Application of two-output port fiber coupler as gasoline level sensor

Detection of gasoline level can be done in a safe and simple way using two output port multimode fiber coupler with a structure of 2 × 2 as a sensor. Two output ports (sensing port) are connected with two reflector displacement device (RDD) and functioned as two probes. These probes are placed on the wall of gasoline tank in a storied and work interchangeably or together depending on setting of these probes. Detection mechanism of the system is based on changes in intensity of reflected light from the reflector RDD that shifts due to changes in level of gasoline (hydrostatic pressure principle). Changes in intensity of light coming into the sensing port are then forwarded to the optical detector. Experiments performed by varying the location of the second probe as 45 cm, 50 cm, and 55 cm above the first probe to detect the level of gasoline in the process of filling and emptying the tank. Experimental results show the process of filling and emptying the tank have small differences of 6% with the dynamic range, the linear region, and resolution are 100 cm, 70 cm, and 0.4 cm respectively. Sensor sensitivity in filling and emptying process of the tank are 2.7 mV/cm and 2.8 mV/cm respectively. These results were the best performance of the sensor, which occurs when the level of the second probe was 55 cm above the first probe.     

An all-fiber Fabry-Pérot interferometer for pressure sensing in different gaseous environments

A gas pressure sensor based on an all-fiber Fabry-Pérot interferometer (FFPI) is reported. The sensing head consists of a small section of silica rod spliced with a large offset between two single-mode fibers. The silica rod is used only as mechanical support so that an air cavity can be formed between both SMF. It is shown that the FFPI sensor is sensitive to gas pressure variation and when submitted to different gaseous environments, namely carbon dioxide, nitrogen and oxygen – sensitivities of 6.2, 4.1 and 3.6 nm/MPa, respectively, were attained. The refractive index change on nitrogen environment by means of gas pressure variation was also determined and a sensitivity of 1526 nm/RIU was obtained. The response of the sensing device to temperature variations in air was also studied and a sensitivity of −14 pm/°C was attained.     

Simultaneous distributed measurement of the strain and temperature for a four-point bending test using polarization-maintaining fiber Bragg grating interrogated by optical frequency domain reflectometry

We demonstrate a simultaneous distributed strain and temperature measurement technique with the spatial resolution of 1 mm using fiber Bragg gratings inscribed in a polarization-maintaining and absorption-reducing fiber (PANDA-FBGs) and optical frequency domain reflectometry (OFDR). We conduct four-point bending tests in an environmental chamber. Using high birefringent PANDA-FBGs that are manufactured specifically for the simultaneous measurements, the uniform temperature distributions and the typical strain distribution profiles of the four-point bending tests were successfully obtained. The measurement errors of strain were from −31 με to 19 με, and of temperature were from −0.9 °C to 1.3 °C. The spatial standard deviation was 7.5 με and 0.9 °C. We also discussed the effect of the residual strain of the sensor-bonding procedures and the data averaging.     

Effect on crystalline structure of AISI M2 steel using tungsten–thorium electrode through MRR,EWR, and surface finish

To investigate on the crystalline structure of AISI M2 steel by using tungsten–thorium electrode in electrical discharge machining (EDM) process was studied. Furthermore, the investigation were carried out for finding the value of material removal rate (MRR), electrode wear rate (EWR) and surface roughness (SR) of tool steel material depending upon three variable input process parameters. On the basis of weight loss, the value of MRR and EWR were calculated at optimized process parameter. Subsequently, surface topography of the processed material were examined through different characterization techniques like scanning electron microscopy (SEM), Optical surface profiler (OSP) and Atomic force microscopy (AFM), respectively. In XRD study, broadening of the peak was observed which confirmed the change in material properties due to the homogeneous dispersion of the particles inside the matrix. Lowest surface roughness and MRR of 0.001208 mg/min was obtained. Minimum surface roughness was obtained 1.12 μm and 2.18427 nm by OSP and AFM study, respectively. Also, minimum EWR was found as 0.013986 mg/min.     

