镁合金板材温热拉深成形工艺的研究

通过镁合金板材温热拉深试验确定适合板材成形的温度范围，分析了压边力对坯料成形质量的影响，选择适合成形的工艺条件来有效避免工艺缺陷的产生。试验采用刚性压边装置对压边力进行调整，润滑剂采用了液态的PTFE，通过对成形工艺缺陷的分析，确定适合成形的最佳工艺参数，以提高拉深件的极限拉深比。结果表明：成形温度选择在105～170℃范围内，此时镁合金轧制板材具有良好的拉深性能，极限拉深比可达到2．44；坯料的加热时间不宜过长，否则会严重降低板材的塑性变形能力。     

镁合金AZ31B板材热拉深成形工艺参数优化

在不同温度、不同压边力和不同拉深速度下，针对厚度为0．8mm的AZ31B镁合金板材的成形性能用有限元分析软件进行模拟与分析。在25～220℃的温度范围内，采用直径为140mm的坯料进行冲压成形，研究成形温度、拉深速度以及压边力对AZ31B镁合金板成形性能的影响。结果表明：成形温度为200℃时的极限拉深比达到了2.8；成形温度在200℃以下时，随着成形温度的升高。镁合金板材的成形性能越来越好。这证明AZ31B镁合金具有良好的热拉深性能；此外，拉深速度和压边力对AZ31B镁合金的拉深成形也有重要影响。     

镁合金板材的固体颗粒介质拉深工艺参数

提出基于固体颗粒介质成形(SGMF)工艺的镁合金板材差温拉深工艺,并展开试验研究。通过对AZ31B镁合金薄板进行差温拉深成形试验,研究了成形温度、拉深速度、压边力、压边间隙、凹模圆角和润滑条件对拉深性能的影响,确定AZ31B镁合金板料最佳成形工艺参数。结果表明:该工艺可显著提高镁合金板材的成形性能,成形温度及拉深速度对板料拉深性能影响较大,板料最佳成形温度区间为290～310℃,颗粒介质与板料理想温差为110～150℃;压边力和压边间隙对拉深性能产生联合影响;此外,凹模圆角和润滑条件也对拉深性能有一定的影响。当上述工艺参数达到最佳值时成功拉深出极限拉深比(LDR)为2.41的工件。     

镁合金板材颗粒介质拉深工艺参数数值模拟

为提高镁合金板材拉深性能,提出一种基于固体颗粒介质成形(Solid granules medium forming,SGMF)工艺的镁合金板材差温拉深工艺。以单向拉伸试验获取的AZ31B镁合金板材真应力—应变曲线和颗粒材料性能试验构建的介质线性Drucker-Prager本构模型为基础,采用有限元法对板材拉深成形进行热力耦合数值模拟并进行试验验证,研究压边力、压边间隙和温度对板材拉深性能的影响。结果表明:压边间隙和压边力联合控制比单纯控制压边力或是压边间隙更能有效地提高板材拉深性能;AZ31B镁合金板材在拉深过程中对温度有较强敏感性,板材变形温度为250~300℃,颗粒介质与其温差100~150℃时,板材达到最佳拉深性能;颗粒介质能够对工件筒壁部位提供轴向摩擦力,该摩擦力能有效提高材料拉深性能并保证板厚的均匀性,这是SGMF工艺的优势所在。     

AZ31镁合金铸轧板材热拉深工艺研究

用拉伸试验机测试了AZ31镁合金铸轧板材的高温力学性能和直角弯曲性能,并对镁合金铸轧板材进行了热拉深试验,研究了拉深温度、拉深速率、压边间隙、润滑方式等工艺参数对板材成形性能的影响。试验结果表明,AZ31镁合金铸轧板材适合于200℃以上拉深,且最小弯曲半径小于4mm,最佳拉深工艺条件为,拉深温度225℃～275℃,拉深速率50mm/min～100mm/min,压边间隙1.125t～1.15t,采用固体润滑剂PTFE,可以得到最大极限拉深比为2.95。     

AZ31B薄板手机外壳温冲试验研究

通过对AZ31B镁合金手机壳的温冲试验研究,分析了凸、凹模温度、镁板温度和加热时间、冲压速度以及润滑条件对成形结果的影响.试验表明,在保证坯料充分退火和模具结构合理的前提下,拉深凸模温度保持在230 ℃,凹模及压边圈温度保持在280～320 ℃,用石墨对坯料凸缘和压边圈、凹模肩部进行有效润滑,同时,施加合适的压边力作用,便可以成功地冲压出镁合金壳形件.     

