Monitoring mechanical damage in structural materials using complimentary NDE techniques based on thermography and acoustic emission

This work deals with nondestructive evaluation (NDE) of the fracture behavior of metallic materials by combining thermographic and acoustic emission (AE) characterization. A new procedure, based on lock-in infrared (IR) thermography, was developed to determine the crack growth rate using thermographic mapping of the material undergoing fatigue. The thermography results on crack growth rate were found to be in agreement with measurements obtained by the conventional compliance method. Furthermore, acoustic emission was used to record different cracking events. The rate of incoming signals, as well as qualitative features based on the waveform shape, was correlated with macroscopically measured mechanical parameters, such as load and crack propagation rate. Additionally, since the failure modes have distinct AE signatures, the dominant active fracture mode was identified in real time. The application of combined NDE techniques is discussed for characterizing the damage process which leads to catastrophic failure of the material, thereby enabling life prediction in both monolithic aluminum alloys and aluminum alloy/SiC particle (SiC_p) reinforced composites.     

Non-destructive assessment of the fatigue strength and damage progression of satin woven fiber reinforced polymer matrix composites

The aim of this study is to utilize infrared thermography to assess the critical damage states, and to capture the evolving damage processes, of 5HS and 8HS woven carbon fiber/epoxy composites subjected to uniaxial in-plane tensile quasi-static and fatigue loading. Quasi-static test results revealed that the dominant damage mechanisms were matrix cracks contained within the weft yarns, which initiated at the thermally-detected material thermoelastic limit and were confirmed through SEM observations. An established thermographic technique was also used to confirm the existence of a high cycle fatigue limit, which may in fact be a characteristic of all fabric reinforced polymeric composites. Temperature profiles captured during cyclic testing directly correlated with corresponding stiffness degradation profiles, providing support for thermography as an accurate fatigue damage metric. The infrared camera was able to detect the evolution of weft yarn cracking during the initial stage, as well as the initiation and growth of interply delamination cracking during the final stage of three-stage cyclic damage evolution. The reported results and observations provide an important step in the validation of thermography as a powerful non-destructive tool for assessing the development of damage, as well as predicting the critical damage states of fiber reinforced polymeric composite materials.     

A study of fibre and interface parameters affecting the fatigue behaviour of natural fibre composites

The tension–tension fatigue behaviour of different natural fibre reinforced plastics was investigated. The composites used were made of flax and jute yarns and wovens as reinforcements for epoxy resins, polyester resins and polypropylene.Fibre type, textile architecture, interphase properties, fibre properties and content were found to affect the fatigue behaviour strongly as illustrated with damping versus applied maximum load curves. It was found that natural fibre reinforced plastics with higher fibre strength and modulus, stronger fibre–matrix adhesion or higher fibre fractions possess higher critical loads for damage initiation and higher failure loads. In addition, damage propagation rates were reduced.Furthermore, unidirectional composites were less sensitive to fatigue induced damage than woven reinforced ones.     

Fatigue behaviour assessment of flax–epoxy composites

The present study focuses on the characterisation and evaluation of the fatigue behaviour of flax–epoxy composites. A better understanding of this behaviour allows the prediction of long-term properties to assess the viability and long-term durability of these materials. The purpose of this work is to systematically compare the tension–tension fatigue behaviour of flax fibre composites for one random mat, six textile architectures and two laminate configurations, which are used in a wide range of applications. The fibre architecture was found to have a strong effect on the fatigue behaviour, where higher static strength and modulus combinations present the best fatigue characteristics. They have a delayed damage initiation and increased fatigue life as well as a reduced damage propagation rate combined with higher energy dissipation in the early stages of fatigue loading.     

Prediction of initiation of transverse cracks in cross-ply CFRP laminates under fatigue loading by fatigue properties of unidirectional CFRP in 90° direction

A fatigue life to the initiation of transverse cracks in cross-ply carbon fiber-reinforced plastic (CFRP) laminates has been predicted using properties of the fatigue strength of unidirectional CFRP in the 90° direction. In the experiments, unidirectional [90]₁₂ laminates were used to obtain a plot of maximum stress versus number of cycles to breaking, and two types of cross-ply laminates of [0/90₄]_S and [0/90₆]_S were used to evaluate the initiation and multiplication of transverse cracks under fatigue loading. Transverse cracks were studied by optical microscopy and soft X-ray photography. Analytical and experimental results showed good agreement, and the fatigue life for transverse crack initiation in cross-ply laminates was predicted successfully from the fatigue strength properties of the unidirectional CFRP in the 90° direction. The prediction results showed a conservative fatigue life than the experimental results.     