Measurement of the neutral plane of an internal fire whirl using the background-oriented Schlieren technique for a vertical shaft model of a high-rise building

Since the height of the neutral plane is related to the direction of the high-temperature smoke and airflow diffusion of fires in high-rise buildings, the identification of the neutral plane is important for both the evacuation of residents and the safety of fire fighters. As yet, there are no effective methods for directly measuring the constantly changing neutral plane position. There are complex internal fire whirl phenomena in the inner space in particular cases. In this study, the background-oriented Schlieren (BOS) technique was used to visualize the neutral plane when a fire whirl occurs in a vertical shaft with a single corner gap. With n-propanol used as the fuel, the scale modeling experiments of fuel trays 5.8 cm and 7 cm in diameter were tested in a 34 cm (W) × 35 cm (L) × 145 cm (H) model for open and covered roof types. It is observed in the experimental process that the height of the neutral plane changes dynamically as the fire whirl is formed. The thermocouples were used to measure the temperature variation at different heights of openings to validate the measurement accuracy of the BOS technique. It is found that once a fire whirl occurs in the inner space of a high-rise building, the height of the neutral plane increases instantly. The experimental results demonstrate that the BOS technique can measure the neutral plane position of a large-scale model of a high-rise building fire scene directly, immediately and accurately.     

Performance analysis of a DRL-less AFE for battery-powered wearable EEG

The driven-right-leg (DRL) circuit has been commonly used in the wall-powered EEG systems to reduce common-mode interference in the bio-potential amplifier. However, DRL circuit imposes limitations on the number of channels preventing modular development, and its effectiveness is diminished for a newer generation of battery-powered EEG systems. We present a performance investigation of DRL-less EEG circuit by designing a single-channel EEG with a novel Analog Front End (AFE) that contains a differential amplifier followed by a high-Q active notch filter. The prototyped wearable EEG system has been validated to record neural signals with and without the DRL circuit. The time domain and frequency domain signals show that the designed AFE is not impacted significantly (maximum 4 dB difference) by the DRL elimination and maintains similar signal quality. The customized EEG with and without DRL offers CMRR of 72.98 dB and 71.74 dB, respectively, at 60 Hz (power-line interference range in the USA), whereas CMRR of 72.64 dB and 71.01 dB, respectively, at 20 Hz (representative EEG signal range). DRL elimination allows us to envision a sensor-level modular EEG system for neural monitoring in non-clinical environments.     

Design and Analysis of MEMS Comb Drive Capacitive Accelerometer for SHM and Seismic Applications

This work presents the design of a MEMS accelerometer that is specifically intended for Structural Health Monitoring (SHM) applications where sensing low frequency low amplitude accelerations with high resolution is essential. The surface micromachined comb drive capacitance accelerometer structure has been considered in this design. The simulation experiments conducted on these devices using IntelliSuite MEMS design tool show that it has excellent displacement sensitivity of 21.39 μm/g, a capacitive sensitivity of 1.22 pF/g and voltage sensitivity of 1783 mV/g/V when it is designed to measure 0–0.1 g. Further, it is seen that it has a very low noise floor of 1.32 μg/√Hz and therefore high resolution. Since the accelerations can be as low as 0.04 g in SHM applications, excellent resolution is the primary goal in this design. Further, one more sensor specifically meant for strong motion seismic application has also been reported. This device has a bandwidth of 0–250 Hz and a noise floor of 5.612 μg/√Hz in addition to a sensor level voltage sensitivity of 97.9 mV/g/V. Finally, the comparison of these results with other similar devices reported in the past clearly illustrates the comparable performance of the present devices. Further, these devices, unlike the commercial low frequency accelerometers and other similar devices reported in the past can be fabricated by surface micromachining and CMOS compatible processes.     

Thermopower detection of single nanowire using a MEMS device

We present a MEMS-based device on a silicon nitride membrane in order to measure the thermoelectric properties of a single nanowire. A temperature gradient along a nanowire was generated by a nanoheater, and the temperature was measured by Pt thermometers. A thermal simulation using a finite element method was conducted to analyze the temperature distribution over the MEMS device. The validity of the MEMS device was established by testing the Pt nanowires which had different symmetry configurations. From the test results of Pt nanowires, a convincing temperature calibration method was proposed and applied to an actual case of Bi₂Te₃ nanowire. We measured a Seebeck coefficient of −53 μV/K and electrical conductivity of 2.23 × 10⁵ S/m for a single Bi₂Te₃ nanowire with a diameter of 70 nm at 300 K. Our solid design for thermoelectric measurements based on a membrane structure enables the fast and high-yield characterization of one-dimensional nanostructures.     