AZ31B镁合金方盒形件拉深成形工艺参数研究

针对AZ31B镁合金方盒形件进行拉深成形工艺试验,分析了单个工艺参数的变化对盒形件拉深成形过程的影响,在其他因素不变的条件下,凹模温度在150~300℃范围内,成形深度随温度升高而增大,在300℃时成形深度达到最大值;凸模温度保持在120℃左右,差温拉深效果较为明显;压边间隙调整到1.3t(t为板材厚度)时,拉深深度最大;拉深速度在30 mm·min-1时成形深度最大。确定了影响拉深成形深度的各工艺参数的先后顺序为:压边间隙、凸模温度、凹模温度和拉深速度。运用正交试验方法进行各工艺参数优化组合,结果表明,采用最优工艺参数组合可以提高AZ31B镁合金方盒形件拉深成形的成形深度。     

6061高强度铝合金拉深工艺参数优化

基于DynaForm对6061高强度铝合金板料拉深成形过程进行仿真模拟,通过设计正交试验,研究在不同温度、压边力、冲压速度下的拉深件成形质量,采用极差与方差分析了3个工艺参数的影响程度,并对该影响因素进行了优化分析。研究结果表明:最佳的成形工艺参数为,400℃的试验温度、8 kN的压边力和4 mm/s的冲压速度。     

AZ31镁合金复杂形状壳体拉深成形试验研究

通过拉深成形试验研究了AZ31镁合金复杂形状壳体的成形性能,分析了成形温度、拉深速度、坯料加热时间及润滑等工艺参数对镁合金手枪壳体拉深成形件质量的影响规律.结果表明,合理的成形工艺参数:成形温度为290～350 ℃,拉深速度为0.1～0.2 mm/s,加热时间为5～10 min,润滑剂采用二硫化钼和机油的混合物,成功地加工出合格的复杂形状的镁合金手枪壳体.     

AZ31与ME20M镁合金板料热拉深性能实验研究

在不同成形温度、拉深速度、润滑条件下对1．2mm厚的AZ31镁合金板料与3mm厚的ME20M镁合金板料进行热拉深性能实验研究。实验表明：AZ31镁板的最佳成形温度为215℃，而ME20M镁板在250℃以上成形性能才随温度的升高明显改善，说明稀土元素对镁合金的室温拉深性能影响很小，但却显著提高镁合金的高温拉深性能，同时也说明镁合金板料具有较佳的轻薄结构成形性；两种镁合金板料热拉深成形性能都对拉深速度敏感．有润滑条件比无润滑条件成形性能要好。通过对成形件传力区部位金相实验分析得知，合理控制热拉深实验参数，能改善成形件微观组织，进而保证成形件质量。     

Effects of Post-weld Heat Treatment on Microstructure,Mechanical Properties and the Role of Weld Reinforcement in 2219 Aluminum Alloy TIG-Welded Joints

In as-welded state, each region of 2219 aluminum alloy TIG-welded joint shows diff erent microstructure and microhardness due to the diff erent welding heat cycles and the resulting evolution of second phases. After the post-weld heat treatment, both the amount and the size of the eutectic structure or θ phases decreased. Correspondingly, both the Cu content in α-Al matrix and the microhardness increased to a similar level in each region of the joint, and the tensile strength of the entire joint was greatly improved. Post-weld heat treatment played the role of solid solution strengthening and aging strengthening. After the post-weld heat treatment, the weld performance became similar to other regions, but weld reinforcements lost their reinforcing eff ect on the weld and their existence was more of an adverse eff ect. The joint without weld reinforcements after the post-weld heat treatment had the optimal tensile properties, and the specimens randomly crack in the weld zone.     