Tension-compression fatigue behaviour of fibre-reinforced ceramic matrix composite with circular hole

The tension-compression fatigue behaviour of a silicon carbide fibre-reinforced glass ceramic matrix composite, SiC/1723, with a circular hole was investigated at room temperature. Two laminate lay-ups were studied: cross-ply, [0/90]_2s, and unidirectional, [0]₈. At first, the fatigue limit based on one million cycles was established for the tension-tension fatigue condition. Then, the fatigue response under fully reversed (tension-compression) cycling loading with a maximum stress equal to the tension-tension fatigue limit was investigated. This tension-compression loading resulted in an increased amount of damage and ultimately led to the specimen failure well before one million cycles. In the cross-ply laminate, the damage mechanisms in the 90° plies involved transverse cracks only during tension-tension cycling, and transverse and longitudinal cracks during tension-compression cycling. In the unidirectional laminate, the longitudinal cracks which initiated at the hole periphery grew longer in tension-compression fatigue than in tension-tension fatigue. On the other hand, no damage and consequently no effect on fatigue life was observed during the compression-compression fatigue condition only.     

Property Modeling across Transition Temperatures in PMC's: Part III. Bending Fatigue

Parts I [1] and II [2] of the present paper introduced systematic models for the computation of thermal effects on strength and stiffness of unidirectional polymer matrix composites (PMC's) as well as the life prediction of these materials in end-loaded bending at elevated temperatures. The last step of this study was the possibility of introducing such models in durability codes such as MRLife [3]. A recent method was developed for the experimental characterization of end-loaded bending fatigue behavior of composites at elevated temperatures. The literature dealing with the durability of composite materials in bending focuses mainly on 3 and 4 point bending [4–6]. A limited set of data as well as the basis for theoretical modeling for fatigue end-loaded bending is available in the literature [7]. However, the life prediction scheme required elevated temperature experiments. New experiments in fatigue bending were performed in order to complete the available data. Microscopic observations revealed new information for the understanding of the damage process of unidirectional AS4/PPS composites in end-loaded fatigue bending. Finally, the models developed in Parts I and II were integrated into the MRLife integral enabling the life prediction of unidirectional PMC's under combined mechanical and thermal loads from room temperature experimental data.     

Fatigue life prediction of carbon/epoxy laminates by stochastic numerical simulation

A three dimensional (3D) finite element model is developed to predict the progressive fatigue damage and the life of a plain carbon/epoxy laminate (AS4/3501-6) based on the longitudinal, transverse and in-plane shear fatigue characteristic. The model takes into account stress analysis, fatigue failure analysis, random distribution and material property degradation. Different cross- and angle-ply laminates including [0₈], [90₈], [0/90₂]_s, [0/90₄]_s, [0₂/90₂]_s, [30₁₆], [45/−45]_2s with the available experimental data are considered for the fatigue life simulation. In order to consider the random distribution of the laminate’s properties from element to element in the model, the laminate’s stiffness, and strength are randomly generated using a Gaussian distribution function. Sudden and gradual material properties degradation are considered during the fatigue simulation. The progressive fatigue damage and failure analysis is implemented in ABAQUS through user subroutines UMAT (user-defined material) and USDFLD (user-defined field variables). The predicted fatigue life of the simulation for different laminates is in good agreement with the experimental results.     

Progressive damage assessment of centrally notched composite specimens in fatigue

The aim of this study is to assess the residual properties and the corresponding damage states within centrally notched quasi-isotropic [0/−45/+45/90]_S T650/F584 (Hexcel) carbon-fiber/epoxy composites subjected to fatigue loading using Digital Image Correlation (DIC), radiography, and a non-contact vibration measurement technique. Quasi-static tests were performed on virgin samples using DIC to determine the full-field in-plane strains at different applied load levels. Fatigue tests were interrupted during the fatigue lifetimes in order to perform quasi-static tests with DIC measurements. Non-contact vibration measurements were performed to investigate the effect of fatigue damage on residual frequency responses. X-ray computed tomography was used to determine the type, location, and extent of fatigue damage development. The results provide an important step in the validation of DIC and vibration response as a powerful combined non-destructive evaluation tool for monitoring the development of fatigue damage as well as predicting the damage level of notched composite materials.     

A unified fatigue life model based on energy method

A new unified fatigue life model based on the energy method is developed for unidirectional polymer composite laminates subjected to constant amplitude, tension–tension or compression–compression fatigue loading. This new fatigue model is based on static failure criterion presented by Sandhu and substantially is normalized to static strength in fiber, matrix and shear directions. The proposed model is capable of predicting fatigue life of unidirectional composite laminates over the range of positive stress ratios in various fiber orientation angles. By using this new model all data points obtained from various stress ratios and fiber orientation angles are collapsed into a single curve.