Silver nanoparticles/polymethacrylic acid (AgNPs/PMA) hybrid nanocomposites-modified electrodes for the electrochemical detection of nitrate ions

AgNPs/PMA hybrid nanocomposite materials with different Ag loadings have been synthesized using a simple chemical route assisted by UV irradiation. The hybrid composites were characterized by means of SEM and TEM, UV–vis spectroscopy and XPS. The as synthesized hybrid samples, composed of small Ag nanoparticles (AgNPs) embedded within the PMA (poly-methacrylic-acid) matrix, have been used to modify the working electrode of disposable screen printed carbon electrodes (SPCEs). It has been observed that hybrid composite with the lowest Ag loading forms dendritic silver structures on the surface of working electrode, whereas at higher loadings massive structures were formed. The electrocatalytic properties of the AgNPs/PMA/SPCEs were investigated toward the reduction of nitrate at neutral pH. Based on these modified electrodes, both voltammetric and amperometric sensors were developed for the electrochemical sensing of nitrate. Voltammetric sensor showed a wide linear range (0–20 mM) and high sensitivity (130 μA mM⁻¹ cm⁻²).     

Nanometric cutting in a scanning electron microscope

A nanometric cutting device under high vacuum conditions in a scanning electron microscope (SEM) was developed. The performance, tool-sample positioning, and processing capacity of the nanometric cutting platform were studied. The proposed device can be used to realize a displacement of 7 μm, with a closed-loop resolution of 0.6 nm in both the cutting direction and the depth direction. Using a diamond cutting tool with an edge radius of 43 nm formed by focused ion beam (FIB) processing, nanometric cutting experiments on monocrystalline silicon were performed on the developed cutting device under SEM online observation. Chips and machining results of different depths of cut were studied during the cutting process, and cutting depths of less than 10 nm could be obtained with high repeatability. Moreover, the cutting speed was found to exhibit a strong relationship with the brittle–ductile transition depth on brittle material. The experimental results of taper cutting and sinusoidal cutting indicated that the developed device has the ability to perform multiple degrees of freedom (DOFs) cutting and to study nanoscale material removal behaviour.     

Parallel-kinematics XYZ MEMS part 2: Fabrication and experimental characterization

This paper, the second of a set of two papers addressing parallel-kinematics MEMS stages for spatial translation, deals with fabrication, characterization and control of such devices. Double device layer SOI (silicon-on-insulator) substrates are used, providing three layers (two device layers and the handle) into which the elements of the stage can be mapped. Using the mechanism concept, realization scheme, and kinematic and dynamic models developed in the first paper of this set, this paper provides a detailed approach to fabricating these devices. The stages fabricated have a workspace cube of roughly 20 μm on the side, an in-plane stiffness of 96 N/m, and an out-of-plane stiffness of 166 N/m. Further, it characterizes the performance of the individual actuating and sensing elements, configures feedback controllers for each actuated joint, and assesses and verifies the stage’s designed performance. Finally, it demonstrates full 3-axis, closed-loop positioning of a MEMS stage.     

Gasoline level sensor based on displacement sensor using fiber coupler

A simple and fire safe gasoline level sensor has been designed based on displacement sensor using fiber coupler. The sensing principle is to detect displacement of reflector, which is attached to membrane (reflector displacement device), due to the change of gasoline hydrostatic pressure. The displacement of reflector can be detected using fiber coupler from the change of optical power light reflected by the reflector. Three kinds of reflector displacement device used in this experiment are one-layer, two-layer, and three-layer membrane. The experimental results are 0–180 cm of dynamic range, 100–140 cm of linear range, 3.2 mV/cm of sensitivity, and 0.6 cm of resolution for reflector displacement device with one-layer membrane for emptying the tank process. The hysteresis data for emptying and filling the tank process yields the mean of difference 20% for one-layer membrane.     

