-位移曲线及吸能特性评估指标进行对比分析。结果表明:0°、±45°、90°纤维可以显著影响C型柱轴压失效模式及吸能特性。在轴压载荷下,±45°纤维铺设C型柱发生局部屈曲失效模式,吸能特性差。±45°纤维铺设在外部,0°和90°纤维交替铺设在内部的C型柱,其轴压失效过程平稳,吸能特性好。与C型柱轴压试验结果相比,层合壳模型获得的整体变形和局部失效形貌吻合较好,载荷-位移曲线变化趋势和吸能特性评价指标基本一致。研究结果对CFRP薄壁C型柱吸能设计具有一定的指导意义。      

飞机用复合材料斜胶接修补结构的冲击损伤

高传力效率的斜面式胶接在飞机复合材料传力接头和修补中被广泛使用,但该结构的低速冲击损伤阻抗和损伤容限未在飞机结构设计中考虑。本文研究了低速冲击下的较厚的复合材料斜胶接板的力学性能及损伤失效。在胶接区域布置不同冲击点,寻找最敏感位置,在该位置进行冲击能量变化研究,通过冲击响应（冲击载荷、挠度、能量等）及冲击损伤两个方面获取其规律和失效机制。小能量和大能量冲击结果表明,胶接区域5个典型冲击位置中,中心位置冲击损伤最大,冲击敏感性最高,因此中心点为冲击损伤阻抗最小位置。中心点不同能量冲击时,冲击响应研究揭示了冲击过程中冲击载荷具有典型的4阶段行为。冲击载荷还具有双峰值力的现象。冲击后沿试样中心线切开的显微损伤图揭示了该结构有两种损伤模式,包括复合材料损伤及胶层损伤。复合材料的损伤包含90°和45°层基体的开裂和0°与90°层之间的层间损伤。胶层损伤出现在试样冲击点正下方背部的复合材料斜接尖端部位。进一步通过考虑复合材料层内、层间损伤及胶层损伤的渐进损伤模型对试验进行仿真研究,找出导致第Ⅱ阶段冲击载荷突降的主要原因为复合材料层间损伤,第Ⅳ阶段冲击载荷再一次突降是由于胶层出现了损伤。     

铺层顺序对复合材料薄壁圆管轴向压溃吸能特性的影响研究

采用仿真和试验相结合的方法探讨复合材料薄壁圆管在准静态轴向压缩载荷下的失效吸能特性和吸能机理。首先,建立复合材料薄壁圆管"层合壳"有限元模型,通过显式动力学方法求解其在准静态轴向载荷下的压溃失效力学行为。仿真与试验结果在圆管轴向压溃变形过程、初始峰值载荷、平均压溃载荷及比吸能等主要吸能参数上具有很好的一致性,验证了"层合壳"复合材料圆管有限元模型和建模方法的有效性。其次,采用解析模型与仿真分析方法分别对[0/90]_3s、[0/90/0₂/90₂]_s、[0₃/90₃]_s三种不同铺层顺序的复合材料圆管的屈曲载荷与吸能特性进行了对比,进一步分析了铺层顺序对圆管失效吸能特性的影响。研究表明,0°与90°铺层交替程度对复合材料圆管的吸能特性影响较大,保证纤维失效方式在结构宏观失效中占主导地位能够提高材料失效吸收能量。     

微胶囊Mg (OH)2的合成及其对乙烯-乙酸乙烯酯共聚物的阻燃作用

用原位聚合方法合成了以微米Mg（OH）₂粒子为芯材、交联聚脲为壁材的微胶囊Mg（OH）₂（M-Mg（OH）₂）阻燃剂,并把M-Mg（OH）₂加入到乙烯-乙酸乙烯酯共聚物（EVA）中,研究了M-Mg（OH）₂对EVA的阻燃作用。采用FTIR、SEM、热分析和酸滴定方法研究了M-Mg（OH）₂的性质,用极限氧指数（LOI）和垂直燃烧方法（UL-94）研究了M-Mg（OH）₂/EVA复合材料的阻燃性能以及酸腐蚀对M-Mg（OH）₂/EVA复合材料阻燃性能的影响。结果表明,采用原位聚合方法能够成功地在Mg（OH）₂粒子表面包覆交联聚脲壁材,得到M-Mg（OH）₂。与纯Mg（OH）₂相比,M-Mg（OH）₂的颗粒尺寸增大,热稳定性增加,在水中溶解度显著降低,在EVA基体中分散更加均匀。阻燃剂用量相同时,M-Mg（OH）₂/EVA复合材料的LOI总是比Mg（OH）₂/EVA复合材料的数值稍大。阻燃剂与EVA质量比小于135∶100时,两种复合材料的垂直燃烧级别均为V-2级,阻燃剂与EVA质量比在135∶100~150∶100之间时,前者的燃烧级别为V-0级,而后者只能达到V-2级,阻燃剂与EVA质量比超过150∶100时,两种复合材料都能达到V-0级。M-Mg（OH）₂/EVA复合材料的耐酸性比Mg（OH）₂/EVA大幅度提高,可以在酸性环境中使用。     