The new fatigue model is verified by applying it to different experimental data provided by other researchers. The obtained results by the new fatigue model are in good agreements with the experimental data of carbon/epoxy and E-glass/epoxy of unidirectional plies.     

Damage Assessment of CFRP [90/±45/0] Composite Laminates over Fatigue Cycles

The present paper develops a stiffness-based model to characterize the progressive fatigue damage in quasi-isotropic carbon fiber reinforced polymer (CFRP) [90/±45/0] composite laminates with various stacking sequences. The damage model is constructed based on (i) cracking mechanism and damage progress in matrix (Region I), matrix-fiber interface (Region II) and fiber (Region III) and (ii) corresponding stiffness reduction of unidirectional plies of 90°, 0° and angle-ply laminates of ±45° as the number of cycles progresses. The proposed model accumulates damages of constituent plies constructing [90/±45/0] laminates by means of weighting factor η ₉₀, η ₀ and η ₄₅. These weighting factors were defined based on the damage progress over fatigue cycles within the plies 90°, 0° and ±45° of the composite laminates. Damage model has been verified using CFRP [90/±45/0] laminates samples made of graphite/epoxy 3501-6/AS4. Experimental fatigue damage data of [90/±45/0] composite laminates have fell between the predicted damage curves of 0°, 90° plies and ±45°, 0/±45° laminates over life cycles at various stress levels. Predicted damage results for CFRP [90/±45/0] laminates showed good agreement with experimental data. Effect of stacking sequence on the model of stiffness reduction has been assessed and it showed that proposed fatigue damage model successfully recognizes the changes in mechanism of fatigue damage development in quasi-isotropic composite laminates.     

Low-cycle fatigue of unidirectional composites:: Bi-linear S–N curves

Low-cycle fatigue (LCF) behavior of polymer matrix composites (PMCs) is investigated in an experimental study of unidirectional glass/epoxy composites subjected to axial tensile loading along longitudinal 0° orientation of fibers. Under high LCF loads, fatigue life of PMCs is found to be less than 10⁴ loading cycles due to the high property degradation rates that are noticeably higher than those seen during high-cycle fatigue (HCF). In PMC response, unique LCF features have been identified and linked with damage accumulation patterns in unidirectional composites. At high loads near the ultimate strength of specimens, large strains and finite strain rates are found to be significant under semi-rectangular loading so the LCF behavior is affected. Lower and upper limits for the LCF life impose some restrictions on the S–N curves that are obtained for the LCF life assessment. A bi-linear S–N curve is used to approximate the data in the LCF and HCF regions. The bi-linear S–N relationship and the associated fatigue model are described by a proposed analytical formula. The concept of pre-LCF damage state is introduced.     

固化温度对亚麻纤维及其增强复合材料力学性能的影响

研究热压成型过程中,不同固化温度对亚麻纤维及其增强复合材料力学性能的影响。结果表明:亚麻纤维在120,140℃和180℃分别处理2h后单纤维拉伸性能发生不同程度的下降。环氧树脂E-51在120,140℃和180℃下固化2h后拉伸性能未发生明显变化。基于环氧树脂的单向亚麻纱线增强复合材料分别在120℃和140℃固化成型时,拉伸强度和冲击强度变化不大。但当固化温度达到180℃时,由于亚麻纤维在高温环境下损伤较为严重,其增强复合材料的拉伸强度和冲击强度均发生明显的下降。然而复合材料的拉伸模量随着成型温度的升高有一定幅度的提升。     

Fatigue behaviour of hybrid composites

A study has been made of the fatigue behaviour of carbon/Kevlar-49/epoxy hybrid composites. Stress-life data have been obtained for both unidirectional and [(±45, 0, 0)₂]_s laminates in repeated tension and compression-tension cycling tests at various values of the stress (or R) ratio. Goodman (constant life) diagrams are presented for the unidirectional composites which indicate that the fatigue resistance of hybrid mixtures varies linearly with composition. The presence of the Aramid fibre, whose natural resistance to compression loads is suspect, does not appear to exert any unexpected damaging influence on the response of the hybrids either in tensile or tension-compression loading. This is also true of the behaviour of hybrid laminates containing plies at an angle to the main loading direction.     