Energy harvester for a wireless sensor in a boiler environment

Wireless sensors have become a focus of study in the field of measurement technologies. The power supply of many wireless sensors is based on batteries or external power sources. However, there is increasing interest in finding solutions where the batteries can be leaved away and the power for the wireless sensors is produced from the environment in which the sensors operate. The technologies required are called energy harvesting or scavenging technologies.This paper introduces the principles, modeling and a practical implementation of a self-powering solution for a wireless sensor for energy boilers or other hot reactor vessels. With the aid of energy solution introduced, the wireless sensor can operate autonomously without any batteries. One of the design targets in this work was that the top part of harvester’s mechanics must fit to the opening or assembly tube of diameter less than 15 mm in the boiler wall reserved for standard instrument assemblies. So the top of harvester collects and conducts thermal energy to element generating electricity from it. The harvester and further the measuring and communication electronics are mounted outside the hot area.The harvester solution introduced in the paper can produce about 114 mW power, when top of harvester mechanics was inserted to the test oven heated to temperature of +500 °C. The sensor function or type is not defined nor limited in this study. The electric energy generated by harvester can be used to power, for example, temperature, heat flux, flow, vibration or other little energy needing sensors.     

1 Ω and 10 kΩ high precision transportable setup to calibrate multifunction electrical instruments

A temperature controlled 1 Ω and 10 kΩ transportable setup was developed at National Institute of Metrological Research (INRIM) for the calibration and adjustment of multifunction electrical instruments as digital multimeters (DMMs) and multifunction calibrators (MFCs). The two standards are made of two 10 Ω and 100 kΩ resistor nets connected in parallel and inserted in a temperature controlled aluminum structure. Novelties of the realization are the oil insertion of the 1 Ω net with the internal side of the connectors lowering the thermo-electromotive forces (EMFs) effects, and the possibility to know instantly the temperatures of the environment, of the internal of the structure and the last calibration values of the 1 Ω and10 kΩ standards. Short- and mid-term stabilities of the setup standards resulted on the order and in some cases better than other metrology-grade 1 Ω and 10 kΩ commercial items. The transport of the setup even turning off its temperature control did not cause appreciable measurement variations on the two standards. The standards uncertainties meet those requested by DMMs and MFCs manufacturers to calibrate and adjust these instruments. A test to adjust a MFC gave satisfactory results.     

Identification and characterisation of steel corrosion using passive high frequency RFID sensors

High frequency RFID sensors are attractive in diverse applications where sensor performance is required at a low cost and dimension restriction. An approach adapting commercial passive 13.56 MHz RFID tags has been developed for sensing corrosion stage. This investigation includes balance of sensing and positioning of RFID sensors for corrosion detection by analysing real and imaginary parts of the complex impedance. With passive HF RFID sensors, real part and imaginary part of complex impedance have been extracted from the reader coil with VNA (vector network analyser) and delivering a unique capability for corrosion sensing with different atmospheric exposure time steel samples (1 month, 6 months, 10 months and 12 months). With different positioning (5–25 mm), features extraction based on the complex impedance with PCA (principal component analysis) has been designed for position-independent corrosion evaluation.     

Modified nanoporous carbon as a novel sorbent before solvent-based de-emulsification dispersive liquid–liquid microextraction for ultra-trace detection of cadmium by flame atomic absorption spectrophotometry

Combination of different extraction methods is an interesting work in the field of sample pretreatment. In the current study, for the first time, solid phase extraction combined with solvent-based de-emulsification dispersive liquid–liquid microextraction (SPE-SD-DLLME) was developed for preconcentration and trace detection of cadmium in water samples using flame atomic absorption spectrophotometry (FAAS). The adsorbed cadmium ions on prepared SPE (75 mL of aqueous solution) were eluted by optimized elution solvent and introduced to the second microextraction step. The effective variables of SPE including the pH of sample, flow rates, type, concentration and volume of the eluent and the effect of potentially interfering ions of the separation of cadmium were evaluated and optimized. Also, several factors that influence the SD-DLLME step such as pH, neocuproine concentration (the cadmium binding ligand), type of dispersed/de-emulsifier solvent, volume of disperser/de-emulsifier solvent and type and volume of extraction solvents were investigated. SPE-SD-DLLME provides a preconcentration factor of 165 for cadmium ions. Calibration plot was linear in the range of 0.1–50 μg L⁻¹ with correlation of determination (r²) of 0.988. The precision and limit of detection of proposed method were 5.1% (RSD%, n = 8) and 0.03 μg L⁻¹, respectively.     