The First Phase of the SRIF Industrialized Base in ＂West Area＂ Has Been Put into Operation

After nearly two years＇ tense construction, the first phase of industrialized base of Shenyang Research Institute of Foundry （SRIF）, located at the Tiexi Casting and Forging Industrial Park in the west of Tiexi District, has now been completed and formally put into operation.     

Thermodynamics Study on the Decomposition of Chromite with KOH

Institute of Process Engineering, Chinese Academy of Sciences, China, has proposed a method for oxidative leaching of chromite with potassium hydroxide. Understanding the mechanism of chromite decomposition, especially in the potassium hydroxide fusion, is important for the optimization of the operating parameters of the oxidative leaching process. A traditional thermodynamic method is proposed and the thermal decomposition and the reaction decomposition during the oxidative leaching of chromite with KOH and oxygen is discussed, which suggests that chromite is mainly destroyed by reactions with KOH and oxygen. Meanwhile, equilibrium of the main reactions of the above process was calculated at different temperatures and oxygen partial pressures. The stable zones of productions, namely, K2CrO4 and Fe2O3, increase with the decrease of temperature, which indicates that higher temperature is not beneficial to thermodynamic reactions. In addition, a comparison of the general alkali methods is carried out, and it is concluded that the KOH leaching process is thermodynamically superior to the conventional chromate production process.     

Influence of Heat Treatment on Damping Behaviour of the Magnesium Wrought Alloy AZ61

The effect of isochronal heat treatments for 1h on variation of damping, hardness and microstructural change of the magnesium wrought alloy AZ61 was investigated. Damping and hardness behaviour could be attributed to the evolution of precipitation process. The influence of precipitation on damping behaviour was explained in the framework of the dislocation string model of Granato and Lücke.     

Effect of Rare Earth Doping on Impedance,Modulus and Conductivity Properties of Multiferroic Composites:0.5(BiLa_xFe_(1-x)O_3)–0.5(PbTiO_3)

The Lanthanum-doped bismuth ferrite–lead titanate compositions of 0.5(Bi LaxFe1-xO3)–0.5(Pb Ti O3)(x = 0.05,0.10,0.15,0.20)(BLxF1-x-PT) were prepared by mixed oxide method.Structural characterization was performed by X-ray diffraction and shows a tetragonal structure at room temperature.The lattice parameter c/a ratio decreases with increasing of La(x = 0.05–0.20) concentration of the composites.The effect of charge carrier/ion hopping mechanism,conductivity,relaxation process and impedance parameters was studied using an impedance analyzer in a wide frequency range(102–106Hz) at different temperatures.The nature of Nyquist plot confirms the presence of bulk effects only,and non-Debye type of relaxation processes occurs in the composites.The electrical modulus exhibits an important role of the hopping mechanism in the electrical transport process of the materials.The ac conductivity and dc conductivity of the materials were studied,and the activation energy found to be 0.81,0.77,0.76 and 0.74 e V for all compositions of x = 0.05–0.20 at different temperatures(200–300 °C).     

Quantitative Analysis of the Crystallographic Orientation Relationship Between the Martensite and Austenite in Quenching–Partitioning–Tempering Steels

The orientation relationships(ORs)between the martensite and the retained austenite in low-and medium-carbon steels after quenching–partitioning–tempering process were studied in this work.The ORs in the studied steels are identified by selected-area electron diffraction(SAED)as either K–S or N–W ORs.Meanwhile,the ORs were also studied based on numerical fitting of electron backscatter diffraction data method suggested by Miyamoto.The simulated K–S and N–W ORs in the low-index directions generally do not well coincide with the experimental pole figure,which may be attributed to both the orientation spread from the ideal variant orientations and high symmetry of the low-index directions.However,the simulated results coincide well with experimental pole figures in the high-index directions{123}_(bcc).A modified method with simplicity based on Miyamoto’s work was proposed.The results indicate that the ORs determined by modified method are similar to those determined by Miyamoto’method,that is,the OR is near K–S OR for the low-carbon Q–P–T steel,and with the increase of carbon content,the OR is closer to N–W OR in medium-carbon Q–P–T steel.     

