Experimental and parametric study on drying of green peas in spouted bed

Drying of Green Peas (Pisum sativum) was studied experimentally in a lab‐scale spouted bed. Experiments were carried out at different operating conditions, and the effect of inlet air temperature and its flow rate, bed height (initial mass of wet particles) and average diameter of particles were examined on performance of dryer and rate of drying. The obtained experimental results were fitted by an exponential form equation to model the drying kinetic behaviour of green peas in a spouted bed. The fitting parameters are presented in the form of mathematical correlations as a function of operating parameters. As expected, it was found that by increasing inlet air temperature and air‐flow rate, the rate of drying increases, but by increasing the bed height and diameter of particles, the rate of drying decreases. The results can help the design engineers to choose the optimum drying conditions for industrial applications.     

Effects of process parameters on quality changes of shrimp during drying in a jet-spouted bed dryer

ABSTRACT:  The objective of the present study was to investigate the effects of various parameters, that is, concentration of salt solution (2%, 3%, 4%[w/v]), boiling time (3, 5, 7 min), drying air temperature (80, 100, 120 °C), and size of shrimp, on the kinetics of drying and various quality attributes of shrimp, namely, shrinkage, rehydration ability, texture, colors, and microstructure, during drying in a jet-spouted bed dryer. In addition, the effects of these processing parameters on the sensory attributes of dried shrimp were also investigated. Small shrimp (350 to 360 shrimp/kg) and large shrimp (150 to 160 shrimp/kg) were boiled and then dried until their moisture content was around 25% (d.b.). It was found that the degree of color changes, toughness, and shrinkage of shrimp increased while the rehydration ability decreased with an increase in the concentration of salt solution and boiling time. Size of shrimp and drying temperature significantly affected all quality attributes of dried shrimp. The conditions that gave the highest hedonic scores of sensory evaluation for small dried shrimp are the concentration of salt solution of 2% (w/v), boiling time of 7 min, and drying air temperature of 120 °C. On the other hand, the conditions that gave the highest hedonic scores of sensory evaluation for large dried shrimp are the concentration of salt solution of 4% (w/v), boiling time of 7 min, and drying air temperature of 100 °C. The quality attributes of dried shrimp measured by instruments correlated well with the sensory attributes, especially the color of dried shrimp.     

Image analysis and quality attributes of malting barley grain dried with infrared radiation and in a spouted bed

The impact of drying two spring barley cultivars (Mauritia and Prestige) in a spouted‐bed and in infrared radiation (IR) dryers on grain dimensions, colour, pigment content, vitality and malt quality was investigated. The results indicate that the investigated drying methods led to kernel dimension changes. Kernel shrinkage was typical of spouted bed drying, while kernel expansion was observed after IR drying at the intensity of 900 W m^?2. An increase in the intensity of yellowness (b*) on the surface of dried grain and a decrease in the yellowness intensity of kernel cross‐section were also observed. The aforementioned changes were associated with the decomposition of carotenoids (endosperm colour) and reduction of soluble proanthocyanidin and total phenolic compounds (surface colour). The drying processes also lowered germination energy and capacity, in addition to susceptibility to moisture diffusion into the endosperm. These adverse results were cultivar dependent and affected the quality of malt and wort only to a limited extent. The main changes were an increase in the Kolbach index in malt from Mauritia cv., and a fluctuation of the diastatic power of malt that did not exceed ±3%. Generally, drying of barley grain in spouted bed should be conducted at an inlet air temperature of 40 °C and using an IR drier at a radiation intensity of 600 W m^?2.     

Drying of chitosan in a spouted bed: The influences of temperature and equipment geometry in powder quality

The influence of temperature and spouted bed geometry in drying chitosan with relation to powder quality (molecular weight, deacetylation degree, particle size, color) and operation characteristics (product recovery and mass accumulated) were investigated. Chitosan paste was obtained from shrimp wastes and dried in a spouted bed (slot-rectangular and conical-cylindrical geometries) with different inlet air temperatures (90, 100 and 110 °C). Thermogravimetric curves, infra-red analysis and scanning electron microscopy were carried out in order to verify powder quality. Chitosan paste used in drying experiments showed solid content 4%, molecular weight 140 kDa and deacetylation degree 85%. In all drying experiments deacetylation degree was not modified and final moisture content was in the commercial range (10%). Temperature increase caused an increase in molecular weight, powder darkening and increased particle size. The best powder quality was obtained in slot-rectangular spouted bed at 90 °C. In this condition product recovery was 65%, accumulated mass was 20% and the powder presented faint yellow coloration, high thermal stability and porous heterogeneous surface.     