The effect of temperature on fatigue damage of FRP composites

The present study intends to investigate the effect of temperature on cumulative fatigue damage (D) of laminated fibre-reinforced polymer (FRP) composites. The effect of temperature on fatigue damage is formulated based on Ramkrishnan–Jayaraman and Varvani-Farahani–Shirazi residual stiffness fatigue damage models. The models are further developed to assess the fatigue damage of FRP composites at various temperatures (T). This task is fulfilled by formulating the temperature dependency of Young’s modulus (E) and ultimate tensile strength (σ_ult) as the inputs of the models. Temperature-dependant parameters of Young’s modulus and ultimate tensile strength are found to be in good agreement with the experimentally obtained data when used for unidirectional, cross-ply and quasi-isotropic FRP laminates. The proposed fatigue damage model is evaluated using six sets of fatigue damage data. The proposed temperature-dependent model was also found promising to predict the fatigue damage of unidirectional (UD) and orthogonal woven FRP composites at different temperatures.     

Two-stage fatigue loading of woven carbon fibre reinforced laminates

A brief review of the models used to predict the cumulative fatigue damage in FRP composites is presented. Two‐stage fatigue loading of a [0/90,± 45₂,0/90]_s quasi‐ isotropic woven carbon fibre/epoxy resin laminate was evaluated at stress ratio R = 0.05 and the failure mechanisms investigated using x‐radiography after each loading stage. The results are presented in terms of fatigue strength and damage growth and are compared with those in the literature. A low‐to‐high loading sequence is more damaging than a high‐to‐low one and the Palmgren‐Miner linear damage rule may no longer be valid for this kind of material, as previously reported.     

A MECHANISTIC-BASED THERMOMECHANICAL FATIGUE LIFE PREDICTION MODEL FOR METAL MATRIX COMPOSITES

The framework for developing a mechanistic-based life prediction model for metal matrix composites is described. For a composite consisting of unidirectional silicon carbide fibers in a titanium aluminide matrix, SCS-6/Ti-24A1-1INb (at%) [0]₈, three dominant damage mechanisms were identified: (1) matrix fatigue damage, (2) surface-initiated environmental damage, and (3) fiber-dominated damage. Damage expressions were developed for each mechanism along with a method for determining the constants. The damage is summed to obtain the total life. The model is capable of making predictions for a wide range of histories, including isothermal fatigue at different frequencies and stress-ratios, thermomechanical fatigue (TMF) under in-phase and out-of-phase cycling conditions, thermal cycling at constant stress, and stress holds at either maximum or minimum stress. Considering the wide range of cyclic conditions, the predictions compare favorably with experiments. In addition, the controlling damage mechanism for each history is predicted.     

Interlaminar shear behavior of unidirectional glass fiber (U)/random glass fiber (R)/epoxy hybrid and non-hybrid composite laminates

The interlaminar shear behavior of unidirectional glass fiber (U)/random glass fiber (R)/epoxy hybrid composites was studied with short beam shear bending test. Random glass fiber (R)/epoxy means chopped fiber composite having short discontinuous fiber randomly dispersed in epoxy matrix. The effect of stacking sequence and unidirectional glass fiber relative volume fraction (V_fU/V_fT) on the interlaminar shear strength (ILSS) of the manufactured composites has been investigated experimentally and theoretically. The laminates were fabricated by hand lay-up technique with 5 plies. Two non-hybrid composite laminates [R]₅ and [U]₅ were fabricated using the same fabrication technique for the comparison purpose. The average thickness of the manufactured laminates is 5.5 ± 0.2 mm and the total fiber volume fraction (V_fT) is 37%. Failure modes of all specimens were investigated. Experimental results indicated that the ILSS of [U]₅ is higher than those of hybrid and [R]₅ composite. Hybrid composites have higher ILSS than that of random composites. The stacking sequence and (V_fU/V_fT) ratio have a detectable effect on ILSS of the investigated composites.     

Monitoring the damage evolution of flexural fatigue in unidirectional carbon/carbon composites by electrical resistance change method

This paper reported simultaneous monitoring damage evolution of flexural fatigue in unidirectional carbon-fiber-reinforced carbon composites (C/C composites) by electrical resistance change (ERC) methods. The degree of irregularity in electrical resistance changes increased with stress levels increasing. The shapes of electrical resistance change rate–fatigue cycle curves can reflect stress levels and damage types of tested samples: sawtooth shapes reflected delamination at a higher stress level; and “peak” shapes reflected inner damages in one fiber bundle at the fatigue limit stress level. In addition, the similarity of initial electrical resistance–fatigue life curve and S–N curve was observed clearly. In summary, ERC methods can monitor the damage evolution and qualitatively estimate the fatigue life of unidirectional C/C composites.