Using Finite Element and Contour Method to Evaluate Residual Stress in Thick Ti-6Al-4V Alloy Welded by Electron Beam Welding

This work was to reveal the residual stress profile in electron beam welded Ti-6Al-4V alloy plates(50 mm thick) by using finite element and contour measurement methods.A three-dimensional finite element model of 50-mmthick titanium component was proposed,in which a column–cone combined heat source model was used to simulate the temperature field and a thermo-elastic–plastic model to analyze residual stress in a weld joint based on ABAQUS software.Considering the uncertainty of welding simulation,the computation was calibrated by experimental data of contour measurement method.Both test and simulated results show that residual stresses on the surface and inside the weld zone are significantly different and present a narrow and large gradient feature in the weld joint.The peak tensile stress exceeds the yield strength of base materials inside weld,which are distinctly different from residual stress of the thin Ti-6Al-4V alloy plates presented in references before.     

Microstructures and Tensile Properties of Ultrafine-Grained Ni–(1–3.5) wt% SiC_(NP) Composites Prepared by a Powder Metallurgy Route

Silicon carbide nanoparticle-reinforced nickel-based composites(Ni–Si CNP),with a Si CNPcontent ranged from1 to 3.5 wt%,were prepared using mechanical alloying and spark plasma sintering.In addition,unreinforced pure nickel samples were also prepared for comparative purposes.To characterize the microstructural properties of both the unreinforced pure nickel and the Ni–Si CNPcomposites transmission electron microscopy(TEM) was used,while their mechanical behavior was investigated using the Vickers pyramid method for hardness measurements and a universal tensile testing machine for tensile tests.TEM results showed an array of dislocation lines decorated in the sintered pure nickel sample,whereas,for the Ni–Si CNPcomposites,the presence of nano-dispersed Si CNPand twinning crystals was observed.These homogeneously distributed Si CNPwere found located either within the matrix,between twins or on grain boundaries.For the Ni–Si CNPcomposites,coerced coarsening of the Si CNPassembly occurred with increasing Si CNPcontent.Furthermore,the grain sizes of the Ni–Si CNPcomposites were much finer than that of the unreinforced pure nickel,which was considered to be due to the composite ball milling process.In all cases,the Ni–Si CNPcomposites showed higher strengths and hardness values than the unreinforced pure nickel,likely due to a combination of dispersion strengthening(Orowan effects) and particle strengthening(Hall–Petch effects).For the Ni–Si CNPcomposites,the strength increased initially and then decreased as a function of Si CNPcontent,whereas their elongation percentages decreased linearly.Compared to all materials tested,the Ni–Si CNPcomposite containing 1.5% Si C was found more superior considering both their strength and plastic properties.     

Directional Growth of Tin Crystals Controlled by Combined Solute Concentration Gradient Field and Static Magnetic Field

A new method was introduced to achieve directional growth of Sn crystals. Microstructures in liquid(Pb)/liquid(Sn) diffusion couples were investigated under various static magnetic fields. Results show that the β-Sn crystals mainly reveal an irregular dendritic morphology without or with a relatively low static magnetic field(B0.3 T). When the magnetic field is increased to 0.5 T, the β-Sn dendrites close to the final stage of growth begin to show some directional character. With a further increase in the magnetic field to a higher level(0.8–5 T), the β-Sn dendrites have an enhanced directional growth character, but the dendrites show a certain deflection. As the magnetic field is increased to 12 T, the directional growth of the β-Sn dendrites in the center of the couple is severely destroyed. The mechanism of the directional growth of the β-Sn crystals and the deflection of the β-Sn crystals with the application of static magnetic field was tentatively discussed.     

电化学噪声数据处理方法概述

综述了常见的电化学噪声数据处理方法,介绍了直流趋势剔除、统计分析、快速傅立叶变换(FFT)法计算功率谱密度(PSD)以及小波变换处理电化学噪声信号的基本过程,并阐释了各种数学处理及所得参数的物理意义。