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用气体含水量标准物质来校准露点仪器会给校准过程带来很多方便。本文论述了气体含水量标准物质制备的依据、方法,以及制备的条件和不确定度分析。 相似文献
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以自制标准水发生器发生的湿气为测试样品,利用不同的测试样品对两种不同型号的VAISALA电容式湿度传感器进行大量实验。结果表明:正常环境条件下,两种传感器稳定性良好,其输出信号的响应值与水分含量(露点)在特定区间内呈一定的线性关系;VAISALA DRYCAP DMT 152与242两种类型传感器可以分别对露点-80℃和露点-67℃的水分含量给出稳定准确的响应值,前者的检测限要低于后者且适合露点低于-60℃的二氧化碳产品气的测量;使用VAISALA DRYCAP传感器可以满足二氧化碳中微量水分的测定,但需要水标准气体对其进行定期校准。 相似文献
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精密露点仪是露点温度测量中准确度较高的仪器,需要定期开展校准。本文根据JJG499-2004《精密露点仪》的要求,建立DCS低露点校验系统及校准数学模型,介绍了DCS低露点校验系统的组成及工作原理,确定了系统的不确定度来源,给出了该校验系统测量结果的不确定度评定实例。 相似文献
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介绍了目前露点温度传感器领域的研究现状,阐述了光学式、谐振式、电学式、热学式、重量式、化学式露点温度传感器的原理及构造,指出光学式露点温度传感器测量精度极高,其中冷镜式露点仪可作为湿度计量标准;谐振式露点温度传感器具有体积小、成本低、响应时间短、灵敏度高、可靠性好的特点;电学式露点温度传感器灵敏度高、功耗小,便于实现小型化、集成化;重量法是准确度最高的湿度绝对测量方法;化学法常用来测量低湿环境下的有机混合气体。探讨了露点温度传感器在环境监测、工业制造、医疗诊断等领域的应用情况,指出未来露点温度传感器将会向高精度、高稳定性、高响应的方向发展,且应用范围将进一步拓展,以满足极端环境下的测量需求。 相似文献
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R. I. Veltcheva R. L. Rusby D. M. Peters R. E. J. Watkins 《International Journal of Thermophysics》2018,39(5):65
Recently, a requirement arose to provide sensors for measuring the temperature of a substantial reference blackbody cavity to operate in vacuum over a temperature range from ? 100 °C to 80 °C (~?170 K to ~?350 K), with an additional capability to operate at ~? 170 °C (~?100 K) as a point of near-zero radiance. Several 100 Ω industrial platinum resistance sensors (Pt100) are required for control purposes in order to establish the temperature uniformity of the blackbody structure and its surrounding aluminum-alloy isothermal shield. These sensors should remain stable within the uncertainties of 0.03 °C (k?=?3) ideally for 20 years. This paper discusses the testing and calibration of two types of industrial Pt100 resistors, including checking the interchangeability of sensors from a given batch, and the methods of interpolation over the temperature range. It is concluded that the sensors can meet the requirements provided that they have been individually tested, and that there is a degree of duplication of sensors so that long-term changes can be detected. The calibration data could be fitted by cubic or quartic equations expressing temperature as a function of resistance (or resistance ratio), this being simpler than the ITS-90 formulation and more convenient than using the (technically obsolete) Callendar–Van Dusen equation. 相似文献
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Evolved vapor coulometry is a measurement technique that selectively detects water and is used to measure water content of materials. The basis of the measurement is the quantitative electrolysis of evaporated water entrained in a carrier gas stream. Although this measurement has a fundamental principle—based on Faraday’s law which directly relates electrolysis current to amount of substance electrolyzed—in practice it requires calibration. Commonly, reference materials of known water content are used, but the variety of these is limited, and they are not always available for suitable values, materials, with SI traceability, or with well-characterized uncertainty. In this paper, we report development of an alternative calibration approach using as a reference the water content of humid gas of defined dew point traceable to the SI via national humidity standards. The increased information available through this new type of calibration reveals a variation of the instrument performance across its range not visible using the conventional approach. The significance of this is discussed along with details of the calibration technique, example results, and an uncertainty evaluation. 相似文献
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目前大气环境传感器的测试和标定主要依赖于人工手动操作完成,测试和标定效率较低,结果准确率较差。为解决该问题,在分析大气环境传感器工作原理的基础上,搭建了一套由真空泵电机、气压控制器、高低温箱、金属密封腔、标准数字温度计、工控机、待标定大气环境传感器等部分组成的大气环境传感器硬件测试平台,并设计了大气环境自动化软件测试系统,通过工控机控制标准环境,对标准环境参数进行周期采样,自动判定稳态并记录标定所需参数,从而拟合出标定曲线。对待标定温度和压力传感器进行自动化标定测试,结果显示:温度标定的拟合相关系数为0.994 5,重复性误差为0.087%;压力标定的拟合相关系数为0.996,重复性误差为0.046%,验证了测试系统的可行性。此研究成果为大气环境传感器快速部署应用提供了有力支撑,对于推动自动化技术在大气环境参数测量领域中的应用具有重要意义。 相似文献
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气体中水蒸气含量测量在工业生产和科研领域发挥至关重要的作用。随着许多工业生产和科研领域对气体水分含量更加严格的测试要求,对于气体中水蒸气含量测量灵敏度的要求也越来越高。目前测量nmol/mol痕量水分的仪器方法有可调谐二极管激光吸收光谱法、光腔衰荡光谱法、大气压离子质谱仪法;达到这个痕量水平的传感器类测量技术有石英晶体微天平法、冷镜露点法、阻容法、电解法。针对这些测量方法的优缺点以及今后的发展趋势进行了论述分析,通过克服测量过程中的干扰因素,可在一定的程度上提高痕量水含量的测量准确性,对促进痕量水含量准确测量技术的发展有所裨益。 相似文献