THIN LAYER METHOD ANALYSIS OF SPOUTED BED DRIED MALAYSIAN PADDY – CHARACTERISTIC DRYING CURVES

A lab‐scale spouted bed dryer was used for the drying of paddy. The Malaysian grown paddy is a sample of Geldart's Group D particle. Drying was carried out in the dryer at two different internal configurations, namely with or without the installation of a draft tube, and at several drying temperatures (60–90C), air flow rates (1.14–1.45 m/s) and bed heights (30–45 cm). Drying kinetics of paddy in spouted bed showed only induction and falling rate periods, without constant drying rate period. Thin layer method analysis shows characteristic drying rate curves of linear and exponential functions for the first and second falling rate period, respectively, in conventional spouted bed drying. A single power function was observed in spouted bed drying with a draft tube, mainly as a result of a better tempering effect that gave a lower drying rate gradient.     

红外—喷动床联合干燥设备研制与分析

为较好地解决单一红外干燥均匀性差的问题,利用红外加热高效节能的特点,结合喷动床流动性好、传热均匀的特点,设计了红外联合喷动床干燥设备。该装置包括喷动床干燥系统、红外辐射加热系统、回风式空气调节系统、动力循环系统和控制系统等。并以新鲜毛豆为物料,对该装置干燥均匀性和产品品质进行试验验证。结果表明,单一红外干燥耗时270 min,而红外—喷动床联合干燥耗时160 min,与单一的红外干燥相比,红外—喷动床联合干燥时间缩短了40.7%;同时,红外—喷动床联合干燥设备减轻了毛豆仁干瘪皱缩现象,使干制品具有较好的豆香味和感官品质。     

Physical properties of parboiled wheat and bulgur produced using spouted bed and microwave assisted spouted bed drying

The main objective of this study was to compare the spouted bed and microwave assisted spouted bed drying on affecting physical properties of parboiled wheat and bulgur. Drying was performed at different temperatures (50 °C, 70 °C, 90 °C) and microwave powers (288 W, 624 W). Bulk and apparent density, bulk and apparent porosity, sphericity, color, microstructure and pore size distribution of parboiled wheat were investigated after drying. Yield and water absorption capacity were determined in bulgur samples. The effect of air temperature on physical properties of product except color was not significant in spouted bed drying. More porous structure was observed in wheat samples dried in microwave assisted spouted bed compared to air dried ones. Sphericity and bulk density were higher when high temperature was combined with high microwave power. In microwave assisted spouted bed drying, similar yield value but lower water absorption capacity of bulgur were observed as compared to spouted bed drying.     

Drying kinetics and quality of okara dried in a jet spouted bed of sorbent particles

Okara or soy residue is a byproduct of soymilk and tofu production process. Okara has high protein content and can be used as an ingredient in many food products or can be used as animal feed. However, okara deteriorates rapidly; hence raw okara must be dried as early as possible under appropriate conditions. Drying could also help eliminating undesirable antinutritional factors in okara. The present study investigated the feasibility of drying okara using a combined convection-sorption drying, i.e., the use of a jet spouted bed of sorbent particles. The effects of various parameters such as drying air temperature and velocity, mass ratio of sorbent particles to okara, and initial bed height of okara on the drying kinetics were investigated. Also, various quality attributes of okara viz. color, oxidation level, rehydration ability, urease activity and protein solubility as well as the specific energy consumption during drying were investigated in both low- and high-temperature ranges.     