The effect of stacking sequence on impact damage in a carbon fibre/epoxy composite

The effect of stacking sequence on impact damage in a carbon fibre/toughened epoxy composite was studied. The major form of damage was delamination, which initiated at almost every interface through the panel. During the impact event the force-time response was monitored and the energy absorbed analysed in terms of an initiation and a propagation energy. The energy absorbed in delamination initiation was influenced by the stacking sequence, being increased by placing 45° fibres in the surface plies and by increasing the number of dissimilar interfaces. The residual energy absorbed in delamination propagation was found to increase linearly with increasing total delamination area. The compression-after-impact strength was related to the maximum delamination area.     

复合材料层合板低速冲击逐渐累积损伤预测方法

针对复合材料层板在冲击载荷下,各种损伤的产生和扩展是一个随载荷、时间和空间而演变的过程,发展了复合材料层合板低速冲击逐渐累积损伤预测方法.采用刚度退化技术和改进的Chang-Chang失效准则、显式有限元法来模拟复合材料层合板受到低速冲击下逐渐损伤过程.使用所发展的方法分析了[0m/90n/0m]铺层的复合材料层合板在低速冲击过程中的逐渐损伤扩展,结果表明本文的方法能较好地模拟复合材料层板在低速冲击下的损伤扩展及变形过程,计算结果与实验结果吻合较好;对不同冲击能量下层合板损伤扩展研究表明,冲击能量与分层损伤面积成线性关系.     

冲击作用下斜接修补CFRP层间分层和胶层的损伤机制及参数分析

首先,针对斜接修补CFRP抗冲击性能差的问题,分别使用基于接触的内聚力模型（SCZM）和基于单元的内聚力模型（ECZM）描述层间分层和斜接胶层破坏,研究CFRP层板的冲击响应和两种失效的演化规律。然后,分析了冲击能量、斜接角度和预拉伸作用对两种失效的影响。结果表明：层间分层起始时间早于胶层破坏,与冲击能量无关;分层和胶层破坏面积随冲击能量增加而增大,胶层破坏面积增加的更明显;斜接角度主要影响胶层破坏,对分层面积几乎无影响;预拉伸作用对两种失效均具有负面作用。最后,进一步讨论分层对胶层破坏的影响,通过与只考虑胶层破坏的情况进行对比,发现层间分层使胶层破坏的面积降低,延缓了胶层的最终失效。     

Damage resistance of single lap adhesive composite joints by transverse ice impact

This paper focuses specifically on the high velocity transverse impact of composite joints by hailstones. Impact tests with ice spheres onto composite lap joint specimens were conducted to determine the failure threshold energy describing damage initiation, and to investigate the modes of damage. The damage areas imaged by ultrasonic scanning were quantitatively measured and the specimens were also sectioned and observed with optical microscopy to determine the exact location of damage. The damage area versus impact kinetic energy was found to increase dramatically for impacts beyond the failure threshold. Delamination of the composite originated at the bond overlap termination facing away from the impact side. The damage usually occurred at specific ply locations and a transition of the delamination to other ply locations was also observed. Numerical simulation of the impact was conducted and the results show that the plies where delaminations were observed to occur have the highest peel and shear stresses.     

Effect of stitch density and stitch thread thickness on compression after impact strength and response of stitched composites

In this paper, the damage failure and behaviour of stitched composites under compression after impact (CAI) loading are experimentally investigated. This study focuses on the effect of stitch density and stitch thread thickness on the CAI strength and response of laminated composites reinforced by through-thickness stitching. Experimental findings show that stitched composites have higher CAI failure load and displacement, which corresponds to higher energy absorption during CAI damage, mainly attributed to greater energy consumption by stitch fibre rupture. The coupling relationships between CAI strength, impact energy, stitch density and stitch thread thickness are also revealed. It is understood that the effectiveness of stitching has high dependency on the applied impact energy. At low impact energy range, CAI strength is found to be solely dependent on stitch density, showing no influence of stitch thread thickness. It is however observed that stitch fibre bridging is rendered ineffective in moderately stitched laminates during compressive failure, as local buckling occurs between stitch threads, resulting in unstitched and moderately stitched laminates have similar CAI strength. The CAI strength of densely stitched laminates is much higher due to effective stitch fibre bridging and numerous stitch thread breakages. At high impact energy level, CAI strength is discovered to be intimately related to both stitch density and stitch thread thickness. Since CAI failure initiates from impact-induced delamination area, stitch fibre bridging is considerable for all specimens due to the relatively large delamination area present. Stitch threads effectively bridge the delaminated area, inhibit local buckling and suppress delamination propagation, thus leading to increased CAI strength for laminates stitched with higher stitch density and larger stitch thread thickness. Fracture mechanisms and crack bridging phenomenon, elucidated by X-ray radiography are also presented and discussed. This study reveals novel understanding on the effectiveness of stitch parameters for improving impact tolerance of stitched composites.     

