蚀坑法测定铝合金板材织构

介绍了蚀坑法的原理和计算方法,并用蚀坑法和X射线衍射ODF(取向分布函数)图分别测定了HL01铝合金板退火后的再结晶织构.结果表明,再结晶织构主要有戈斯织构、立方织构、S织构、R织构及少量铜型和黄铜R织构.用蚀坑法可以定性测定材料的织构.     

再结晶退火对稀土铝箔组织与织构的影响

由铈的质量分数0.004 8%的稀土铝锭均匀化退火、热轧、冷轧制成0.11 mm厚的稀土铝箔.运用Axiovert25型金相显微镜和蚀坑法,对退火后的稀土铝箔组织和织构进行研究.通过不同温度、不同时间的再结晶退火,得到530℃,600 s时稀土铝泊立方织构含量最高.     

蚀坑法研究冷轧及退火工艺对无取向硅钢织构演变的影响

以太原钢铁公司经酸洗后的热轧低硅板卷为实验材料,采用蚀坑法研究了一定退火工艺及不同冷轧工艺对无取向硅钢织构的影响,结果表明,总变形量及退火工艺是影响织构形成的重要因素,采用可逆轧制方法(冷轧总变形量控制在70%左右,分8道次完成,并且平均分配各道次压下率)和890 ℃加热,保温4 min,然后水冷,可以获得较高的{100}面系织构组分占有率的无取向硅钢.     

冷轧及退火工艺对包钢CSP薄板织构演变的影响

对包钢CSP热轧板进行了冷轧及退火,利用显微镜观察了试样的织构蚀坑,并进行了硬度测试.结果表明,对于同一试样,在1/4厚度处的{111}织构明显比1/2厚度处的多,且在1/2厚度处{100}织构有明显的增加;当退火工艺与试样厚度位置等条件都相同时,试样的{111}/{100}织构的线密度比值随冷轧压下率增大先上升后下降,在67%时达到最大值,与有利{111}织构组分变化相同;压下率相同时,保温时间越长,线密度{111}/{100}的值越大,有利织构组分越大,从而深冲性能越好.     

高压阳极铝箔制备过程中组织与织构的演变

以高纯铝为原料,通过热轧、中间退火、冷轧和再结晶退火制成0.11 mm厚的高压阳极铝箔,运用光学显微镜和蚀坑法研究了此制备过程中铝箔组织与织构的演变过程.结果表明,伴随着组织的变化,织构的类型也由形变织构变为典型的再结晶织构,且再结晶织构形成机制符合择优生长理论.     

退火工艺及冷轧压下率对CSP工艺低碳冷轧板微观组织及织构演变规律的影响

以包钢CSP工艺生产的5.0 mm热轧板在实验室分别压下到1.75,1.25和0.75 mm冷硬板为原料,在实验室模拟了包钢罩式退火工艺,观察了不同压下率试样的显微组织.实验表明,通过观察罩式退火过程中试样的组织的变化,确定了再结晶开始温度在540℃左右,再结晶终了温度为700℃左右.并用X射线检测了试样在热轧和成品两个阶段的织构.结果表明,随着冷轧压下率的增大,再结晶进行的速度增:大,成品试样的织构密度增大,织构类型以{111}<110>和{111}<112>织构为主,但两者织构密度相差不大.     

IF钢生产过程中的织构演变

对IF钢生产过程中热轧、冷轧及退火试样的织构演变进行研究。分别借助EBSD和XRD测定和计算了热轧、退火及冷轧试样的取向分布函数及相关织构组分的体积分数。结果发现,热轧板在变形过程中发生了动态再结晶,晶粒为细小的等轴晶,为后续组织发展提供了基础;热轧后试样中的织构很弱,不会影响冷轧织构组分及含量。冷轧过程是织构形成的主要过程,试样中含有4种主要的织构组分：{001}〈110〉、{111}〈110〉、{111}〈112〉和{112}〈110〉。退火过程中发生再结晶,4种冷轧织构组分在退火过程中均分别转变为{111}面织构。     

工业铜单晶线材浸蚀蚀坑的研究

对工业铜单晶线材用不同浸蚀剂,浸蚀时间,材料晶体取向等方面进行了浸蚀试验.结果表明,在氯化铁盐酸溶液中仅当配比为20 g(FeCl3)∶5 ml(HCl)∶100 ml(H2O)时会有蚀坑产生;蚀坑密度(EPD)随试样浸蚀时间和试样的变形量的增加而增大,当达到一定程度时会趋于饱和;铜单晶线材中(111)面EDP值高于(100)面;经过扫描电镜观察,判定该蚀坑为位错蚀坑.铜单晶线材中位错蚀坑密度与材料浸蚀时间,变形量以及晶体学取向有关.     

再结晶退火温度对无取向硅钢织构和磁性能的影响

对冷轧及退火后无取向硅钢织构及磁性能的变化进行研究。借助电子背散射衍射（EBSD）技术测量退火试样的极图,计算取向分布函数（ODF）和织构组分的体积分数,并利用TYU-2000M磁性能测量仪测量试样的磁性能。结果表明,810、840、880℃下退火3min后,试样的再结晶均充分完成,且晶粒随着退火温度的升高而长大;退火后,试样中首先显现{111}〈112）织构组分,且随退火温度的升高呈增强趋势;退火温度继续升高时,{111}〈110〉织构组分增强,一次再结晶后材料中出现{111}面织构,导致试样的磁感应强度B50降低,同时由于晶粒的长大使得试样的铁损P15减小。     

稀土电解电容器铝箔制备过程中的织构演变规律

采用蚀坑法、EBSD微取向分析和X射线法等手段,对稀土电解电容器用铝箔制备过程中的织构演变规律进行了研究.结果表明,冷轧态织构主要要类型是立方织构({001}《100》)、黄铜织构({011}《211》)、高斯织构({011}《100》)、S织构({123}《634》)和铜型织构({112}《111》).铝箔的再结晶织构主要类型是立方织构({001}《100》)、高斯织构({011}《100》)、R织构({124}《211》).随着Ce含量的增加,稀土铝箔的再结晶织构中立方织构增加,但并不是越多越好.在稀土的质量分数为0.007 4%时立方织构含量最多.同时R织构随Ce含量的增加先减少,后略有增加.随着再结晶退火温度的增加立方织构的含量增加,R织构含量减少,在530 ℃退火时立方织构含量最多.     