Drying of yellow pea starch on inert carriers: Drying kinetics,moisture diffusivity,and product quality

This study aimed at investigating the drying of yellow pea starch dispersions on inert solid carriers and determining the drying kinetics, moisture diffusivity and the product quality, quantified through damage index and final moisture content. Drying kinetics accomplished in a convective drying tunnel show that the overall mass transfer is controlled by internal migration of moisture within the starch particles. For a given inlet air temperature from 100 to 180 °C, the apparent diffusion coefficient derived from the drying curves increases exponentially with the instantaneous moisture content, with values ranging from 4 × 10⁻¹¹ to 3 × 10⁻⁸ m²/s. Due to low diffusivity and the thin coat formed on the surface of solid carriers, the resistance to internal diffusion is negligible as compared to the overall mass transfer resistance when drying of starch dispersions takes place on inert solid carriers. Drying of yellow pea starch dispersion on Teflon particles as inert carriers was studied in laboratory and pilot fast spouted bed dryer for inlet air temperatures from 140 to 240 °C, and initial solid content of 38%, mass (d.b.). The starch damage index for targeted product moisture content was below 2.5% in the inlet air temperature range from 120 to 210 °C, when atomizing from the bottom of dryer.     

MICROWAVE and SPOUTED BED DRYING of FROZEN BLUEBERRIES: the EFFECT of DRYINGAND PRETREATMENT METHODS ON PHYSICAL PROPERTIES and RETENTION of FLAVOR VOLATILES

Frozen blueberries (Vaccinium corymbosum L cv. 'Elliott') were dried in a microwave and spouted bed combined dryer (MWSB) at 70C air temperature and 3.7 W/g microwave power (wet material). the effect of pretreatment using a 2.5% Ethyl Oleate & 0.2 NaOH dipping solution followed by sucrose osmotic treatment was investigated. the drying kinetics of MWSB drying was compared with spouted bed (SB) drying with dipping treatment, and with tray drying. the rehydration ratio, the color, and the bulk density of MWSB dried blueberries were compared with those of freeze, tray, and SB drying. the drying time needed to reduce blueberry moisture content from 82.5% to 15% (wet basis) using MWSB drying was 1/19 and 1/24 (with and without pretreatment) of the time for tray drying. the MWSB drying resulted in a low bulk density and more reddish and less blue color compared with other methods. MWSB dried frozen blueberries exhibited a higher rehydration ratio in short soaking times. Analysis of flavor volatiles by GC/MS identified ten heat-generated compounds. Microwave heating generated three unique flavor compounds (2-Butanone, 2-methyl butanal, and 3-methyl butanal). Freeze-dried frozen blueberries lost several flavor compounds including the typical blueberry aroma, the 1, 8-Cineole.     

Batch drying of banana pieces — effect of stepwise change in drying air temperature on drying kinetics and product colour

Slices of banana were dried in a two-stage heat pump dryer capable of producing stepwise control of the inlet drying air temperature while keeping absolute humidity constant. Two stepwise air temperature profiles were tested. The incremental temperature step change in temperature of the drying air about the mean air temperature of 30°C was 5°C. The total drying time for each temperature-time profile was 240 min. The drying kinetics and temporal colour change of the products dried under these stepwise variation of the inlet air temperature were measured and compared with constant air temperature drying. The effects of the profile starting temperature and cycle time on both drying kinetics and product quality were also studied. It was observed that by employing stepwise-varying drying air temperature with appropriate starting temperature and cycle time, it was possible to reduce significantly the drying time to reach the desired moisture content with improved product colour.     

OPTIMIZATION OF SPRAY DRYING CONDITIONS FOR PRODUCTION OF BIFIDUS MILK POWDER FROM COW MILK

Bifidus milk powder was prepared by supplementing cow's milk with predetermined level of additives to obtain slurry of desired concentration. The slurry was sterilized, cooled and inoculated with 24‐h‐old bulk culture of Bifidobacterium bifidum at 10% and incubated at 37C for 24 h, cooled and dried in SM Scientech Lab model spray dryer with predetermined spray drying conditions. The bifidus milk powder contains bifidobacteria counts from 1.88 × 10⁹ to 15.80 × 10⁹ cells/g dry weight and their percent survival was 4.17–35.11%. Maximum survival was obtained by using the following spray drying conditions: inlet temperature of 164.02C, slurry concentration of 25.62% total soluble solids and air pressure of 2.5 kg/cm². The high temperature and air pressure of spray drying markedly influenced the color and appearance of final product. The inlet temperature and air pressure showed a significant effect on survival of bifidobacteria in the final product.     