Determination of haloperidol drug in ampoules and in urine samples using a potentiometric modified carbon paste electrode

A modified carbon paste electrode for haloperidol drug based on haloperidol-phosphomolybdate (HP-PM) as an ion-exchanger dissolved in plasticizer DBP and its potentiometric characteristics were discussed. The electrode exhibited a good Nernstian slope of 56.9 ± 0.3 mV/decade with a linear concentration range from 3.2 × 10⁻⁶ to 1.0 × 10⁻² M for the haloperidol ion. The limit of detection (LOD) was 1.5 × 10⁻⁶ M. It had response time of 5–8 seconds (s), useable in pH range of 6.2–8.6 and temperature of 20–60 °C. The electrode shows clear discrimination of haloperidol drug from several inorganic ions, sugars and some common drug excipients. The sensor was applied for determination of haloperidol drug in urine and in pharmaceutical formulations using potentiometric determination, standard addition and the calibration curve methods. The results are satisfactory with excellent percentage recovery comparable or better than those obtained by other routine methods.     

Design and characterization of a real-time,wearable, endosomatic electrodermal system

This paper presents the design and characterization of a compact wearable system for long-term assessment of skin potential response, with the aim of monitoring mental stress in a variety of applications. Literature reports that the expected skin potential has peak-to-peak amplitudes of few millivolts in the frequency band [0.1, 10] Hz. The designed system is characterized by a slightly wider bandwidth of [0.08, 40] Hz, and it is based on a 12-bit ADC working with a sampling rate of 200 Sa/s, which can be increased up to 3.5 kSa/s. Data can be continuously acquired for up to 40 h with a battery of 3.7 V/1800 mAh. A Graphical User Interface was also developed for the host computer in .NET framework. The system, to our knowledge the first example of wearable endosomatic electrodermal activity sensor, joins to several skin conductance wearable measuring systems recently proposed in literature, and opens up opportunities for future comparisons of endosomatic and exosomatic responses in real life.The device is thoroughly characterized in accordance with the state-of-the-art of the metrological research in the field.     

Effect of CuO as a dopant in TiO2 on ammonia and hydrogen sulphide sensing at room temperature

The heterogeneous nanocomposites of CuO doped TiO₂ nanoparticles were synthesized using sol gel method by varying the concentration of CuO as 0.1, 0.5 and 1 mol% for the sensing of ammonia and hydrogen sulphide. The substitutional doping of CuO in TiO₂ matrix was confirmed by the X-ray diffraction. Average crystallite size of the doped nanocomposites was found to reduce with increase in concentration of CuO. The 0.1 mol% CuO doped TiO₂ nanocomposites showed highest sensitivity to ammonia (97%) with response time of 2 s, while 1 mol% was selective to H₂S gas (77%) with response time of 45 s for 50 ppm of each gas at room temperature.     

Performance tests of a new non-invasive sensor unit and ultrasound electronics

Industrial applications involving pulsed ultrasound instrumentation require complete non-invasive setups due to high temperatures, pressures and possible abrasive fluids. Recently, new pulser-receiver electronics and a new sensor unit were developed by Flow-Viz. The complete sensor unit setup enables non-invasive Doppler measurements through high grade stainless steel. In this work a non-invasive sensor unit developed for one inch pipes (22.5 mm ID) and two inch pipes (48.4 mm ID) were evaluated. Performance tests were conducted using a Doppler string phantom setup and the Doppler velocity results were compared to the moving string target velocities. Eight different positions along the pipe internal diameter (22.5 mm) were investigated and at each position six speeds (0.1–0.6 m/s) were tested. Error differences ranged from 0.18 to 7.8% for the tested velocity range. The average accuracy of Doppler measurements for the 22.5 mm sensor unit decreased slightly from 1.3 to 2.3% across the ultrasound beam axis. Eleven positions were tested along the diameter of the 48.4 mm pipe (eight positions covered the pipe radius) and five speeds were tested (0.2–0.6 m/s). The average accuracy of Doppler measurements for the 48.4 mm sensor unit was between 2.4 and 5.9%, with the lowest accuracy at the point furthest away from the sensor unit. Error differences varied between 0.07 and 11.85% for the tested velocity range, where mostly overestimated velocities were recorded. This systematic error explains the higher average error difference percentage when comparing the 48.4 mm (2.4–5.9%) and 22.5 mm (1.3–2.3%) sensor unit performance. The overall performance of the combined Flow-Viz system (electronics, software, sensor) was excellent as similar or higher errors were typically reported in the medical field. This study has for the first time validated non-invasive Doppler measurements through high grade stainless steel pipes by using an advanced string phantom setup.