CSP工艺不同冷轧压下率低碳钢板退火织构的演变

采用基于包钢CSP热轧工艺下2.75和4.5 mm现场冷轧至1.0 mm的SPCC钢板,冷轧压下率分别为64%和78%,实验室模拟了罩式退火工艺,并利用XRD测得了冷轧和退火过程中织构的演变.结果表明,两种不同冷轧压下率的钢板在冷轧和退火过程中织构演变规律相似,但是冷轧基料厚度为2.75 mm的钢板在整个过程变化幅度更大,而且成品的织构类型更有利.     

Texture evolution of 440 MPa grade Nb-bearing high strength IF steel during rolling and annealing process

The texture evolution from rolling process to annealing process of 440 MPa grade Nb-bearing high strength IF steel (IF-HSS) was studied. Moreover, the texture of different section in thickness direction of steel sheet after annealing was investigated. Macro-texture measurements using XRD shows that hot rolling texture in Nb-bearing IF-HSS includes a weak γ-fiber and α-fiber, of which main texture components are {001}<110>,{111}<110> and {111}<112>. It is worthy of note that the γ-fiber skeleton line formed after hot rolling. During cold rolling, the absolute maximum shifts to {111}<112> along the γ-fiber and the maximum along the α-fiber shifts to {112} <110>. During recrystallization annealing process, the weaker α-fiber and stronger γ-fiber cold rolling texture transformed to a very strong γ-fiber annealing texture. After annealing the main components from surface to mid-section along thickness display the same character for both α-fiber and γ-fiber, while textures intensity at 1/4 section is higher than that of surface and mid-section.     

Annealing Texture Evolution of Ti-IF Steel during Batch Annealing

Texture development and recrystallization behavior of Ti-IF steel during Batch Annealing (BA) were investigared with X-ray diffraction and EBSP in lab, and the results were compared with research work on continu ous annealing (CA) with rapid heating rate. The basic tendencies are similar that eary nucleation takes place in <111>ND fibers, <110>RD fibers are consumed at the end of recrystallization, and <111>ND texture dominates over annealing texture. However, the detailed texture transformation during batch annealing is different and somewhat more compicated than tha in rapid-heating process. Moreover, misorientation plays an important role in texture transformation of BA In addition, the results of EBSP are consistent with that of ODF well.     

化学成分及退火温度对连续退火再结晶织构的影响

在MULTIPAS平台上模拟了不同化学成分的IF钢的两种连续退火生产方案。通过X衍射仪和全自动拉伸试验机对样品进行了检测,结合织构分布及力学性能分析了化学成分及退火温度等对IF钢再结晶织构的影响。研究发现当退火温度大于800℃时,退火温度对〈111〉//ND织构强度无显著影响,得到了C、N、Ti元素含量与样品织构的关系。     

Simulation of annealing process effect on texture evolution of deep-drawing sheet St15

A two-dimensional cellular automaton method was used to simulate grain growth during the recrystallization annealing of deep-drawing sheet St 15, taking the simulated result of recrystallization and the experimental result of the annealing texture of deepdrawing sheet St15 as the initial condition and reference. By means of computer simulation, the microstructures and textures of different periods of grain growth were predicted. It is achieved that the grain size, shape and texture become stable after the grain growth at a constant temperature of 700℃ for 10 h, and the advantaged texture components { 111 } 〈 110 〉 and { 111 } 〈 112〉 are dominant.     

Microstructure,Texture, and Hardness Evolutions of Al-Mg-Si-Cu Alloy during Annealing Treatment

Microstructure, texture and hardness evolutions of Al-Mg-Si-Cu alloy during annealing treatment were studied by microstructure, texture and hardness characterization in the present study. The experimental results show that microstructure, texture and hardness will change to some extent with the increase of annealing temperature. The microstructure transforms from the elongated bands to elongated grains first, and then the grains grow continuously. The texture transforms from the initial deformation texture b fiber to recrystallization texture mainly consisting of CubeND {001}310 and P {011}122 orientations first, and then the recrystallization texture may be enhanced continuously as a result of the grain growth. Hardness decreases slowly at first, and then decreases sharply and increases significantly finally. Besides, the particle distributions also have great changes. As the annealing temperature increases, they increase firstly as a result of precipitation, and then gradually disappear as a result of dissolution. Finally, the effect of annealing temperature on microstructure, texture and hardness evolutions is discussed.     

退火温度对Ti-IF钢性能及织构的影响

对冷轧压下率为80%、厚1 mm的Ti-IF钢经不同温度退火处理后进行拉伸试验,测量其塑性应变比r值。观察退火试样的显微组织,并利用电子背散射衍射技术（EBSD）对其性能和再结晶织构进行分析。结果表明,冷轧试验钢分别在780、810、840℃退火3 min后,均发生了再结晶;随着退火温度的升高,大多数晶粒尺寸由5-6μm增大到9-10μm;试验钢的r值随退火温度升高而增大;退火钢再结晶织构表现为强烈的{111}织构,主要由{111}〈110〉和{111}〈112〉两类取向晶粒组成。