香椿芽热泵式冷风干燥模型及干燥品质

为获得干燥速率快、品质高的香椿芽制品,以新鲜香椿芽为原料对其进行冷风干燥处理,研究不同干燥条件下香椿芽的干燥特性;采用Weibull函数模型对干燥曲线进行拟合并分析干燥过程;以干燥时间、干燥能耗、叶绿素含量、VC含量以及复水率为指标对不同条件下香椿芽冷风干燥过程进行加权综合评价;以热风干燥和真空冷冻干燥为参照,对比研究较优冷风干燥参数下香椿芽干制品的品质。结果表明,提升干燥温度、进口风速以及减少装载厚度均能显著减少香椿芽冷风干燥耗时（P＜0.05）,不同干燥条件对干燥耗时的影响程度由大到小为：温度＞进口风速＞装载厚度;Weibull函数模型能够准确描述香椿芽冷风干燥过程中水分含量变化过程（R2＞0.9）,其形状参数均小于1,整个干燥过程为降速干燥,主要由内部水分扩散控制;香椿芽冷风干燥有效水分扩散系数在（6.272～9.637）×10－9 m2/s之间,均属于10－9数量级,且受温度的影响最大;当干燥温度、装载厚度和进口风速分别为20 ℃、3.0 mm、2 m/s时,香椿芽冷风干燥的综合评分值最高,实验范围内,该条件较适合应用于香椿芽的冷风干燥中;相对于热风干燥而言,冷风干燥产品的品质更接近真空冷冻干燥产品的品质。     

Analysis of giant pumpkin (Cucurbita maxima) drying kinetics in various technologies of convective drying

The paper analyses the results of the research on drying a variety of giant pumpkin (Justynka – 957). The research involved drying kinetics of pumpkin as well as changes in the volume of 10 mm pumpkin cubes, dried at the temperature of 80 °C, using free (natural) convection and in the forced convection in the tunnel dryer, with the drying factor speed of 1.2 m s⁻¹ and in the fluid bed dryer. Drying kinetics of pumpkin pieces dried in the tunnel dryer, fluid bed dryer and during two-stage initial drying in the tunnel, and in the fluid bed dryer were examined. Measurements results were used to verify the theoretical models of drying kinetics of the first period taking volume shrinkage into consideration, and the second period of the examined processes.     

TWO-PHASE MODELING AND THE QUALITY OF SOYBEAN SEEDS DRIED IN A COUNTER-CURRENT MOVING BED DRIER

The purpose of the present work is to study the simultaneous heat and mass transfer between air and soybean seeds in a countercurrent moving bed dryer, based on the application of a two‐phase model to the drying process. The numerical solution of the model is obtained by using a computational code based on backwards differential formulae. The experimental data of air humidity and temperature and of seed moisture content and temperature at the dryer outlet are compared to the simulated values, showing a good agreement. This work also analyzes the effect of the main process variables (drying air temperature, air relative humidity, air velocity and solids flow rate) on the soybean seeds quality during drying. Empirical equations fitted to the experimental data are proposed for predicting the soybean seed quality (germination, vigor and fissures) as a function of the investigated variables.     

Conical spouted bed drying of Baker's yeast: Experimentation and multi-modeling

Baker's yeast drying experiments in a conical spouted bed are used to characterize the effects of operating conditions on drying behavior. A novel multiscale model, describing Baker's yeast drying in a conical spouted bed, is presented; it is based on an intrinsic drying model developed for a single pellet, combined with a gas–solid flow model developed for a conical spouted bed. The resulting phenomenological model, which has only one adjustable parameter, is in good agreement with the experimental results. The model is capable of adequately predicting the drying rate of Baker's yeast pellets during the entire drying period in a conical spouted bed: from the beginning, where the water removal rate is limited by the air saturation with vapor during its residence time in the bed; to the end, where the water removal rate is dictated by internal resistance within the yeast pellets.The quality of dried Baker's yeast was characterized by measuring the gassing power in bread dough. This parameter was monitored during the conical spouted bed drying experiments. It was found that yeast degradation is linked to intracellular water removal (type D, end of the drying below a moisture content of around 0.5 (d.b.)) and it is mostly the rate of this water removal that controls the final quality of the product. Intercellular water removal (type E, beginning of the drying) was found to have no significant influence on yeast degradation. In all the cases, degradation is amplified when solid temperature is higher than 40 °C.     