碳纤维增强树脂基复合材料层合板的损伤阻抗表征

通过落锤冲击试验与准静态压痕试验研究了碳纤维增强树脂基复合材料层合板的损伤阻抗,发现两种试验中,复合材料层合板都具有三个损伤阶段。两种试验都具有两个表征损伤阶段变化的拐点:第一个拐点为分层拐点,表征分层起始;第二个拐点为损伤拐点,表征分层扩展趋于饱和。本文建议利用一个三维坐标点(x,y,z,其中x为第二拐点对应的冲击能量,y为相应的凹坑深度,z为分层投影面积)表示的损伤拐点来衡量材料抵抗冲击的能力,此损伤拐点不仅仅代表了材料抵抗冲击的关键点,也揭示了此时的内部损伤状态。     

The influence of hygrothermal conditions on the damage processes in quasi-isotropic carbon/epoxy laminates

The effects of hygrothermal conditions on damage development in quasi-isotropic carbon-fiber/epoxy laminates are described. First, monotonic and loading/unloading tensile tests were conducted on dry and wet specimens at ambient and high temperatures to compare the stress/strain response and damage development. The changes in the Young's modulus and Poisson's ratio were obtained experimentally from the monotonic tensile tests. The critical stresses for transverse cracking and delamination for the above three conditions are compared. The delamination area is measured by using scanning acoustic microscopy (SAM) at various loads to discuss the effects of delamination on the nonlinear stress/strain behavior. Next, the stress distributions under tensile load including hygrothermal residual stresses are computed by a finite-element code and their effects on damage initiation are discussed. Finally, a simple model for the prediction of the Young's modulus of a delaminated specimen is proposed. It is found that moisture increases the critical stresses for transverse cracking and delamination by reducing the residual stresses while high temperature decreases the critical stresses in spite of relaxation of the residual stresses. The results of the finite-element analysis provide some explanations for the onset of transverse cracking and delamination. The Young's modulus predicted by the present model agrees with experimental results better than that predicted by conventional models.     

低速冲击下复合材料层合板损伤分析

根据低速冲击下复合材料层合板的分层损伤机理,发展了一种分层失效准则,该准则同时考虑了层间拉应力、层间剪应力和基体开裂等因素对分层损伤的影响,并在损伤分析中,区分了冲击正面由挤压应力引起的纤维挤压损伤和冲击背面由弯曲拉应力引起的纤维断裂损伤,模拟了纤维断裂、纤维挤压、基体开裂、基体挤压、分层等五种损伤的起始和扩展过程,完善了作者以前发展了低速冲击逐渐累积损伤模型.通过与实验结果进行比较,验证了模型的合理性.     

Effect of damage levels and curing stresses on delamination growth behaviour emanating from circular holes in laminated FRP composites

This paper deals with the study of the effect of drilling induced delamination damage levels and residual thermal stresses (developed during manufacturing process of cooling the laminate form curing temperature to room temperature) on delamination growth behaviour emanating form circular holes in graphite/epoxy laminated FRP composites. Two sets of full three dimensional finite element analyses (one with the residual thermal stresses developed while curing the laminate and the other without residual thermal stresses i.e. with mechanical loading only) have been performed to calculate the displacements and interlaminar stresses along the delaminated interfaces responsible for the delamination onset and propagation. Modified crack closure integral (MCCI) techniques based on the concepts of linear elastic fracture mechanics (LEFM) have been used to calculate the distribution of individual modes of strain energy release rates (SERR) to investigate the interlaminar delamination initiation and propagation characteristics. Asymmetric variations of SERR obtained along the delamination front are caused by the overlapping stress fields due to the coupling effect of thermal and mechanical loadings. It is found that parameters such as ply orientation, drilling induced damage levels and material heterogeneity at the delaminated interface dictate the interlaminar fracture behaviour of laminated FRP composites.     

层间颗粒增韧HT3/QY8911的损伤阻抗和损伤容限

采用热塑性颗粒对双马基体复合材料层合板HT3/ Q Y8911 进行层间增韧, 制备未加入增韧颗粒的对比件和加入增韧颗粒的改性件。通过准静态压痕(QSI) 实验和冲击后压缩实验, 研究了层间增韧后HT3/ Q Y8911的损伤阻抗和损伤容限特性。结果和分析表明, 改性件在静压痕力下具有较高的分层起始载荷, 或在相同载荷水平下具有较小的损伤面积。提出从分层起始点载荷大小和载荷下降程度两方面来衡量试件对准静压痕力的响应。在相同的静压痕力或单位厚度冲击能量下, 层间增韧后的HT3/ Q Y8911 具有较深的凹坑, 表明塑性变形较大的层间区域以凹坑为代价换取了较小的损伤面积, 具有较高的损伤阻抗。在冲击后压缩面积相差不大的情况下, 层间增韧件的冲击后压缩强度和压缩破坏应变显著增加。