Protein quality of dried enzymatic hydrolysate from anchovy produced in a spouted bed of inert particles

The anchovy (Engraulis anchoita) is a pelagic fish and due to its abundance in South America shows a sustainable exploitation. The enzymatic hydrolysis of anchovy protein associated to the drying technique in spouted bed was analysed in order to obtain products with the best characteristics. The drying conditions were inlet air temperature, concentration and flow rate of suspension. The degree of hydrolysis of the anchovy suspension was of 3.8%, and its available lysine and specific antioxidant activity were of 86 g kg^?1_protein and 4.31 mm _DPPH kg^?1 min^?1, respectively. In spouted bed drying, the lowest reduction in available lysine (9%) and loss of specific antioxidant activity (8%) were found at 90 °C, and suspension concentration and flow rate of 65 g L^?1 and 200 mL h^?1, respectively. The dried product was characterised as a protein source of high biological value due to the essential amino acids profile.     

造纸红液喷雾干燥研究

在3种不同的进出口气体条件下对亚硫酸镁盐法蒸煮苇浆的造纸红液进行了离心喷雾干燥实验。综合考虑产品的湿含量及成份,以进气温度250℃,出口气体85℃时所得产品质量最佳。进一步测定了干粉的干燥曲线,以验证一级喷雾干燥的合理性。另外在实验过程中发现了产品具有吸湿性,并测定了干粉的等温吸附线。图3表1参9     

SELECTION OF CHEMICAL AND THERMAL PRETREATMENT COMBINATION TO REDUCE THE DEHYDRATION TIME OF SOUR CHERRY (Prunus cerasus L.)

Sour cherry (Prunus cerasus L.) is a good source of anthocyanins showing antioxidant and anti‐inflammatory activities. Contemporary drying processes of fruits and vegetables should be fast and at relatively low drying temperatures to minimize the energy consumption and the thermal degradation of their nutritional composition. Therefore, sour cherries placed into sample bags were dipped in one of eight different pretreatment combinations consisting of chemical solutions (2% ethyl oleate, 2% K₂CO₃, 1% citric acid or water) and dipping temperature (23 or 60C) for 1 min to accelerate the skin moisture diffusivity by breaking down the waxy cuticular surface of sour cherry. Pretreated sour cherry samples were dehydrated by three different methods (artificial drying, solar drying and open sun drying). Sour cherries treated with 2% ethyl oleate solution at room temperature (23C) were the fastest to reach the final weight loss percentage (75%). They dried in 24 h in the laboratory tray dryer providing 45.2C drying air. The untreated samples reached the same weight loss percentage of 75% at a drying time of 92 h. A high dipping temperature (60C) eliminated the positive effect of ethyl oleate. Solar drying and open sun drying of sour cherries treated with 2% ethyl oleate at room temperature finished approximately in 149 h and 372 h, respectively. The color of dried sour cherries was used as a quality indicator. The increase of dehydration time decreased redness values as seen in solar drying and open sun drying. The recommended pretreatment and drying processes for sour cherries are dipping them into 2% ethyl oleate solution at room temperature for 1 min and then drying them artificially at 45.2C air temperature to effectively retain their original color.     

Microwave Finish Drying of Diced Apples in a Spouted Bed

The combination of a spouted bed with microwave heating to improve heating uniformity was evaluated. Experiments were performed on a laboratory system in which evaporated diced apples of about 24% moisture were dried to about 5% at 70°C air temperature using four levels of microwave power density (0 to 6.1 W/g). With the combination method, temperature uniformity in diced apples was greatly improved as compared to that with a stationary bed during microwave drying. Products had less discoloration and higher rehydration rates as compared to conventional hot air drying or spouted bed (SB) drying. Drying time could be reduced by >80% compared with SB drying without microwave heating.